Method for the manufacture of soil modifiers from waste materials of the
manufacture of titanium dioxide
    2.
    发明授权
    Method for the manufacture of soil modifiers from waste materials of the manufacture of titanium dioxide 失效
    从二氧化钛生产废料制造土壤改性剂的方法

    公开(公告)号:US4077794A

    公开(公告)日:1978-03-07

    申请号:US775683

    申请日:1977-03-08

    IPC分类号: C05D9/00 C09K17/02

    CPC分类号: C05D9/00 C09K17/02 Y10S71/903

    摘要: A soil modifier comprising from 80 to 95% by weight of a mixture of ferric oxide and ferric sulphate in an oxide/sulphate weight ratio of from 0.25:1 to 1:1, is prepared by calcining at 500.degree.-600.degree. C in an oxidizing atmosphere a blend of by-product obtained in the manufacture of titanium oxide by the sulphate process, with at least 20% by weight with respect to said by-product, of a material based on ferric sulphate and/or ferric oxide. Calcining is then continued under the same conditions, replacing said material in the blend continuously fed in by a recycle fraction of the product continuously discharged.

    摘要翻译: 通过在500-600℃下煅烧,通过在氧化物/硫酸盐重量比为0.25:1至1:1的温度下煅烧80至95重量%的氧化铁和硫酸铁的混合物, 在氧化气氛中,通过硫酸盐法制备氧化钛中获得的副产物与相对于所述副产物的至少20重量%的基于硫酸铁和/或氧化铁的材料的共混物。 然后在相同的条件下继续煅烧,将连续排出的产品的再循环部分连续进料的共混物中的所有材料置换。

    Process for the purification of titanium tetrachloride
    7.
    发明授权
    Process for the purification of titanium tetrachloride 失效
    四氯化钛净化方法

    公开(公告)号:US3939244A

    公开(公告)日:1976-02-17

    申请号:US309828

    申请日:1972-11-27

    IPC分类号: C01G23/02 C22B34/12

    摘要: Process for the purification of titanium tetrachloride, in which the said titanium tetrachloride is brought into contact with a purifying agent consisting of an inert support in granular form on which metallic sodium or other reducing metal has been deposited in sub-divided form, the said contact taking place either on crude liquid titanium tetrachloride with subsequent distillation to recover the purified titanium tetrachloride or on crude vaporised titanium tetrachloride with subsequent condensation to recover the purified titanium tetrachloride.

    摘要翻译: 四氯化钛的纯化方法,其中所述四氯化钛与由分散形式沉积金属钠或其它还原金属的颗粒形式的惰性载体组成的净化剂接触,所述接触 在粗液四氯化钛上进行,随后进行蒸馏以回收纯化的四氯化钛或粗汽化的四氯化钛,随后冷凝以回收纯化的四氯化钛。

    Method for the manufacture of soil modifiers from waste material of the
manufacture of titanium dioxide
    10.
    发明授权
    Method for the manufacture of soil modifiers from waste material of the manufacture of titanium dioxide 失效
    用于制造二氧化钛制造废物的土壤改性剂的方法

    公开(公告)号:US4045205A

    公开(公告)日:1977-08-30

    申请号:US703144

    申请日:1976-07-07

    CPC分类号: C01G49/00 Y10S71/903

    摘要: Soil modifiers comprising from 80 to 95% by weight of a mixture of ferric oxide and ferric sulphate in an oxide/sulphate weight ratio of from 0.2:1 to 2:1 are prepared by calcining at 500.degree.-600.degree. C in the presence of an oxidizing gas a material consisting essentially of ferrous sulphate with an average number of molecules of crystallization of from 1 to 5 obtained by partial dehydration of the waste materials, consisting essentially of ferrous sulphate heptahydrate, obtained in the manufacture of titanium dioxide from ilmenites or ilmenite slags by the sulphate process. These modifiers are particularly suitable for clay soils.

    摘要翻译: 包含80至95重量%氧化铁和硫酸铁的氧化物/硫酸盐重量比为0.2:1至2:1的混合物的土壤改性剂通过在500-600℃下,在存在 一种氧化气体,一种主要由硫酸亚铁组成的材料,其平均结晶分子数为1至5,通过废料的部分脱水获得,其基本上由硫酸亚铁七水合物制成,其由钛铁矿或钛铁矿制造二氧化钛 硫酸盐过程渣。 这些改性剂特别适用于粘土。