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    Method for producing dispersions and use thereof
    1.
    发明授权
    Method for producing dispersions and use thereof 有权
    分散体的制造方法及其用途

    公开(公告)号：US08497315B2

    公开(公告)日：2013-07-30

    申请号：US12515393

    申请日：2007-11-15

    Applicant: Hongli Willimann ,  Jakob Wolfisberg ,  Ulf Kehrer

    Inventor： Hongli Willimann ,  Jakob Wolfisberg ,  Ulf Kehrer

    IPC: C08F2/24

    CPC classification number: C08F2/24

    Abstract: The present invention pertains to a process for the preparation of aqueous dispersions which are stabilized with a water-insoluble stabilizing colloid, characterized in that a) in a first step a water-insoluble stabilizing colloid is prepared, with this being prepared, based on the amount of monomer used for the preparation of the stabilizing colloid, by means of radical polymerization, followed by b) the addition of at least one further olefinically unsaturated monomer and at least one initiator, in which process by means of radical polymerization of the further olefinically unsaturated monomer an aqueous dispersion is obtained, on which c) optionally a residual monomer reduction is performed, with this being carried out by means of polymerization of residual monomers and/or by means of physical removal of the residual monomers and optionally further volatile organic components by means of the introduction of vapor and/or gas.

    Abstract translation: 本发明涉及一种制备用水不溶性稳定胶体稳定的水分散体的方法，其特征在于：a）在第一步中制备水不溶性稳定胶体，基于 用于制备稳定胶体的单体的量，通过自由基聚合，然后b）加入至少一种其它烯属不饱和单体和至少一种引发剂，其中通过进一步烯属的自由基聚合 不饱和单体获得水分散体，其中c）任选地进行残余单体还原，其中通过残余单体的聚合和/或通过物理除去残余单体和任选的其它挥发性有机组分进行 通过引入蒸气和/或气体。

    Dispersion compositions for tile adhesives
    2.
    发明申请
    Dispersion compositions for tile adhesives 有权
    瓷砖粘合剂用分散组合物

    公开(公告)号：US20090192242A1

    公开(公告)日：2009-07-30

    申请号：US11909194

    申请日：2006-03-13

    Applicant: Hongli Willimann ,  Hans Wicki ,  Ulf Kehrer

    Inventor： Hongli Willimann ,  Hans Wicki ,  Ulf Kehrer

    IPC: C08K3/00 ,  C08L67/00

    CPC classification number: C04B40/0042 ,  C04B24/2623 ,  C04B2103/0057 ,  C04B2103/0065 ,  C04B2111/00672 ,  C04B2111/62 ,  C04B2111/72 ,  C08L31/04 ,  C08L2666/04 ,  C09D131/04 ,  C09J131/04 ,  Y02W30/97 ,  C04B14/06 ,  C04B14/106 ,  C04B14/28 ,  C04B18/24 ,  C04B24/2647 ,  C04B24/2652 ,  C04B24/2688 ,  C04B24/383 ,  C04B2103/0088 ,  C04B2103/12 ,  C04B2103/22 ,  C04B2103/30 ,  C04B2103/304 ,  C04B2103/44

    Abstract: The invention relates to an aqueous dispersion and dispersion powder composition for highly flexible, waterproof, hydraulically binding tile adhesives having an extended open time, and containing an emulsion polymer (A) having a glass transition temperature (Tg) of approximately 10° C. to 80° C., and an emulsion polymer (B) having a glass transition temperature (Tg) of approximately −60° C. to +20° C. The difference of the glass transition temperatures (Tg) of the emulsion polymers (A and B) is at least approximately 5° C. The proportion of vinyl acetate monomer units is 0 to 70 mol-% and the minimum film forming temperature according to DIN 53787 of the 50% aqueous dispersion composition is approximately 15° C. or less, and the monomers, stabilization systems and optionally the additional additives of the dispersion and/or dispersion powder composition are selected such that a good cement compatibility is guaranteed. Due to the inventive dispersion and dispersion powder composition, tile adhesive can be produced in an economical manner which meets the requirements of C2S2- and C2ES2-norm according to EN12004.

    Abstract translation: 本发明涉及一种水性分散体和分散体粉末组合物，其用于具有延长的开放时间的高柔性，防水，水硬性粘合剂粘合剂，并且含有玻璃化转变温度（Tg）为约10℃至约10℃的乳液聚合物（A） 80℃的玻璃化转变温度（Tg）和玻璃化转变温度（Tg）约为-60℃至+ 20℃的乳液聚合物（B）。乳液聚合物（A和 B）为至少约5℃。乙酸乙烯酯单体单元的比例为0-70mol％，50％水分散体组合物根据DIN 53787的最低成膜温度为约15℃或更低， 并且选择分散体和/或分散体粉末组合物的单体，稳定体系和任选的另外的添加剂，使得保证良好的水泥相容性。 由于本发明的分散和分散粉末组合物，瓦片粘合剂可以以符合EN12004的C2S2-和C2ES2-norm的要求的经济方式生产。

    METHOD FOR PRODUCING DISPERSIONS AND USE THEREOF
    4.
    发明申请
    METHOD FOR PRODUCING DISPERSIONS AND USE THEREOF 有权
    生产分散体的方法及其用途

    公开(公告)号：US20100081736A1

    公开(公告)日：2010-04-01

    申请号：US12515393

    申请日：2007-11-15

    Applicant: Hongli Willimann ,  Jakob Wolfisberg ,  Ulf Kehrer

    Inventor： Hongli Willimann ,  Jakob Wolfisberg ,  Ulf Kehrer

    IPC: C08L23/00 ,  C08L31/00 ,  C08L41/00 ,  C08L33/26 ,  C08L43/04 ,  C08L39/06 ,  C08L1/00 ,  C08L1/26 ,  C08L3/08 ,  C08L5/00

    CPC classification number: C08F2/24

    Abstract: The present invention pertains to a process for the preparation of aqueous dispersions which are stabilised with a water-insoluble stabilising colloid, characterised in that a) in a first step a water-insoluble stabilising colloid is prepared, with this being prepared, based on the amount of monomer used for the preparation of the stabilising colloid, by means of radical polymerization of a1) about 1 to 90 wt. % of at least one olefinically unsaturated monomer, containing at least one sulfate and/or sulfonate group, which optionally may be protonated, a2) about 5 to 99 wt. % of at least one olefinically unsaturated monomer with a water solubility at 20° C. of less than 50 g/l, and a3) up to 50 wt. % of at least one olefinically unsaturated monomer with a water solubility at 20° C. of more than 50 g/l, in water, followed by b) the addition of at least one further olefinically unsaturated monomer and at least one initiator, in which process by means of radical polymerization of the further olefinically unsaturated monomer an aqueous dispersion is obtained, on which c) optionally a residual monomer reduction is performed, with this being carried out by means of polymerization of residual monomers and/or by means of physical removal of the residual monomers and optionally further volatile organic components by means of the introduction of vapour and/or gas. The dispersions obtained in this manner can be converted into water-redispersible polymer powders with the aid of drying. Moreover, the invention pertains to the use of the water-insoluble stabilising colloid, the dispersion, and the water-redispersible polymer-powder.

    Abstract translation: 本发明涉及一种制备用水不溶性稳定胶体稳定的水分散体的方法，其特征在于：a）在第一步中制备水不溶性稳定胶体，基于 用于制备稳定胶体的单体的量，通过a1）约1-90wt。％的自由基聚合。 至少一种含有至少一种硫酸盐和/或磺酸盐基团的烯属不饱和单体的％，其任选地可被质子化，a2）约5至99重量％ ％的至少一种在20℃下的水溶性低于50g / l的烯属不饱和单体和a3）至多50wt。 ％的至少一种在20℃下具有大于50g / l水溶性的烯属不饱和单体，在水中，然后b）加入至少一种其它烯属不饱和单体和至少一种引发剂，其中 通过进一步的烯属不饱和单体的自由基聚合，获得水分散体的方法，其中c）任选地进行残余单体还原，其中通过残余单体的聚合和/或通过物理去除 的残余单体和任选地通过引入蒸气和/或气体的其它挥发性有机组分。 以这种方式获得的分散体可借助于干燥转化为水可再分散的聚合物粉末。 此外，本发明涉及水不溶性稳定胶体，分散体和水分散性聚合物粉末的用途。

    Dry cement formulation for cementing holes in the earth
    5.
    发明授权
    Dry cement formulation for cementing holes in the earth 有权
    干式水泥配方，用于泥土钻孔

    公开(公告)号：US08393391B2

    公开(公告)日：2013-03-12

    申请号：US12515195

    申请日：2007-11-15

    Applicant: Hongli Willimann ,  Franck Vallee ,  Charles Zhang

    Inventor： Hongli Willimann ,  Franck Vallee ,  Charles Zhang

    IPC: E21B33/138 ,  C04B11/30 ,  C04B7/02

    CPC classification number: C04B40/0608 ,  C04B14/06 ,  C04B24/2641 ,  C04B24/2676

    Abstract: The present invention pertains to a dry cement formulation for cementing earth boreholes, in particular oil, gas and/or terrestrial heat boreholes, containing a) about 20 to 99.9 wt. % cement, b) about 0 to 65 wt. % powdered quartz/or quartz dust, c) about 0.1 to 30 wt. % water-redispersible dispersion powder, and d) about 0 to 20 wt. % further additives. Furthermore, the invention pertains to the use of the dry cement formulation for preparing a cement slurry as well as to the use of water-redispersible dispersion powders in a cement slurry for cementing earth boreholes, wherein the cement slurries can be used for reducing the water loss of the cement slurry, for reducing the gas and/or water penetration and/or for sealing off the gas and/or water channels by means of the cement slurry which has been introduced into the borehole and has set.

    Abstract translation: 本发明涉及一种用于固井地下钻孔，特别是油，气和/或陆地热钻孔的干式水泥配方，其包含a）约20至99.9wt。 ％水泥，b）约0至65wt。 ％粉状石英/或石英粉尘，c）约0.1至30重量％ ％的水分散性分散粉末，和d）约0〜20wt。 ％进一步添加剂。 此外，本发明涉及干水泥制剂用于制备水泥浆料的用途，以及在水泥浆中使用水可再分散分散粉末用于粘结地球钻孔，其中水泥浆料可用于还原水 水泥浆的损失，用于减少气体和/或水的渗透和/或通过已被引入井眼并已经固定的水泥浆来密封气体和/或水通道。

    Redispersible powder and its aqueous dispersion, preparation, process and use
    7.
    发明授权
    Redispersible powder and its aqueous dispersion, preparation, process and use 有权
    可再分散粉末及其水分散体，制备方法及用途

    公开(公告)号：US07674860B2

    公开(公告)日：2010-03-09

    申请号：US11955342

    申请日：2007-12-12

    Applicant: Hongli Willimann ,  Robert Koelliker

    Inventor： Hongli Willimann ,  Robert Koelliker

    IPC: C08F2/22 ,  C08F291/00

    CPC classification number: C08F2/22 ,  A23L27/74 ,  A23L33/25 ,  A61K47/32 ,  C04B24/26 ,  C04B2103/0004 ,  C04B2103/0005 ,  C04B2103/0057 ,  C04B2103/0058 ,  C08F265/04 ,  C08F265/06 ,  C08F291/00 ,  C08L33/14 ,  C08L57/12 ,  C09D151/00 ,  C04B2103/0051 ,  C04B2103/0052

    Abstract: The invention relates to a redispersible powder obtainable by (co)polymerization, using a polymer with cationic functionality in an aqueous medium, optionally accompanied by the use of conventional additives, the polymer with cationic functionality being obtained by (co)polymerization in an aqueous medium of olefinically unsaturated (co)monomers, wherein at least one (co)monomer has a cationic functionality, further (co)monomers are added and polymerization takes place in the presence of suitable initiators, and by drying the aqueous dispersion obtained, the (co)polymerizate having one or more reactive groups. According to another embodiment, the polymer with cationic functionality is formed in situ in the presence of a seed. According to another embodiment, the process is controlled in such a way that a (co)polymerizate particle with heterogeneous morphology is formed. The invention also relates to the aqueous dispersions, a process for the preparation of the redispersible powder and the use thereof.

    Abstract translation: 本发明涉及通过（共）聚合可获得的可再分散粉末，其使用在水性介质中具有阳离子官能度的聚合物，任选地伴随常规添加剂的使用，具有阳离子官能度的聚合物通过在水介质中（共）聚合而获得 的烯属不饱和（共）单体，其中至少一种（共）单体具有阳离子官能度，另外（共）单体被加入，并且在合适的引发剂存在下进行聚合，并且通过干燥获得的水分散体 ）具有一个或多个反应性基团的聚合物。 根据另一个实施方案，具有阳离子官能团的聚合物在种子存在下原位形成。 根据另一个实施方案，以这样的方式控制该方法：形成具有不均匀形态的（共）聚合物颗粒。 本发明还涉及水分散体，制备可再分散粉末的方法及其用途。

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