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    Reduced by product polyamine-epihalohydrin resins
    2.
    发明授权
    Reduced by product polyamine-epihalohydrin resins 有权
    由产品多胺 - 表卤代醇树脂减少

    公开(公告)号：US07175740B2

    公开(公告)日：2007-02-13

    申请号：US10396155

    申请日：2003-03-25

    申请人： Richard James Riehle ,  Anthony J. Allen ,  Michaela Hofbauer ,  Alfred Jacques Haandrikman ,  Ronald Busink ,  Mark T. Crisp ,  John James Hoglen ,  Huai Nan Cheng ,  Francis J. Carlin, Jr. ,  John Arthur Lapre ,  Harold Jabloner

    发明人： Richard James Riehle ,  Anthony J. Allen ,  Michaela Hofbauer ,  Alfred Jacques Haandrikman ,  Ronald Busink ,  Mark T. Crisp ,  John James Hoglen ,  Huai Nan Cheng ,  Francis J. Carlin, Jr. ,  John Arthur Lapre ,  Harold Jabloner

    IPC分类号： D21H17/55 ,  D21H21/20 ,  C08G69/46

    CPC分类号： D21H17/55 ,  C08G73/022 ,  C08G73/0286 ,  D21H17/56 ,  D21H27/08 ,  D21H27/10

    摘要： Processes for rendering a polyamine-epihalohydrin resin storage stable, including processes that prepare a storage stable resin and/or processes that treat resins. A composition containing a polyamine-epihalohydrin resin which includes CPD-forming species can be treated with at least one agent under conditions to at least one of inhibit, reduce and remove the CPD-forming species to obtain a reduced CPD-forming resin so that a composition containing the reduced CPD-forming polyamine-epihalohydrin resin when stored for 2 weeks at 50° C., and a pH of about 2.5 to 3.5 contains less than about 250 ppm dry basis of CPD. The invention is also directed to a gelation storage stable reduced CPD-forming resin so that a composition containing the reduced CPD-forming polyamine-epihalohydrin resin, when stored at pH 1 for 24 hours at 50° C. and measured at 24 hours, produces less than about 1000 ppm dry basis of CPD. A paper product containing the storage stable polyaminopolyamide-epihalohydrin resin, when corrected for adding at about a 1 wt % addition level of the polyaminopolyamide-epihalohydrin resin, contains less than about 250 ppb of CPD. Moreover, a resin can be prepared starting from a prepolymer having a low acid number or low concentration of acid end groups. The invention is also directed to papers containing the resins.

    摘要翻译： 使多胺 - 表卤代醇树脂保存稳定的方法，包括制备储存稳定树脂的方法和/或处理树脂的方法。 包含CPD形成物质的含有多胺 - 表卤醇树脂的组合物可以在至少一种抑制，减少和除去CPD形成物质的条件下用至少一种试剂处理，以获得减少的CPD形成树脂，使得 含有减少的形成CPD的多胺 - 表卤代醇树脂的组合物在50℃下储存2周时，pH约2.5-3.5含有低于约250ppm干基的CPD。 本发明还涉及一种凝胶储存稳定的减少CPD形成树脂，使得含有减少的形成CPD的多胺 - 表卤代醇树脂的组合物在50℃下储存24小时并在24小时时测量时产生 小于约1000ppm的干燥基础的CPD。 含有储存稳定的聚氨基多酰胺 - 表卤代醇树脂的纸产品在校正后加入多氨基聚酰胺 - 表卤代醇树脂的约1重量％时含有小于约250ppb的CPD。 此外，可以从具有低酸值或低浓度酸端基的预聚物开始制备树脂。 本发明还涉及含有树脂的纸张。

    Reduced byproduct polyamine-epihalohydrin resins
    5.
    发明申请
    Reduced byproduct polyamine-epihalohydrin resins 审中-公开
    副产物多胺 - 表卤代醇树脂

    公开(公告)号：US20070137821A1

    公开(公告)日：2007-06-21

    申请号：US11645968

    申请日：2006-12-27

    申请人： Richard Riehle ,  Anthony Allen ,  Michaela Hofbauer ,  Alfred Haandrikman ,  Ronald Busink ,  Mark Crisp ,  John Hoglen ,  Huai Cheng ,  Francis Carlin ,  John Lapre ,  Harold Jabloner

    发明人： Richard Riehle ,  Anthony Allen ,  Michaela Hofbauer ,  Alfred Haandrikman ,  Ronald Busink ,  Mark Crisp ,  John Hoglen ,  Huai Cheng ,  Francis Carlin ,  John Lapre ,  Harold Jabloner

    IPC分类号： D21H19/30 ,  C08G69/48

    CPC分类号： D21H17/55 ,  C08G73/022 ,  C08G73/0286 ,  D21H17/56 ,  D21H27/08 ,  D21H27/10

    摘要： Processes for rendering a polyamine-epihalohydrin resin storage stable, including processes that prepare a storage stable resin and/or processes that treat resins. A composition containing a polyamine-epihalohydrin resin which includes CPD-forming species can be treated with at least one agent under conditions to at least one of inhibit, reduce and remove the CPD-forming species to obtain a reduced CPD-forming resin so that a composition containing the reduced CPD-forming polyamine-epihalohydrin resin when stored for 2 weeks at 50° C., and a pH of about 2.5 to 3.5 contains less than about 250 ppm dry basis of CPD. The invention is also directed to a gelation storage stable reduced CPD-forming resin so that a composition containing the reduced CPD-forming polyamine-epihalohydrin resin, when stored at pH 1 for 24 hours at 50° C. and measured at 24 hours, produces less than about 1000 ppm dry basis of CPD. A paper product containing the storage stable polyaminopolyamide-epihalohydrin resin, when corrected for adding at about a 1 wt % addition level of the polyaminopolyamide-epihalohydrin resin, contains less than about 250 ppb of CPD. Moreover, a resin can be prepared starting from a prepolymer having a low acid number or low concentration of acid end groups. The invention is also directed to papers containing the resins.

    摘要翻译： 使多胺 - 表卤代醇树脂保存稳定的方法，包括制备储存稳定树脂的方法和/或处理树脂的方法。 包含CPD形成物质的含有多胺 - 表卤醇树脂的组合物可以在至少一种抑制，减少和除去CPD形成物质的条件下用至少一种试剂处理，以获得减少的CPD形成树脂，使得 含有减少的形成CPD的多胺 - 表卤代醇树脂的组合物在50℃下储存2周时，pH约2.5-3.5含有低于约250ppm干基的CPD。 本发明还涉及一种凝胶储存稳定的减少CPD形成树脂，使得含有减少的形成CPD的多胺 - 表卤代醇树脂的组合物在50℃下储存24小时并在24小时时测量时产生 小于约1000ppm的干燥基础的CPD。 含有储存稳定的聚氨基多酰胺 - 表卤代醇树脂的纸产品在校正后加入多氨基聚酰胺 - 表卤代醇树脂的约1重量％时含有小于约250ppb的CPD。 此外，可以从具有低酸值或低浓度酸端基的预聚物开始制备树脂。 本发明还涉及含有树脂的纸张。

    Reduced byproduct polyamine-epihalohydrin resins
    6.
    发明授权
    Reduced byproduct polyamine-epihalohydrin resins 有权
    副产物多胺 - 表卤代醇树脂

    公开(公告)号：US06554961B1

    公开(公告)日：2003-04-29

    申请号：US09592681

    申请日：2000-06-12

    申请人： Richard James Riehle ,  Anthony J. Allen ,  Michaela Hofbauer ,  Alfred Jacques Haandrikman ,  Ronald Busink ,  Mark T. Crisp ,  John James Hoglen ,  Huai Nan Cheng ,  Francis J. Carlin, Jr. ,  John Arthur Lapre ,  Harold Jabloner

    发明人： Richard James Riehle ,  Anthony J. Allen ,  Michaela Hofbauer ,  Alfred Jacques Haandrikman ,  Ronald Busink ,  Mark T. Crisp ,  John James Hoglen ,  Huai Nan Cheng ,  Francis J. Carlin, Jr. ,  John Arthur Lapre ,  Harold Jabloner

    IPC分类号： D21H1755

    CPC分类号： D21H17/55 ,  C08G73/022 ,  C08G73/0286 ,  D21H17/56 ,  D21H27/08 ,  D21H27/10

    摘要： Processes for rendering a polyamine-epihalohydrin resin storage stable, including processes that prepare a storage stable resin and/or processes that treat resins. A composition containing a polyamine-epihalohydrin resin which includes CPD-forming species can be treated with at least one agent under conditions to at least one of inhibit, reduce and remove the CPD-forming species to obtain a reduced CPD-forming resin so that a composition containing the reduced CPD-forming polyamine-epihalohydrin resin when stored for 2 weeks at 50° C., and a pH of about 2.5 to 3.5 contains less than about 250 ppm dry basis of CPD. The invention is also directed to a gelation storage stable reduced CPD-forming resin so that a composition containing the reduced CPD-forming polyamine-epihalohydrin resin, when stored at pH 1 for 24 hours at 50° C. and measured at 24 hours, produces less than about 1000 ppm dry basis of CPD. A paper product containing the storage stable polyaminopolyamide-epihalohydrin resin, when corrected for adding at about a 1 wt % addition level of the polyaminopolyamide-epihalohydrin resin, contains less than about 250 ppb of CPD. Moreover, a resin can be prepared starting from a prepolymer having a low acid number or low concentration of acid end groups. The invention is also directed to papers containing the resins.

    摘要翻译： 使多胺 - 表卤代醇树脂保存稳定的方法，包括制备储存稳定树脂的方法和/或处理树脂的方法。 包含CPD形成物质的含有多胺 - 表卤醇树脂的组合物可以在至少一种抑制，减少和除去CPD形成物质的条件下用至少一种试剂处理，以获得减少的CPD形成树脂，使得 含有减少的形成CPD的多胺 - 表卤代醇树脂的组合物在50℃下储存2周时，pH约2.5-3.5含有低于约250ppm干基的CPD。 本发明还涉及一种凝胶储存稳定的减少CPD形成树脂，使得含有减少的形成CPD的多胺 - 表卤代醇树脂的组合物在50℃下储存24小时并在24小时时测量时产生 小于约1000ppm的干燥基础的CPD。 含有储存稳定的聚氨基多酰胺 - 表卤代醇树脂的纸产品在校正后加入多氨基聚酰胺 - 表卤代醇树脂的约1重量％时含有小于约250ppb的CPD。 此外，可以从具有低酸值或低浓度酸端基的预聚物开始制备树脂。 本发明还涉及含有树脂的纸张。

    Thermosettable resin compositions
    7.
    发明授权
    Thermosettable resin compositions 失效
    热固性树脂组合物

    公开(公告)号：US5095074A

    公开(公告)日：1992-03-10

    申请号：US503023

    申请日：1990-04-02

    申请人： Sung G. Chu ,  Harold Jabloner ,  Tuyen T. Nguyen

    发明人： Sung G. Chu ,  Harold Jabloner ,  Tuyen T. Nguyen

    IPC分类号： C08G73/12 ,  C08J5/24

    CPC分类号： C08J5/24 ,  C08G73/12 ,  C08J2379/08

    摘要： A novel polyfunctional maleimide-based thermosettable resin composition comprising: (a) at least one polyfunctional maleimide compound selected from the group consisting of bismaleimide and polymaleimide, and (b) at least one ether derivative of an alkenylphenol.

    摘要翻译： 一种新型多官能马来酰亚胺类可热固树脂组合物，其包含：（a）至少一种选自双马来酰亚胺和聚马来酰亚胺的多官能马来酰亚胺化合物，和（b）至少一种烯基苯酚的醚衍生物。

    Thermosetting epoxy resin compositions and thermosets therefrom
    8.
    发明授权
    Thermosetting epoxy resin compositions and thermosets therefrom 失效
    热固性环氧树脂组合物和热固性材料

    公开(公告)号：US4822832A

    公开(公告)日：1989-04-18

    申请号：US35525

    申请日：1987-04-07

    申请人： Sung G. Chu ,  Harold Jabloner ,  Brian J. Swetlin

    发明人： Sung G. Chu ,  Harold Jabloner ,  Brian J. Swetlin

    IPC分类号： C08G59/50 ,  C08G59/56 ,  C08J5/24 ,  C08L63/00 ,  H05K1/03 ,  C08K3/04

    CPC分类号： C08J5/24 ,  C08G59/50 ,  C08G59/5033 ,  C08G59/56 ,  C08L63/00 ,  C08J2363/00 ,  H05K1/0326 ,  Y10S428/901 ,  Y10S525/906 ,  Y10T428/24917

    摘要： Described are novel thermosetting epoxy resin compositions suitable for making cured resins, prepregs and stiff, tough thermoset composites. The thermosetting compositions comprise a polyepoxide component, an amine hardner and a specified amount of certain aromatic oligomers containing functional groups which are reactive with the polyepoxide and/or hardener under curing conditions for the composition. The cured resins have a multiphase morphology which comprises at least one glassy continuous phase and at least one glassy discontinuous phase and have a fracture toughness, K.sub.IC, of at least 1.0 MPam.sup.1/2.

    摘要翻译： 描述了适用于制备固化树脂，预浸料和刚性坚韧的热固性复合材料的新型热固性环氧树脂组合物。 热固性组合物包含聚环氧化物组分，胺硬化剂和指定量的含有官能团的某些芳族低聚物，所述官能团在组合物的固化条件下与聚环氧化物和/或硬化剂反应。 固化树脂具有多相形态，其包括至少一个玻璃状连续相和至少一个玻璃态不连续相，并具有至少1.0MPam1 / 2的断裂韧性KIC。

    Polyarylene polyether made using mixed base system
    9.
    发明授权
    Polyarylene polyether made using mixed base system 失效
    聚亚芳基聚醚用混合基体制成

    公开(公告)号：US4789722A

    公开(公告)日：1988-12-06

    申请号：US80144

    申请日：1987-07-29

    申请人： Harold Jabloner ,  Tuyen T. Nguyen

    发明人： Harold Jabloner ,  Tuyen T. Nguyen

    IPC分类号： C08G65/40 ,  C08G65/48 ,  C08G75/23

    CPC分类号： C08G65/48 ,  C08G65/4093

    摘要： Polyarylene polyethers, made by a process comprising reacting a dihydroxy compound and strong and weak bases in a liquid reaction medium at 100.degree.-200.degree. C. to form a double salt and then reacting the double salt with a slight molar excess of dihalobenzenoid compound bearing two replaceable halogens, are disclosed. The process reliably produces halogen-terminated polyarylene polyethers of select degrees of polymerization and desirable correspondence between weight and number average molecular weights. In subsequent steps amine-terminated polyarylene polyethers are made using the strong and weak bases. The resulting amine-terminated polyethers have a low, select degree of polymerization, desirable correspondence between weight and number average molecular weights and high level of amine termination.

    摘要翻译： 聚亚芳基聚醚，其通过包括在液体反应介质中在100℃-200℃下使二羟基化合物与强碱和弱碱反应以形成双重盐，然后使双重盐与少量摩尔过量的二卤代苯基化合物 两种可更换的卤素被公开。 该方法可靠地生产具有选择聚合度的卤素封端的聚亚芳基聚醚，并且其重量和数均分子量之间是期望的对应关系。 在随后的步骤中，使用强碱和弱碱制备胺封端的聚亚芳基聚醚。 所得的胺封端的聚醚具有低的选择聚合度，重量和数均分子量之间的期望对应性以及高水平的胺终止。

    Preparation of stable aqueous dispersions of polyolefin fibers
    10.
    发明授权
    Preparation of stable aqueous dispersions of polyolefin fibers 失效
    稳定的聚烯烃纤维水分散体的制备

    公开(公告)号：US4404314A

    公开(公告)日：1983-09-13

    申请号：US338931

    申请日：1982-01-12

    申请人： Harold Jabloner

    发明人： Harold Jabloner

    IPC分类号： D06M15/267 ,  B01F17/52 ,  C04B20/10 ,  C08J3/03 ,  C08L23/02 ,  C08L33/26 ,  D01F11/06 ,  D06M15/285 ,  D06M101/00 ,  D06M101/16 ,  D06M101/18 ,  D21H13/14 ,  D21H17/37

    CPC分类号： C04B20/1033 ,  D21H13/14 ,  D21H5/202

    摘要： Stable aqueous dispersions of polyolefin fibers are formed by contacting the fibers with an aqueous solution of a cationic copolymer of an acrylamide and an acrylate or methacrylate ester, the pH of the aqueous solution having been adjusted to be in the range of from about 9.5 to about 12 either prior to, during or after contacting the fibers with said solution. An exemplary copolymer is that formed by the copolymerization of acrylamide and .beta.-methacryloyloxyethyltrimethylammonium methyl sulfate.

    摘要翻译： 通过使纤维与丙烯酰胺和丙烯酸酯或甲基丙烯酸酯的阳离子共聚物的水溶液接触而形成聚烯烃纤维的稳定的水性分散体，将该水溶液的pH调节至约9.5至约 12在纤维与所述溶液接触之前，期间或之后。 示例性共聚物是通过丙烯酰胺和β-甲基丙烯酰氧基乙基三甲基甲基硫酸铵的共聚形成的共聚物。