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    METHOD FOR MAKING A POLYSACCHARIDE DIALDEHYDE HAVING HIGH PURITY
    1.
    发明申请
    METHOD FOR MAKING A POLYSACCHARIDE DIALDEHYDE HAVING HIGH PURITY 审中-公开
    制备具有高纯度的多糖二盐酸盐的方法

    公开(公告)号：US20130274225A1

    公开(公告)日：2013-10-17

    申请号：US13811474

    申请日：2011-07-19

    申请人： Douglas J. Adelman

    发明人： Douglas J. Adelman

    IPC分类号： C08B37/02

    CPC分类号： C08B37/0021 ,  A61K9/70 ,  A61L15/58 ,  C08B11/20 ,  C08B15/02 ,  C08B31/18 ,  C08B37/00 ,  C08B37/0057 ,  C08B37/0069 ,  C08B37/0072

    摘要： A method for making polysaccharide dialdehydes is disclosed, which uses a combination of precipitation and separation steps to purify the polysaccharide dialdehyde formed by oxidation of a polysaccharide with periodate. The method is simple, rapid, and provides a polysaccharide dialdehyde having very low levels of iodine-containing species and a low ash content. The polysaccharide dialdehyde is particularly suitable for preparing hydrogel adhesives for medical applications.

    摘要翻译： 公开了一种制备多糖二醛的方法，其使用沉淀和分离步骤的组合来纯化由多糖与高碘酸盐氧化形成的多糖二醛。 该方法简单，快速，提供了含有非常低含量碘含量和低灰分含量的多糖二醛。 多糖二醛特别适用于制备用于医疗应用的水凝胶粘合剂。

    PRINTING FORM AND PROCESS FOR PREPARING THE PRINTING FORM WITH CURABLE COMPOSITION HAVING EPOXY NOVOLAC RESIN
    2.
    发明申请
    PRINTING FORM AND PROCESS FOR PREPARING THE PRINTING FORM WITH CURABLE COMPOSITION HAVING EPOXY NOVOLAC RESIN 审中-公开
    印刷形式和制备具有环氧氯酚树脂的可固化组合物的印刷方法

    公开(公告)号：US20120285930A1

    公开(公告)日：2012-11-15

    申请号：US13469337

    申请日：2012-05-11

    申请人： Douglas J. Adelman ,  Cara L. Blankenbicker ,  Andrew P. Davis ,  Barbara B. Fones ,  Helen S. M. Lu ,  Mark E. Wagman

    发明人： Douglas J. Adelman ,  Cara L. Blankenbicker ,  Andrew P. Davis ,  Barbara B. Fones ,  Helen S. M. Lu ,  Mark E. Wagman

    IPC分类号： B29C59/16 ,  B05C21/00 ,  B05D5/00

    CPC分类号： B41N1/22 ,  B41C1/045 ,  B41C1/05 ,  B41N1/06 ,  B41N1/12 ,  C08G59/08 ,  C08G59/5006 ,  C08L63/04

    摘要： The invention pertains to a printing form and a process for preparing the printing form from a curable composition that includes an epoxy novolac resin having an epoxide equivalent weight of 156 to 300 g/equivalent, and an amine curing agent selected from primary amines and secondary amines, the agent having an amine equivalent weight of less than or equal to 60 g/equivalent. The process includes applying the curable composition to a supporting substrate to form a layer, curing the layer at one or more temperatures in a temperature range, and engraving to form at least one cell in the cured layer. The process prepares printing forms, particularly gravure printing forms, having a cured resin composition layer that is engravable, resistant to solvent inks and to mechanical wear, and capable of printing gravure-quality images.

    摘要翻译： 本发明涉及一种印刷形式和从包含环氧当量为156-300g /当量的环氧酚醛清漆树脂和选自伯胺和仲胺的胺固化剂的可固化组合物制备印刷形式的方法 该胺的当量重量小于或等于60g /当量。 该方法包括将可固化组合物施加到支撑基底以形成层，在一个或多个温度范围内固化该层，并雕刻以在固化层中形成至少一个电池。 该方法制备具有可雕刻，耐溶剂油墨和机械磨损的固化树脂组合物层并且能够印刷凹版印刷图像的印刷形式，特别是凹版印刷形式。

    PRINTING FORM AND PROCESS FOR PREPARING THE PRINTING FORM WITH CURABLE COMPOSITION HAVING BISPHENOL-BASED EPOXY RESIN
    5.
    发明申请
    PRINTING FORM AND PROCESS FOR PREPARING THE PRINTING FORM WITH CURABLE COMPOSITION HAVING BISPHENOL-BASED EPOXY RESIN 审中-公开
    用具有双酚基环氧树脂的可固化组合物制备印刷形式的印刷形式和方法

    公开(公告)号：US20120285342A1

    公开(公告)日：2012-11-15

    申请号：US13469257

    申请日：2012-05-11

    申请人： DOUGLAS J. ADELMAN ,  Garret D. Figuly ,  Helen Shin Min Lu ,  Usha Sharma

    发明人： DOUGLAS J. ADELMAN ,  Garret D. Figuly ,  Helen Shin Min Lu ,  Usha Sharma

    IPC分类号： B41N1/16 ,  B41M3/00 ,  B29C59/16 ,  B23P15/00 ,  B05D3/02 ,  B05D3/12

    CPC分类号： B41N1/12 ,  B41C1/045 ,  B41C1/05 ,  B41N1/22 ,  C08G59/223 ,  C08G59/502 ,  C08L63/00 ,  Y10T29/49401

    摘要： The invention pertains to a process for preparing a printing form from a curable composition that includes an bisphenol-based epoxy resin; an amine curing agent selected from primary amines and secondary amines, the agent having an amine equivalent weight of less than or equal to 200 g/equivalent; and, a multi-epoxy reactive diluent. The process includes applying the curable composition to a supporting substrate to form a layer, curing the layer at one or more temperatures in a temperature range, and engraving to form at least one cell in the cured layer. The process prepares printing forms, particularly gravure printing forms, having a cured resin composition layer that is engravable, resistant to solvent inks and to mechanical wear, and capable of printing gravure-quality images.

    摘要翻译： 本发明涉及一种由包含双酚基环氧树脂的可固化组合物制备印刷形式的方法; 选自伯胺和仲胺的胺固化剂，胺当量重量小于或等于200g /当量; 和多环氧反应性稀释剂。 该方法包括将可固化组合物施加到支撑基底以形成层，在一个或多个温度范围内固化该层，并雕刻以在固化层中形成至少一个电池。 该方法制备具有可雕刻，耐溶剂油墨和机械磨损的固化树脂组合物层并且能够印刷凹版印刷图像的印刷形式，特别是凹版印刷形式。

    PROCESS FOR PREPARING ALKANE LIQUIDS FOR USE IN IMMERSION LITHOGRAPHY
    6.
    发明申请
    PROCESS FOR PREPARING ALKANE LIQUIDS FOR USE IN IMMERSION LITHOGRAPHY 审中-公开
    用于制备浸出液中使用的碱性液体的方法

    公开(公告)号：US20090299113A1

    公开(公告)日：2009-12-03

    申请号：US12128020

    申请日：2008-05-28

    申请人： Douglas J. Adelman ,  Hoang Vi Tran

    发明人： Douglas J. Adelman ,  Hoang Vi Tran

    IPC分类号： C07C5/02

    CPC分类号： C07C7/163 ,  C07C9/00

    摘要： A method for purifying liquid alkanes, especially dicyclic alkanes, for use in immersion lithography is provided. The method produces alkanes having absorbance at 193 nm of ≦0.1/cm, and residue of ≦100 ppm. The liquid alkane compositions are useful as immersion liquids in photomicrolithography employed for production of electronic circuits.

    摘要翻译： 提供了用于浸没式光刻中使用的用于净化液态烷烃，特别是二环烷烃的方法。 该方法产生在193nm处具有<= 0.1 / cm的吸光度和<= 100ppm的残留物的烷烃。 液体烷烃组合物可用作用于生产电子电路的微光刻中的浸液。

    Process for preparing amide acetals
    7.
    发明授权
    Process for preparing amide acetals 失效
    制备酰胺缩醛的方法

    公开(公告)号：US07439354B2

    公开(公告)日：2008-10-21

    申请号：US11002747

    申请日：2004-12-02

    申请人： Christian Peter Lenges ,  Josef Huybrechts ,  Douglas J. Adelman

    发明人： Christian Peter Lenges ,  Josef Huybrechts ,  Douglas J. Adelman

    IPC分类号： C07D491/04

    CPC分类号： C08G18/792 ,  C07D498/04 ,  C08G18/3827 ,  C08G18/6229 ,  C09D175/04

    摘要： A process for preparing amide acetals represented in Formula I comprising dehydrating a reactant mixture comprising reactants selected from a group consisting of N-acyl dialkanol amines, O-acyl dialkanol amines and mixtures thereof wherein n and m are independently 2 or 3; p is 1, 2 or 3; R1 and R2 can be the same or different and are each independently hydrogen, a linear or branched alkyl, cycloalkyl or aryl group with 1-20 C atoms; R represents hydrogen, a branched or linear alkyl, cycloalkyl, aryl or an alkenyl group with 1-20 C-atoms, each may have one or more substituents.

    摘要翻译： 一种制备式I表示的酰胺缩醛的方法，包括使包含选自N-酰基二链烷醇胺，O-酰基二链烷醇胺及其混合物的反应物的反应物混合物脱水，其中n和m独立地为2或3; p为1,2或3; R 1和R 2可以相同或不同，各自独立地为氢，具有1-20个C原子的直链或支链烷基，环烷基或芳基; R表示氢，具有1-20个C原子的支链或直链烷基，环烷基，芳基或烯基，各自可具有一个或多个取代基。

    Nitro substituted alpha -olefin synthesis catalysts
    8.
    发明申请
    Nitro substituted alpha -olefin synthesis catalysts 审中-公开
    硝基取代的α-烯烃合成催化剂

    公开(公告)号：US20080194768A1

    公开(公告)日：2008-08-14

    申请号：US11502863

    申请日：2006-08-11

    申请人： Douglas J. Adelman ,  Alex Seregy Ionkin

    发明人： Douglas J. Adelman ,  Alex Seregy Ionkin

    IPC分类号： C08F126/06 ,  C07F15/02

    CPC分类号： C07F15/025 ,  C07C2/32 ,  C07D213/53

    摘要： Iron, cobalt, chromium or vanadium complexes of 2,6-pyridinedicarboxaldehydes diimines and 2,6-diacylpyridines diimines which are suitable for catalyzing the oligomerization of ethylene to α-olefins exhibit more prolonged catalytic activity if aryl groups attached to the imino carbon atom(s) are substituted with at least one nitro group.

    摘要翻译： 适用于催化乙烯低聚至α-烯烃的2,6-吡啶二甲醛二亚胺和2,6-二酰基吡啶二亚胺的铁，钴，铬或钒络合物如果连接在亚氨基碳原子上的芳基 s）被至少一个硝基取代。

    Poly(1,3-propylene-co-1,4:3,6-dianhydro-D-sorbitol terephthalate) and manufacturing process
    9.
    发明授权
    Poly(1,3-propylene-co-1,4:3,6-dianhydro-D-sorbitol terephthalate) and manufacturing process 有权

    公开(公告)号：US07049390B2

    公开(公告)日：2006-05-23

    申请号：US10172112

    申请日：2002-06-14

    申请人： Douglas J. Adelman ,  Robin N. Greene ,  Donald E. Putzig

    发明人： Douglas J. Adelman ,  Robin N. Greene ,  Donald E. Putzig

    IPC分类号： C08G63/68 ,  C08G63/78

    CPC分类号： C08G63/672 ,  C08G63/80 ,  C08G63/82

    摘要： A melt polymerization process for the preparation of poly(1,3-propylene-co-isosorbide) terephthalate (3GIT), new 3GITs and products made from the 3GITs. The process comprises (a) providing a mixture comprising terephthalic acid or its alkyl ester, 1,3-propanediol and isosorbide in a molar ratio of diols to terephthalic acid or its alkyl ester of from about 1.1:1 to about 1.6:1 and a molar ratio of 1,3-propanediol to isosorbide of from about 2:1 to about 10:1; (b) reacting the mixture in an inert atmosphere at a temperature of about 180 to about 245° C., with concurrent removal of a distillate comprising at least 80% of the water or alkanol volatile reaction product, wherein the distillate contains less than about 5 weight % 1,3-propanediol and less than 1 weight % isosorbide; and (c) continuing the reaction in the presence of a polycondensation catalyst at a pressure of about 0.25 to about 2 mm Hg and about 245 to about 260° C. to form a 3GIT containing about 4 to about 20 mole % isosorbide units, based on the 3GIT.

    Manufacture of 1,3-propanediol esters from formaldehyde and ethylene using a modified prins reaction
    10.
    发明授权
    Manufacture of 1,3-propanediol esters from formaldehyde and ethylene using a modified prins reaction 有权
    使用改性的苯酚反应从甲醛和乙烯制备1,3-丙二醇酯

    公开(公告)号：US06111135A

    公开(公告)日：2000-08-29

    申请号：US203985

    申请日：1998-12-02

    申请人： Douglas J. Adelman ,  Neville Everton Drysdale

    发明人： Douglas J. Adelman ,  Neville Everton Drysdale

    IPC分类号： B01J31/12 ,  C07B61/00 ,  C07C67/00 ,  C07C69/08 ,  C07C69/76 ,  C08G63/82

    CPC分类号： C07C67/00

    摘要： Disclosed is a process for manufacturing an ester of 1,3-propanediol, comprising, contacting at a temperature of about 0.degree. C. to about 250.degree. C., ethylene, formaldehyde or a form of formaldehyde, a carboxylic acid, and a compound of the formula MZ.sub.n.Q.sub.t, wherein:M is a zirconium[IV], cobalt[II], vanadium[IV], bismuth[II], tin[II], a rare earth metal, scandium or yttrium;n is the oxidation state of M;at least one of Z is an anion of the formula R.sup.1 SO.sub.3.sup.- or R.sup.1 CO.sub.2.sup.-, wherein R.sup.1 is hydrocarbyl or substituted hydrocarbyl containing 1 to 20 carbon atoms or part of a polymer, and the remainder of Z is oxo or one or more monovalent anions;Q is a neutral ligand; andt is 0 or an integer of 1 to 12.

    摘要翻译： 公开了一种制备1,3-丙二醇酯的方法，包括在约0℃至约250℃的温度下接触乙烯，甲醛或甲醛，羧酸和化合物的形式 其中：M是锆[IV]，钴[II]，钒[IV]，铋[II]，锡[II]，稀土金属，钪或钇; n是M的氧化态; Z中的至少一个是式R 1 SO 3 - 或R 1 CO 2 - 的阴离子，其中R 1是含有1至20个碳原子或部分聚合物的烃基或取代的烃基，并且其余的Z是氧代或一个或多个一价阴离子; Q是中性配体; t为0或1〜12的整数。