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    Chemical microreactor and method thereof
    1.
    发明申请
    Chemical microreactor and method thereof 失效
    化学微反应器及其方法

    公开(公告)号：US20060057039A1

    公开(公告)日：2006-03-16

    申请号：US11196634

    申请日：2005-08-02

    申请人： Jeffrey Morse ,  Alan Jankowski

    发明人： Jeffrey Morse ,  Alan Jankowski

    IPC分类号： B01J19/24 ,  B81B1/00

    CPC分类号： B01J19/0093 ,  B01J2219/00783 ,  B01J2219/00824 ,  B01J2219/00828 ,  B01J2219/00831 ,  B01J2219/00835 ,  B01J2219/00844 ,  B01J2219/00871 ,  B01J2219/00873

    摘要： Disclosed is a chemical microreactor that provides a means to generate hydrogen fuel from liquid sources such as ammonia, methanol, and butane through steam reforming processes when mixed with an appropriate amount of water. The microreactor contains capillary microchannels with integrated resistive heaters to facilitate the occurrence of catalytic steam reforming reactions. Two distinct embodiment styles are discussed. One embodiment style employs a packed catalyst capillary microchannel and at least one porous membrane. Another embodiment style employs a porous membrane with a large surface area or a porous membrane support structure containing a plurality of porous membranes having a large surface area in the aggregate, i.e., greater than about 1 m2/cm3. Various methods to form packed catalyst capillary microchannels, porous membranes and porous membrane support structures are also disclosed.

    摘要翻译： 公开了一种化学微反应器，其提供了当与适量的水混合时通过蒸汽重整过程从液体源例如氨，甲醇和丁烷产生氢燃料的手段。 微反应器包含具有集成电阻加热器的毛细管微通道，以促进催化蒸汽重整反应的发生。 讨论了两种不同的实施方式。 一种实施方案采用填充催化剂毛细管微通道和至少一种多孔膜。 另一实施例采用具有大表面积的多孔膜或多孔膜支撑结构，其包含多个聚集体中具有大表面积的多孔膜，即大于约1m 2 / cm 3 。 还公开了形成填充催化剂毛细管微通道，多孔膜和多孔膜支撑结构的各种方法。

    Vapor-deposited porous films for energy conversion
    2.
    发明申请
    Vapor-deposited porous films for energy conversion 失效
    用于能量转换的蒸镀多孔膜

    公开(公告)号：US20050016832A1

    公开(公告)日：2005-01-27

    申请号：US10612177

    申请日：2003-07-01

    申请人： Alan Jankowski ,  Jeffrey Hayes ,  Jeffrey Morse

    发明人： Alan Jankowski ,  Jeffrey Hayes ,  Jeffrey Morse

    IPC分类号： C23C14/16 ,  H01M4/66 ,  H01M4/80 ,  C23C14/00 ,  C23C14/32 ,  H05H1/24

    CPC分类号： C23C14/165 ,  H01M4/661 ,  H01M4/808

    摘要： Metallic films are grown with a “spongelike” morphology in the as-deposited condition using planar magnetron sputtering. The morphology of the deposit is characterized by metallic continuity in three dimensions with continuous and open porosity on the submicron scale. The stabilization of the spongelike morphology is found over a limited range of the sputter deposition parameters, that is, of working gas pressure and substrate temperature. This spongelike morphology is an extension of the features as generally represented in the classic zone models of growth for physical vapor deposits. Nickel coatings were deposited with working gas pressures up 4 Pa and for substrate temperatures up to 1000 K. The morphology of the deposits is examined in plan and in cross section views with scanning electron microscopy (SEM). The parametric range of gas pressure and substrate temperature (relative to absolute melt point) under which the spongelike metal deposits are produced appear universal for other metals including gold, silver, and aluminum.

    摘要翻译： 使用平面磁控溅射在沉积条件下以“海绵状”形态生长金属膜。 沉积物的形态特征在于三维金属连续性，亚微米尺度具有连续且开放的孔隙度。 在溅射沉积参数的有限范围，即工作气体压力和衬底温度的范围内发现海绵状形态的稳定性。 这种海绵状形态是通常在物理气相沉积生长的经典区域模型中表示的特征的延伸。 镍涂层沉积工作气体压力高达4 Pa，衬底温度高达1000 K。沉积物的形态在扫描电子显微镜（SEM）中以平面图和截面图进行检查。 产生海绵状金属沉积物的气体压力和基底温度（相对于绝对熔点）的参数范围对于其他金属（包括金，银和铝）似乎是通用的。

    CHEMICAL MICROREACTOR AND METHOD THEREOF
    3.
    发明申请
    CHEMICAL MICROREACTOR AND METHOD THEREOF 有权
    化学微粒及其方法

    公开(公告)号：US20090223925A1

    公开(公告)日：2009-09-10

    申请号：US12412599

    申请日：2009-03-27

    申请人： Jeffrey D. Morse ,  Alan Jankowski

    发明人： Jeffrey D. Morse ,  Alan Jankowski

    IPC分类号： B44C1/22

    CPC分类号： B01J19/0093 ,  B01J2219/00783 ,  B01J2219/00824 ,  B01J2219/00828 ,  B01J2219/00831 ,  B01J2219/00835 ,  B01J2219/00844 ,  B01J2219/00871 ,  B01J2219/00873

    摘要： A method for forming a chemical microreactor includes forming at least one capillary microchannel in a substrate having at least one inlet and at least one outlet, integrating at least one heater into the chemical microreactor, interfacing the capillary microchannel with a liquid chemical reservoir at the inlet of the capillary microchannel, and interfacing the capillary microchannel with a porous membrane near the outlet of the capillary microchannel, the porous membrane being positioned beyond the outlet of the capillary microchannel, wherein the porous membrane has at least one catalyst material imbedded therein.

    摘要翻译： 用于形成化学微反应器的方法包括在具有至少一个入口和至少一个出口的基底中形成至少一个毛细管微通道，将至少一个加热器集成到化学微反应器中，将毛细管微通道与入口处的液体化学容器 的毛细管微通道，并且将毛细管微通道与毛细管微通道出口附近的多孔膜接合，多孔膜位于毛细管微通道出口之外，其中多孔膜具有嵌入其中的至少一种催化剂材料。

    Chemical microreactor and method thereof
    7.
    发明授权
    Chemical microreactor and method thereof 有权
    化学微反应器及其方法

    公开(公告)号：US07993534B2

    公开(公告)日：2011-08-09

    申请号：US12412599

    申请日：2009-03-27

    申请人： Jeffrey D. Morse ,  Alan Jankowski

    发明人： Jeffrey D. Morse ,  Alan Jankowski

    IPC分类号： C23F1/00

    CPC分类号： B01J19/0093 ,  B01J2219/00783 ,  B01J2219/00824 ,  B01J2219/00828 ,  B01J2219/00831 ,  B01J2219/00835 ,  B01J2219/00844 ,  B01J2219/00871 ,  B01J2219/00873

    摘要： A method for forming a chemical microreactor includes forming at least one capillary microchannel in a substrate having at least one inlet and at least one outlet, integrating at least one heater into the chemical microreactor, interfacing the capillary microchannel with a liquid chemical reservoir at the inlet of the capillary microchannel, and interfacing the capillary microchannel with a porous membrane near the outlet of the capillary microchannel, the porous membrane being positioned beyond the outlet of the capillary microchannel, wherein the porous membrane has at least one catalyst material imbedded therein.

    摘要翻译： 用于形成化学微反应器的方法包括在具有至少一个入口和至少一个出口的基底中形成至少一个毛细管微通道，将至少一个加热器集成到化学微反应器中，将毛细管微通道与入口处的液体化学容器 的毛细管微通道，并且将毛细管微通道与毛细管微通道出口附近的多孔膜接合，多孔膜位于毛细管微通道出口之外，其中多孔膜具有嵌入其中的至少一种催化剂材料。