摘要:
In one aspect, the present invention is directed to methods and apparatuses for recovering target metals from scrap. In some embodiments, the methods comprise dissolving a portion of a mixed metal scrap into a molten salt to form a molten salt and metal mixture, the scrap including a target metal species and at least one contaminant metal species; bubbling a gas through the molten salt and metal mixture to form a gas and metal vapor mixture comprising target metal vapors; and condensing at least a portion of the target metal vapors. In some embodiments, the apparatuses comprise a housing; a divider at least partially disposed within the housing, the divider forming at least a first chamber, a second chamber, and a fluid conduit between the first and second chambers; a top wall cooperating with a lower housing wall and at least one of the plurality of side walls to enclose the second chamber; a plurality of gas inlets disposed in the second chamber; and a gas outlet in fluid communication with the second chamber.
摘要:
In a method of producing a metal structure by photoreducing metal ion, a substance capable of suppressing growth of metal crystal is added to a medium in which metal ion is dispersed to prevent growth of the metal crystal produced by photoreduction of the metal ion, thereby processing resolution of a metal structure formed of the metal crystal is improved.
摘要:
An alteration of the traditional zinc/zinc-amalgam reduction procedure which eliminates both the hazardous mercury and dangerous hydrogen gas generation. In order to avoid the presence of water and hydrated protons in the working solution, which can oxidize Eu2+ and cause hydrogen gas production, a process utilizing methanol as the process solvent is described. While methanol presents some flammability hazard in a radiological hot cell, it can be better managed and is less of a flammability hazard than hydrogen gas generation.
摘要:
A method for producing an intermetallic compound, the method comprising: (1) providing components A, B and X; and forming by solid state reaction of components A, B and X an intermetallic compound having a filled skutterudite structure and formula of AaBbXc; (2) melting the intermetallic compound having a filled skutterudite structure produced in step (1) in the presence of additional X; and (3) annealing the intermetallic compound of step (2) in the presence of additional X at a temperature equal to, or greater than the phase formation temperature of the intermetallic compound.
摘要:
Metallic titanium is continuously produced in an electric-arc furnace under a vacuum by the metallothermic reduction of titanium tetrachloride by a reducing agent such as magnesium. The nanoparticles of titanium obtained from the reduction are simultaneously melted in a bath of molten titanium formed by the heat of an electric arc between a consumable titanium electrode and the molten titanium. A voltage applied across the electrode and the molten titanium is adjusted so that molten titanium is maintained in a cooled crystallizer during the entire process. The molten titanium solidifies on the top of a dummy bar that is drawn down as additional titanium is produced. Upon completion of each iterative reduction reaction, the vaporized reducing agent chloride is pumped out of the electric-arc furnace into a condenser using a vacuum pump. Then, additional reducing agent and titanium tetrachloride are added into the furnace, and the process is repeated.
摘要:
Implantable medical devices made from a single beta phase Tantalum alloy utilizing Titanium as an alloying agent that are biocompatible, radiopaque and visible under x-ray and fluoroscopy, the alloy having mechanical properties that allow it to be machined by conventional, machining methods for forming the devices, and a method for making the alloy. The alloy is between approximately 10 percent and 25 percent Ti by weight and preferably has a density of 12 g/cm3 or greater.
摘要:
The invention concerns a method for the continuous or discontinuous extraction of a metal or several metals from a slag that contains the metal or a compound of the metal, in which the liquefied metal-containing slag is heated in a primary or secondary smelting unit (1). To provide an improved method for extracting metals, especially copper, from slags, the invention provides that the metal-containing slag is heated in a primary or secondary smelting unit (1) designed as an alternating-current electric furnace, and the molten material is then fed from the primary or secondary smelting unit (1) into a furnace (2) designed as a direct-current electric furnace, in which the metal to be extracted is subjected to an electrolytic separation, where a reducing agent in the form of calcium silicide (CaSi), calcium carbide (CaC2), ferrosilicon (FeO), aluminum (Al), and/or reducing gases is added and/or injected into the primary or secondary smelting unit (1).
摘要:
A method of oxidizing carbonaceous ores to assist in the recovery of metals is provided. The method includes the steps of heating a bed of carbonaceous ore in the reaction chamber of a reactor vessel, using microwave energy to initiate and sustain oxidation of the carbonaceous ore within the bed into carbon dioxide, controlling the inflow of oxygen into the reaction chamber to provide sufficient oxygen to maintain the reaction C+O2═CO2, and monitoring the depletion of carbon from the carbonaceous ore.
摘要翻译:提供了一种氧化含碳矿石以辅助回收金属的方法。 该方法包括以下步骤:在反应容器的反应室中加热碳质矿床,使用微波能量引发和维持床内碳质矿石氧化成二氧化碳,控制进入反应室的氧气流入 提供足够的氧以保持反应C + O 2 -CO 2,并监测来自碳质矿石的碳的消耗。
摘要:
The process for the synthesis of rhenium powders comprises the injection of ammonium perrhenate powder through a carrier gas in a plasma torch of a plasma reactor operated using a mixture including hydrogen as the plasma gas, yielding metallic rhenium under the following chemical reaction: 2 NH4ReO4+4 H2→2 Re+N2↑+8 H2O↑. The reactor is provided with a quench zone for cooling the metallic rhenium so as to yield rhenium nano and micro powders.
摘要翻译:用于合成铼粉末的方法包括通过使用包括氢作为等离子体气体的混合物操作的等离子体反应器的等离子体炬中的载气注入高铼酸铵粉末,在下列化学反应中产生金属铼:<α -line-formula description =“In-line Formulas”end =“lead”?> 2 NH 4 ReO 4 + 4 H 2 - > 2 Re + N 2↑+ 8 H 2 O↑。 <?in-line-formula description =“在线公式”end =“tail”?>反应器设有用于冷却金属铼的淬火区域,以产生铼纳米和微粉末。
摘要:
A process for selectively reducing calcine from a copper/nickel containing sulfidic material includes subjecting the calcine to a mildly reducing atmosphere at relative high temperatures. CuO is selectively converted to Cu2O which can easily be separated by leaching from other metals which may be present in the material.
摘要翻译:从含铜/镍的硫化物质中选择性地还原煅烧的方法包括在相对高的温度下使煅烧物温和还原的气氛。 CuO被选择性地转化为Cu 2 O 2,其可以通过从可能存在于材料中的其它金属浸出而容易地分离。