Purification of diphenyl terephthalate
    43.
    发明授权
    Purification of diphenyl terephthalate 失效
    对苯二甲酸二苯酯的纯化

    公开(公告)号:US4020099A

    公开(公告)日:1977-04-26

    申请号:US544259

    申请日:1975-01-27

    CPC classification number: C07C69/82

    Abstract: Diphenyl phthalates are purified by crystallizing them from dipolar-aprotic solvents or solutions of solvents containing such solvents. The phthalate solutions are advantageously, but not necessarily, treated in a carbon column in hydrocarbon solvent without dipolar-aprotic solvents present to remove part of the color and impurities, and then dipolar-aprotic solvents are added to the solution before crystallization to aid in the final removal of color and impurities.

    Abstract translation: 邻苯二甲酸二苯酯通过将其从偶极非质子溶剂或含有这些溶剂的溶剂溶液中结晶来纯化。 邻苯二甲酸酯溶液有利但不一定在烃溶剂中的碳柱中处理,而不存在偶极非质子溶剂以除去部分颜色和杂质,然后在结晶之前将偶极非质子溶剂加入到溶液中以帮助 最终去除颜色和杂质。

    Diesters of tetrabromophthalic anhydride
    44.
    发明授权
    Diesters of tetrabromophthalic anhydride 失效
    四溴邻苯二甲酸酐的混合物

    公开(公告)号:US3989653A

    公开(公告)日:1976-11-02

    申请号:US580041

    申请日:1975-05-23

    CPC classification number: C08G18/5075 C08G18/4607 C08G18/5012 C08G18/6666

    Abstract: Diesters comprising the reaction product of tetrabromophthalic anhydride and a polyhydroxy compound containing at least 3 hydroxyl groups are disclosed. The diesters are prepared, in one step, by reacting tetrabromophthalic anhydride with the polyhydroxy compound at a temperature of from about 130.degree. C. to about 190.degree. C. in the presence of an alkaline material. The diesters are especially useful in the preparation of fire-retardant, self-extinguishing, polyurethane foams.

    Abstract translation: 公开了包含四溴邻苯二甲酸酐和含有至少3个羟基的多羟基化合物的反应产物的二酯。 在碱性物质的存在下,在约130℃至约190℃的温度下,通过使四溴邻苯二甲酸酐与多羟基化合物反应,一步制备二酯。 二酯在制备阻燃,自熄,聚氨酯泡沫体方面特别有用。

    Bromine-containing esters
    45.
    发明授权
    Bromine-containing esters 失效
    含溴的酯

    公开(公告)号:US3891695A

    公开(公告)日:1975-06-24

    申请号:US41816973

    申请日:1973-11-23

    CPC classification number: C08F22/20 G03G5/0546 G03G5/0589

    Abstract: Photoconductive coating compositions for application to solid substrates which are to be utilized in electrophotographic operations are described; the resultant photoconductive coatings comprise a layer of photoconductive pigment particles bonded to themselves and to the solid substrate with a binder comprising a novel interpolymer, at least one of whose constituent monomers contains bromine. Novel bromine-containing monomers are also disclosed.

    Abstract translation: 描述了用于在电照相操作中使用的用于固体基质的光导涂料组合物; 所得到的光导涂层包含一层光导性颜料颗粒,其与粘合剂本身和固体基质一起使用含有新型互聚物的粘合剂,其中至少一种构成单体含有溴。 还公开了新的含溴单体。

    Production of unsaturated esters
    46.
    发明授权
    Production of unsaturated esters 失效
    生产不饱和脂肪酸酯

    公开(公告)号:US3865868A

    公开(公告)日:1975-02-11

    申请号:US33604673

    申请日:1973-02-26

    Applicant: ICI LTD

    Inventor: LEWIS JACK

    CPC classification number: C07C67/055 C07C69/80 C07C69/145

    Abstract: Unsaturated esters are produced by reacting an acyclic conjugated diolefine such as butadiene with a carboxylic acid, particularly orthophthalic acid, in the presence of ethylene and a platinum or iridium compound. The esters produced are oligomers of butadiene, the ethylene giving enhanced catalyst stability and life.

    Abstract translation: 不饱和酯通过在乙烯和铂或铱化合物的存在下使无环共轭二烯烃如丁二烯与羧酸,特别是邻苯二甲酸反应来制备。 所生产的酯是丁二烯的低聚物,乙烯具有增强的催化剂稳定性和寿命。

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