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公开(公告)号：US20130274519A1
公开(公告)日：2013-10-17
申请号：US13828505
申请日：2013-03-14
Applicant: BASF SE
Inventor： Klaus Joachim MUELLER-ENGEL , Thomas Walter , Frank Huetten , Markus Ottenbacher , Ulrich Hammon
IPC: C07C51/42
CPC classification number: B01J19/32 , B01D3/16 , B01D3/225 , B01F3/0446 , B01J2219/322 , B01J2219/3327 , C07C51/42 , C07C67/48 , C07C57/04 , C07C69/54
Abstract: A thermal separation process between a gas ascending in a separating column and a liquid descending in the separating column, which comprise (meth)acrylic monomers, wherein the separating column comprises a sequence of crossflow mass transfer trays, the crossflow mass transfer trays of which have passage orifices for the ascending gas in crossflow direction both in front of and beyond a downcomer for the descending liquid, and such crossflow mass transfer trays and one such crossflow mass transfer tray in a sequence of crossflow mass transfer trays present in a separating column.
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12.发明授权公开(公告)号：US11447439B2
公开(公告)日：2022-09-20
申请号：US17263415
申请日：2019-07-16
Applicant: BASF SE
Inventor： Nicole Janssen , Peter Zurowski , Ulrich Hammon , Sylke Haremza
Abstract: Process for inhibiting the undesired free-radical polymerization of acrylic acid present in a liquid phase P, wherein the acrylic acid content of P is at least 10% by weight, the liquid phase P comprises in the range from 25 to 1000 ppmw of glyoxal based on the weight of the acrylic acid present in P and the liquid phase P is admixed with furfural in an amount that results in a furfural content in the range from 25 to 1000 ppmw based on the weight of the acrylic acid present in P. Liquid phase P, wherein the acrylic acid content of P is at least 10% by weight and the liquid phase P comprises in the range from 25 to 1000 ppmw of glyoxal and in the range from 25 to 1000 ppmw of furfural in each case based on the weight of the acrylic acid present in P.
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公开(公告)号：US10682631B2
公开(公告)日：2020-06-16
申请号：US16250244
申请日：2019-01-17
Applicant: BASF SE
Inventor： Kazuhiko Amakawa , Christian Walsdorff , Klaus Joachim Mueller-Engel , Cornelia Katharina Dobner , Ulrich Hammon
IPC: B01J23/00 , B01J35/00 , B01J37/00 , C07C45/35 , B01J23/887 , C07C51/215 , B01J35/10 , B01J23/888 , B01J37/08 , B01J37/02 , C01G39/00 , B01J35/02 , B01J37/04 , C01B33/32
Abstract: Multimetal oxide composition comprising Mo, Bi, Fe, Cu and one or more than one of the elements Co and Ni and use thereof.
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14.发明授权公开(公告)号：US10173147B2
公开(公告)日：2019-01-08
申请号：US14738033
申请日：2015-06-12
Applicant: BASF SE
Inventor： Joerg Heilek , Rainer Askani , Ulrich Hammon , Wolfgang Schneider , Thomas Walter
Abstract: The present invention relates to an apparatus (1) for separation of a target product from a liquid phase P comprising the target product, comprising at least one primary space (3) for a heat transfer medium W, at least one first feed unit (5a) and one first removal unit (5b) for the heat transfer medium W, at least one secondary space (7) for the liquid phase P, at least one second feed unit (9) for the liquid phase P, at least one crystallization surface (13) which divides the primary space (3) and the secondary space (7), at least one second removal unit (15) for the target product and at least one application unit (11) for a liquid phase P0 essentially directly to the crystallization surface (13) or the surfaces of lines that conduct the heat transfer medium W. The present invention further relates to a process for removing a target product from a liquid phase P comprising the target product.
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公开(公告)号：US09797657B2
公开(公告)日：2017-10-24
申请号：US14661408
申请日：2015-03-18
Applicant: BASF SE
Inventor： Ulrich Hammon , Thomas Walter , Armin Schraut
CPC classification number: F28D7/16 , B01J8/067 , B01J2208/00221 , B01J2208/00256 , F28D2021/0022 , F28D2021/0064 , F28F27/00 , F28F2265/12
Abstract: A heat exchanger (1) contains: a bundle of at least two heat exchanger tubes (3), a heat exchanger housing (5) surrounding the bundle of heat exchanger tubes (3), wherein a liquid heat-transfer medium (7) is passed around the bundle of heat exchanger tubes (3) in the heat exchanger housing (5), a heat exchanger cap (9) sealing the top of the heat exchanger housing (5), a heat exchanger bottom (11) sealing the bottom of the heat exchanger housing (5), a feed point (13) for the heat-transfer medium (7), an outlet (15) for the heat-transfer medium (7), an emergency relief port (17) disposed in proximity to the heat exchanger cap (9). The heat exchanger (1) contains a safety device (19) disposed in proximity to the heat exchanger bottom (11).
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Patent Agency Ranking
公开(公告)号：US09636651B2
公开(公告)日：2017-05-02
申请号：US14737025
申请日：2015-06-11
Applicant: BASF SE
Inventor： Ulrich Hammon , Thomas Walter
IPC: C07C45/00 , C07C45/27 , C07C45/28 , C07C45/32 , C07C45/33 , C07C45/34 , C07C45/35 , C07C47/00 , C07C47/20 , C07C47/21 , C07C47/22 , C07C51/00 , C07C51/16 , C07C51/21 , C07C51/25 , B01J8/02 , B01J8/06 , B01J8/00
CPC classification number: B01J8/0278 , B01J8/065 , B01J8/067 , B01J2208/00017 , B01J2208/00176 , B01J2208/0053 , B01J2208/00893 , C07C45/28 , C07C45/35 , C07C51/16 , C07C51/252 , Y02P20/582 , C07C57/04 , C07C47/22
Abstract: The present invention relates to a plant for performance of heterogeneously catalyzed gas phase reactions. The plant entails a reactor, at least one line leading into the reactor for introduction of reactants into the reactor, at least one first feed for providing at least one first reactant A, which leads into the line, at least one second feed for providing at least one second reactant B, which leads into the line, at least one third feed for providing a cycle gas G, which leads into the line, a temperature control unit which is disposed in the line upstream of the reactor and is for controlling the temperature of the first reactant A and/or second reactant B and/or cycle gas G prior to entry into the reactor and at least one outlet for products, by-products and/or unreacted reactants from the gas phase reaction.
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公开(公告)号：US09018416B2
公开(公告)日：2015-04-28
申请号：US13828505
申请日：2013-03-14
Applicant: BASF SE
Inventor： Klaus Joachim Mueller-Engel , Thomas Walter , Frank Huetten , Markus Ottenbacher , Ulrich Hammon
CPC classification number: B01J19/32 , B01D3/16 , B01D3/225 , B01F3/0446 , B01J2219/322 , B01J2219/3327 , C07C51/42 , C07C67/48 , C07C57/04 , C07C69/54
Abstract: A thermal separation process between a gas ascending in a separating column and a liquid descending in the separating column, which comprise (meth)acrylic monomers, wherein the separating column comprises a sequence of crossflow mass transfer trays, the crossflow mass transfer trays of which have passage orifices for the ascending gas in crossflow direction both in front of and beyond a downcomer for the descending liquid, and such crossflow mass transfer trays and one such crossflow mass transfer tray in a sequence of crossflow mass transfer trays present in a separating column.
Abstract translation: 在分离塔中上升的气体和分离塔中下降的液体之间的热分离过程，其包含（甲基）丙烯酸单体，其中分离塔包括一系列交叉流传质托盘，其交叉流传质托盘具有 用于下降液体的降液管之前和之后的横流方向的上升气体的通道孔，以及存在于分离塔中的交叉流传质托盘中的这种交叉流传质托盘和一个这样的交叉流传质托盘。
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18.发明申请CATALYST FOR PREPARATION OF AN UNSATURATED CARBOXYLIC ACID BY GAS PHASE OXIDATION OF AN UNSATURATED ALDEHYDE 有权用于通过气相氧化不饱和二醛制备不饱和羧酸的催化剂公开(公告)号：US20150080605A1
公开(公告)日：2015-03-19
申请号：US14487383
申请日：2014-09-16
Applicant: BASF SE
Inventor： Cathrin Alexandra WELKER-NIEUWOUDT , Cornelia Katharina Dobner , Holger Borchert , Ulrich Hammon , Josef Macht , Andrey Karpov , Christian Walsdorff
IPC: B01J23/888 , B01J37/04 , C07C51/25 , B01J35/04
CPC classification number: B01J23/8885 , B01J23/002 , B01J23/8877 , B01J23/94 , B01J35/0006 , B01J35/002 , B01J35/008 , B01J35/023 , B01J35/04 , B01J35/1004 , B01J35/1033 , B01J35/1038 , B01J35/1066 , B01J35/1071 , B01J35/1076 , B01J35/108 , B01J37/0009 , B01J37/0018 , B01J37/0036 , B01J37/0045 , B01J37/0223 , B01J37/0232 , B01J37/04 , B01J37/08 , B01J2523/00 , C07C51/235 , C07C51/25 , C07C51/252 , Y02P20/584 , Y10T428/13 , Y10T428/249953 , Y10T428/273 , B01J2523/17 , B01J2523/55 , B01J2523/68 , B01J2523/69 , C07C57/04
Abstract: What is described is a catalyst for preparation of an α,β-unsaturated carboxylic acid by gas phase oxidation of an α,β-unsaturated aldehyde, comprising a shaped support body with an active composition applied thereto, wherein the active composition coverage q q = Q ( 100 - Q ) S m is at most 0.3 mg/mm2, where Q is the active composition content of the catalyst in % by weight and Sm is the specific geometric surface area of the shaped support body in mm2/mg. Also described are a process for preparing the catalyst and a process for preparing an α,β-unsaturated carboxylic acid by gas phase oxidation of an α,β-unsaturated aldehyde over a fixed catalyst bed comprising a bed of the catalyst. The catalyst, with constantly high conversion of acrolein, reduces overoxidation to COx and increases the selectivity of acrylic acid formation.
Abstract translation: 所描述的是通过α，bgr-不饱和醛的气相氧化制备α，β-不饱和羧酸的催化剂，其包括施加有活性组合物的成型载体，其中活性组合物覆盖率qq = Q（100-Q）S m为至多0.3mg / mm 2，其中Q为催化剂的活性组成含量，重量％，Sm为成形载体的特定几何表面积，单位为mm2 / mg。 还描述了制备催化剂的方法和通过在包含催化剂床的固定催化剂床上气相氧化α，β-不饱和醛来制备α，β-不饱和羧酸的方法。 具有不断高的丙烯醛转化率的催化剂减少了对COx的过氧化，并增加了丙烯酸形成的选择性。
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公开(公告)号：US09958201B2
公开(公告)日：2018-05-01
申请号：US14817351
申请日：2015-08-04
Applicant: BASF SE
Inventor： Ulrich Hammon , Thomas Walter
IPC: F25J3/02 , C07C67/54 , C07C45/82 , B01D3/20 , B01D3/42 , C07C45/78 , C07C45/80 , C07C51/44 , C07C51/48 , B01D3/22 , B01D3/32
CPC classification number: F25J3/0271 , B01D3/20 , B01D3/22 , B01D3/32 , B01D3/4261 , C07C45/783 , C07C45/80 , C07C45/82 , C07C51/44 , C07C51/48 , C07C67/54 , C07C47/22 , C07C57/04 , C07C69/54
Abstract: The present disclosure includes a column (1) having a cylindrical, vertical column body (2) forming a column cavity (3), and a mass transfer tray (4) disposed in the column cavity (3) and forming a collecting area (5). The column (1) is characterized by a circulation device (9) having at least one drain orifice (10) formed in the column body (2) above the collecting area (5), a circulation line (11) in fluid connection with the drain orifice (10) and at least one recycling orifice (14; 14-1 to 14-3) which is in fluid connection with the circulation line (11) and is formed in the column body (2) above the collecting area (5). Also disclosed herein is a thermal separating process in which a gas ascends within a column (1) of the present disclosure, and a liquid descends within the column (1), said gas and/or liquid containing (meth)acrylic monomers.
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公开(公告)号：US20150158011A1
公开(公告)日：2015-06-11
申请号：US14562481
申请日：2014-12-05
Applicant: BASF SE
Inventor： Klaus Joachim Mueller-Engel , Thomas Walter , Frank Huetten , Markus Ottenbacher , Ulrich Hammon
CPC classification number: B01J19/32 , B01D3/16 , B01D3/225 , B01F3/0446 , B01J2219/322 , B01J2219/3327 , C07C51/42 , C07C67/48 , C07C57/04 , C07C69/54
Abstract: A thermal separation process between a gas ascending in a separating column and a liquid descending in the separating column, which comprise (meth)acrylic monomers, wherein the separating column comprises a sequence of crossflow mass transfer trays, the crossflow mass transfer trays of which have passage orifices for the ascending gas in crossflow direction both in front of and beyond a downcomer for the descending liquid, and such crossflow mass transfer trays and one such crossflow mass transfer tray in a sequence of crossflow mass transfer trays present in a separating column.
Abstract translation: 在分离塔中上升的气体和分离塔中下降的液体之间的热分离过程，其包含（甲基）丙烯酸单体，其中分离塔包括一系列交叉流传质托盘，其交叉流传质托盘具有 用于下降液体的降液管之前和之后的横流方向的上升气体的通道孔，以及存在于分离塔中的交叉流传质托盘中的这种交叉流传质托盘和一个这样的交叉流传质托盘。
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