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    DIRECT ONE-STEP SYNTHESIS OF CF3-I
    91.
    发明申请
    DIRECT ONE-STEP SYNTHESIS OF CF3-I 失效
    直接一步合成CF3-I

    公开(公告)号：US20060129006A1

    公开(公告)日：2006-06-15

    申请号：US11007919

    申请日：2004-12-09

    Applicant: Sudip Mukhopadhyay ,  Hsueh Tung

    Inventor： Sudip Mukhopadhyay ,  Hsueh Tung

    IPC: C07C19/07

    CPC classification number: C07C17/093 ,  C07C17/158 ,  C07C17/204 ,  C07C19/16

    Abstract: The present invention provides a process for the preparation of trifluoromethyl iodide. The process includes the step of: contacting in a reactor a compound represented by the formula: CF3—W and a compound represented by the formula: Z-I wherein W is selected from CF3, hydrogen and bromine; Z is selected from hydrogen, iodine and chlorine. The step of contacting is carried out, optionally in the presence of a catalyst and further optionally in the presence of air, at a temperature, pressure and for a length of time sufficient to produce the trifluoromethyl iodide.

    Abstract translation: 本发明提供了制备三氟甲基碘的方法。 该方法包括以下步骤：在反应器中接触由下式表示的化合物：<？in-line-formula description =“In-line Formulas”end =“lead”？> CF 3 - W <？in-line-formula description =“In-line Formulas”end =“tail”？>和由以下公式表示的化合物：<？in-line-formula description =“In-line Formulas”end =“lead “？”ZI <？in-line-formula description =“In-line Formulas”end =“tail”？>其中W选自CF 3，氢和溴; Z选自氢，碘和氯。 任选地在催化剂存在下进一步任选地在空气存在下，在足以产生三氟甲基碘的温度，压力和一段时间内进行接触步骤。

    Processes for synthesis of 1,3,3,3-tetrafluoropropene
    92.
    发明申请
    Processes for synthesis of 1,3,3,3-tetrafluoropropene 有权
    合成1,3,3,3-四氟丙烯的方法

    公开(公告)号：US20060030744A1

    公开(公告)日：2006-02-09

    申请号：US11118530

    申请日：2005-04-29

    Applicant: Sudip Mukhopadhyay ,  Haridasan Nair ,  HsuehSung Tung ,  Michael Van Der Puy

    Inventor： Sudip Mukhopadhyay ,  Haridasan Nair ,  HsuehSung Tung ,  Michael Van Der Puy

    IPC: C07C17/087

    CPC classification number: C07C17/06 ,  C07C17/04 ,  C07C17/206 ,  C07C17/21 ,  C07C17/25 ,  C07C21/18 ,  C07C19/14 ,  C07C19/16 ,  C07C19/01 ,  C07C19/10

    Abstract: Disclosed in one embodiment is a process for the synthesis of 1,3,3,3-tetrafluoropropene that comprises (a) reacting a compound of formula (I) X1X2 with a compound of formula (II) CF3CH═CH2 to produce a reaction product comprising a compound of formula (III) CF3CHX1CH2X2, wherein X1 and X2 are each independently selected from the group consisting of hydrogen, chlorine, bromine and iodine, provided that X1 and X2 are not both hydrogen; (b) when X2 in formula (III) is not fluorine, fluorinating the compound of formula (III) to produce a reaction product comprising a compound of formula (III) wherein X1 is as described above and X2 is fluorine; and (c) exposing said compound of formula (III) to reaction conditions effective to convert said compound to 1,3,3,3-tetrafluoropropene. In another embodiment, the process comprises (a) reacting chlorine with a compound of formula (I) CH3CH═CH2 to produce a reaction product comprising a compound of formula (II) CCl3CHC1CH2C1; (b) fluorinating the compound of formula (II) to produce a reaction product comprising a compound of formula (III) CF3CHC1CH2F; and (c) exposing said compound of said formula (III) to reaction conditions effective to convert said compound to 1,3,3,3-tetrafluoropropene.

    Abstract translation: 在一个实施方案中公开了一种用于合成1,3,3,3-四氟丙烯的方法，其包括（a）使式（I）化合物X 1，X 2， 与式（II）化合物CF 3 CH-CH 2取代，生成包含式（III）化合物的反应产物CF 3 其中X 1和X 2都是（CH 2）2 CH 2，其中X 1和X 2都是 各自独立地选自氢，氯，溴和碘，条件是X 1和X 2都不是氢; （b）当式（III）中的X 2不是氟时，氟化式（III）化合物以产生包含式（III）化合物的反应产物，其中X 1， / SUP>如上所述，X 2是氟; 和（c）将所述式（III）化合物暴露于有效将所述化合物转化为1,3,3,3-四氟丙烯的反应条件。 在另一个实施方案中，该方法包括（a）使氯与式（I）CH 3 CH-CH 2 2的化合物反应以产生包含式 （II）CCl 3 CHClCH 2 C 1; （b）氟化式（II）化合物以产生包含式（III）化合物的反应产物：CF 3 CHClCH 2 F; 和（c）将所述式（III）的所述化合物暴露于有效将所述化合物转化为1,3,3,3-四氟丙烯的反应条件。

    Flurofunctional statistical polymers with low glass transition temperature and method for obtaining the same
    94.
    发明申请
    Flurofunctional statistical polymers with low glass transition temperature and method for obtaining the same 审中-公开
    具有低玻璃化转变温度的功能性统计聚合物及其获得方法

    公开(公告)号：US20040254319A1

    公开(公告)日：2004-12-16

    申请号：US10480819

    申请日：2004-06-15

    Inventor： Bruno Michel Ameduri ,  Mario Boucher ,  Bernard Leon Boutevin

    IPC: C08F012/20

    CPC classification number: C07C309/81 ,  C07C17/02 ,  C07C17/278 ,  C07C19/16

    Abstract: The invention concerns fluorofunctional statistical polymers of formula (V1), wherein: X, Y and Z represent a hydrogen atom and exhibiting in particular low glass transition temperatures obtained in particular from a B monomer of formula (I): F2CnullCFnullRFnullSO2F, wherein: RF represents one or several vinylidene fluoride units and/or a hexafluoropropene unit and/or a chlorotrifluoroerthylene unit. The crosslinkable fluorosulphonated elastomers thus obtained are advantageously usable for making membranes, polymeric electrolytes, ionomers, membranes for fuel cells in particular hydrogen or methanol fuel cells, for obtaining gaskets and O-rings, rubber hose, pipes, pump bodies, diaphragms, piston heads (used in aeronautics, oil, automotive, mining and nuclear industries) and for plastics processes (as processing aids).

    Abstract translation: 本发明涉及式（V1）的氟官能统计聚合物，其中：X，Y和Z表示氢原子，特别表现出从式（I）的B单体获得的特别低的玻璃化转变温度：F2C = CF-RF- SO 2 F，其中：RF表示一个或多个偏二氟乙烯单元和/或六氟丙烯单元和/或三氟甲苯单元。 如此获得的可交联氟磺化弹性体有利地用于制造膜，聚合物电解质，离聚物，用于燃料电池，特别是氢或甲醇燃料电池的膜，用于获得垫圈和O形环，橡胶软管，管道，泵体，隔膜，活塞头 （用于航空，石油，汽车，矿业和核工业）和塑料加工（作为加工助剂）。

    Process for the manufacture of halocarbons and selected compounds and azeotropes with HF
    95.
    发明授权
    Process for the manufacture of halocarbons and selected compounds and azeotropes with HF 失效
    用于制造卤代烃和所选化合物以及与HF共沸的方法

    公开(公告)号：US06291730B1

    公开(公告)日：2001-09-18

    申请号：US09011401

    申请日：1998-01-28

    Applicant: Ralph Thomas Baker ,  Viacheslav Alexandrovich Petrov ,  Velliyur Nott Mallikarjuna Rao ,  Allen Capron Sievert

    Inventor： Ralph Thomas Baker ,  Viacheslav Alexandrovich Petrov ,  Velliyur Nott Mallikarjuna Rao ,  Allen Capron Sievert

    IPC: C07C1710

    CPC classification number: C07C19/10 ,  C07C17/206 ,  C07C17/275 ,  C07C17/278 ,  C07C17/38 ,  C07C17/386 ,  C07C19/08 ,  Y02P20/582 ,  C07C19/01 ,  C07C19/16

    Abstract: A liquid phase process is disclosed for producing halogenated alkane adducts of the formula: CAR1R2CBR3R4 (where A, B, R1, R2, R3, and R4 are as defined in the specification) which involves contacting a corresponding halogenated alkane, AB, with a corresponding olefin, CR1R2═C3R4 in a dinitrile or cyclic carbonate ester solvent which divides the reaction mixture into two liquid phases and in the presence of a catalyst system containing: (i) at least one catalyst selected from monovalent and divalent copper; and optionally (ii) a promoter selected from aromatic or aliphatic heterocyclic compounds which contain at least one carbon-nitrogen double bond in the heterocyclic ring. When hydrochlorofluorocarbons are formed, the chlorine content may be reduced by reacting the hydrochlorofluorocarbons with HF. New compounds disclosed include CF3CF2CCl2CH2CCl3, CF3CCl2CH2CH2Cl and CF3CCl2CH2CHClF. These compounds are useful as intermediates for producing hydrofluorocarbons. Azeotropes of CClF2CH2CF3 with HF and azeotropes of CF3CH2CHF2 with HF are also disclosed; as are processes for producing such azeotropes. A process for purification of certain hydrofluorocarbons and/or chloroprecursors thereof from mixtures of such compounds with HF is also disclosed.

    Abstract translation: 公开了制备下式的卤化烷烃加成物的液相方法：CAR1R2CBR3R4（其中A，B，R1，R2，R3和R4如说明书中所定义），其涉及使相应的卤代烷烃AB与相应的 烯烃，CR1R2 = C3R4在二腈或环状碳酸酯溶剂中，其将反应混合物分成两个液相，并且在催化剂体系存在下，包含：（i）至少一种选自单价和二价铜的催化剂; 和任选地（ii）选自在杂环中含有至少一个碳 - 氮双键的芳族或脂族杂环化合物的促进剂。 当形成氢氯氟烃时，可以通过氢氯氟烃与HF反应来降低氯含量。 所公开的新化合物包括CF 3 CF 2 CCl 2 CH 2 ClCl 3，CF 3 CCl 2 CH 2 CH 2 Cl和CF 3 CCl 2 CH 2 CHClF。 这些化合物可用作生产氢氟烃的中间体。 还公开了CClF 2 CH 2 CF 3与HF的共沸物和CF 3 CH 2 CHF 2与HF的共沸物质; 生产这种共沸物的方法也是如此。 还公开了从这些化合物与HF的混合物中纯化某些氢氟烃和/或其氯前体的方法。

    Partially fluorinated polymers
    97.
    发明授权
    Partially fluorinated polymers 有权
    部分氟化聚合物

    公开(公告)号：US06255543B1

    公开(公告)日：2001-07-03

    申请号：US09730434

    申请日：2000-12-05

    Applicant: Zhen-Yu Yang

    Inventor： Zhen-Yu Yang

    IPC: C07C2118

    CPC classification number: C08F14/185 ,  C07C17/278 ,  C07C17/361 ,  C07C67/293 ,  C07C19/16 ,  C07C21/18 ,  C07C69/63

    Abstract: Selected novel partially fluorinated &agr;,&ohgr;-dienes can be free radically (co)polymerized to form polymers in which cyclic structures are present. The polymers are useful for films, coatings and molded parts.

    Abstract translation: 选择的新型部分氟化的α，ω-二烯可以自由基（共）聚合形成其中存在环状结构的聚合物。 聚合物可用于薄膜，涂料和模制件。

    Partially fluorinated polymers
    98.
    发明授权
    Partially fluorinated polymers 有权
    部分氟化聚合物

    公开(公告)号：US06214955B1

    公开(公告)日：2001-04-10

    申请号：US09194282

    申请日：1998-11-23

    Applicant: Zhen-Yu Yang

    Inventor： Zhen-Yu Yang

    IPC: C08F1418

    CPC classification number: C08F14/185 ,  C07C17/278 ,  C07C17/361 ,  C07C67/293 ,  C07C19/16 ,  C07C21/18 ,  C07C69/63

    Abstract: Selected partially fluorinated &agr;,&ohgr;-dienes bearing CF3 substitution can be free radically (co)polymerized to form polymers in which cyclic structures are present. The polymers are useful for films, coating and molded parts.

    Abstract translation: 含有CF 3取代的选择性部分氟化的α，ω-二烯可以自由基（共）聚合形成其中存在环状结构的聚合物。 聚合物可用于薄膜，涂料和模制件。

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