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    Pigment composition
    1.
    发明授权
    Pigment composition 失效
    颜料组成

    公开(公告)号：US5380363A

    公开(公告)日：1995-01-10

    申请号：US133129

    申请日：1993-11-15

    Applicant: Gerard Coispeau ,  John D. Schofield

    Inventor： Gerard Coispeau ,  John D. Schofield

    IPC: C09B63/00 ,  C09B67/20 ,  C09B67/46 ,  C09D11/10 ,  C09B45/01 ,  C09B41/00

    CPC classification number: C09B63/005 ,  C09B67/0085

    Abstract: A process for the manufacture of an azo metal salt pigment, wherein a transparent or translucent alkaline aqueous solution of a resin and a dispersant of formula (1) or formula (3) is added to an azo compound, said formula (1) beingYCO--OM (1)whereinYCO is the residue of a polyester derived from a hydroxycarboxylic acid, andM is H, a metal or optionally substituted ammonium, and said formula (3) beingYCO--Z--R (3)whereinZ is a divalent bridging group containing an oxygen or a nitrogen atom through which Z is attached to the carbonyl groupR is a primary, secondary or tertiary amino group or a salt thereof with an acid, or a quaternary ammonium salt group, andYCO is as herein defined.

    Abstract translation: PCT No.PCT / GB93 / 00317 Sec。 371日期：1993年11月9日 102（e）日期1993年11月9日PCT提交1993年2月15日PCT公布。 公开号WO93 / 16137 日本8月19日，1993.一种制备偶氮金属盐颜料的方法，其中将一种树脂的透明或半透明碱性水溶液和式（1）或式（3）的分散剂加入到偶氮化合物中， 所述式（1）为YCO-OM（1），其中YCO为衍生自羟基羧酸的聚酯的残基，M为H，金属或任选取代的铵，所述式（3）为YCO-ZR ）其中Z是含有氧原子或氮原子的二价桥连基，Z连接到羰基上R是伯，仲或叔氨基或其与酸或季铵盐基团的盐，以及 YCO如本文所定义。

    Process for the preparation of metal complex dyes
    2.
    发明授权
    Process for the preparation of metal complex dyes 失效
    制备金属复合染料的方法

    公开(公告)号：US5209832A

    公开(公告)日：1993-05-11

    申请号：US805428

    申请日：1991-12-11

    Applicant: Wilhelm Schmidt ,  Gerhard Beck

    Inventor： Wilhelm Schmidt ,  Gerhard Beck

    IPC: C09B45/01 ,  C09B45/08 ,  C09B45/10 ,  C09B45/12 ,  C09B45/20 ,  C09B55/00

    CPC classification number: C09B45/01 ,  C09B45/20

    Abstract: The invention relates to a process for the preparation of a metal complex dye under production conditions, which comprises reacting at least one dye with a metal donor, adding said metal donor or said dye discontinuously before the end point of the metallizing is reached, and determining the end of the metallizing voltametrically.The process makes it possible to prepare metal complex dyes in good yield and purity.

    Abstract translation: 本发明涉及在生产条件下制备金属络合物染料的方法，该方法包括使至少一种染料与金属供体反应，在达到金属化终点之前不连续地加入所述金属供体或所述染料，并确定 金属化电压的结束。 该方法使得可以以良好的产率和纯度制备金属络合染料。

    Process for the preparation of concentrated 1:2 metal complex dye preparations
    3.
    发明授权
    Process for the preparation of concentrated 1:2 metal complex dye preparations 失效
    制备浓缩的1：2金属络合染料制剂的方法

    公开(公告)号：US5019132A

    公开(公告)日：1991-05-28

    申请号：US442101

    申请日：1989-11-28

    Applicant: Herb Davis ,  Charles R. Wetzel

    Inventor： Herb Davis ,  Charles R. Wetzel

    IPC: C09B55/00 ,  C09B45/01 ,  C09B67/22 ,  C09B67/24 ,  C09B67/26 ,  C09B67/44

    CPC classification number: C09B67/0073 ,  C09B45/01 ,  C09B67/0072

    Abstract: Stable, concentrated, liquid preparations of 1:2 metal complex azo or azomethine dyes containing at most one sulfonic acid group are obtained by metallizing the metal-free azo or azomethine intermediates in form of their moist, almost salt-free washed, filter cakes with aqueous slurries of complex forming, preferably cobalt or chromium salts. Without isolation of the thus obtained metal complex dyes the dye slurries are then in situ converted into the stable, concentrated dye preparations by adjusting them to a final dye concentration.The dye preparations are produced in a very economic manner by avoiding any isolation of the metal complex dyes after the metallization step and by considerably reducing the amounts of effluents.The dye preparations obtained are suitable for the preparation of dye-baths or printing pastes which may be used in particular for dyeing and printing textile materials made of natural or synthetic polyamide fibres, and further of leather and paper.

    Method of forming copper complexes of azo-dyestuffs using non-salt-forming copper (II) compounds
    4.
    发明授权
    Method of forming copper complexes of azo-dyestuffs using non-salt-forming copper (II) compounds 失效
    使用非成盐铜（II）化合物形成偶氮染料铜络合物的方法

    公开(公告)号：US4400317A

    公开(公告)日：1983-08-23

    申请号：US281635

    申请日：1981-07-09

    Applicant: Anthony J. Corso

    Inventor： Anthony J. Corso

    IPC: C09B45/01 ,  C09B45/08 ,  C09B45/18 ,  C09B45/28

    CPC classification number: C09B45/01

    Abstract: A method of directly producing copperized azo-dyestuffs of predetermined inorganic salt content is disclosed wherein an ortho, ortho'-dihydroxyazo-dyestuff is reacted with about one molar equivalent of a copper (II) compound consisting of from 1.0 to 0.1 molar equivalent of a non-salt-forming copper compound selected from CuCO.sub.3.Cu(OH).sub.2, 2CuCO.sub.3.Cu(OH).sub.2, Cu(OH).sub.2, CuO and mixtures thereof, and correspondingly from 0 to 0.9 molar equivalent of a salt-forming copper (II) compound selected from CuSO.sub.4, CuCl.sub.2 and Cu(NO.sub.3).sub.2. The disclosed method provides standard strength copperized dyestuff compositions at increased yields and without the need to precipitate the product from the reaction solution.

    Abstract translation: 公开了一种直接生产预定无机盐含量的铜化偶氮染料的方法，其中邻位邻位二羟基偶氮染料与约1摩尔当量的由（C 1 -C 6） 选自CuCO 3 Cu（OH）2，2CuCO 3，Cu（OH）2，Cu（OH）2，CuO及其混合物的非成盐铜化合物，相应地为0至0.9摩尔当量的成盐铜 （II）化合物，选自CuSO 4，CuCl 2和Cu（NO 3）2。 所公开的方法以增加的产率提供标准强度的铜化染料组合物，并且不需要将产物从反应溶液中沉淀出来。

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