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    Process for preparing tin tetrachloride
    5.
    发明授权
    Process for preparing tin tetrachloride 失效
    四氯化锡的制备方法

    公开(公告)号：US6001323A

    公开(公告)日：1999-12-14

    申请号：US139204

    申请日：1998-08-24

    Applicant: Siegfried Benninger

    Inventor： Siegfried Benninger

    IPC: B01J8/20 ,  C01G19/08 ,  C01B9/02

    CPC classification number: C01G19/08 ,  B01J8/20

    Abstract: The preparation of tin tetrachloride from tin granules and chlorine can be conducted safely even at high temperatures if the chlorine, before coming into contact with the tin, is brought into a highly disperse distribution in the circulating tin tetrachloride and develops a uniform flow profile.

    Abstract translation: 如果在与锡接触之前，氯在四氯化碳循环中形成高度分散的分布，并且形成均匀的流动分布，则即使在高温下也可以安全地进行锡颗粒和氯的四氯化锡的制备。

    Chlorination of ores containing alkali or alkaline earth values
    6.
    发明授权
    Chlorination of ores containing alkali or alkaline earth values 失效
    含有碱金属或碱土金属的矿石的氯化

    公开(公告)号：US4652434A

    公开(公告)日：1987-03-24

    申请号：US762213

    申请日：1985-08-05

    Applicant: James P. Bonsack ,  Michael Robinson

    Inventor： James P. Bonsack ,  Michael Robinson

    IPC: C01G1/06 ,  B01J8/12 ,  B01J19/00 ,  B08B17/02 ,  C01F11/28 ,  C01G19/08 ,  C01G23/02 ,  C01G23/07 ,  C22B1/08 ,  C22B1/10 ,  C22B1/26 ,  C22B21/00 ,  C22B25/02 ,  C22B26/00 ,  C22B34/12 ,  C01F5/30

    CPC classification number: B01J19/002 ,  B08B17/02 ,  C01F11/28 ,  C22B1/08 ,  C22B1/10 ,  C22B1/26 ,  C22B34/1222 ,  B01J2219/00252 ,  Y02P10/23

    Abstract: The invention pertains to an entrained-downflow chlorination process of fine metalliferous ores particularly containing alkali and/or alkaline earth metals greater than about 0.3% by weight as the oxide. The process includes a quenching step following the chlorination step where the chlorinated products are quenched by liquid cooling fluid spray patterns adapted to prevent solidification of the alkali and/or alkaline earth materials onto the reactor walls. The chlorinator unit of this invention prevents disruption of the chlorination process due to presence of liquids or sticky particles and it contains a quenching spray means disposed below the chlorination zone in the entrained-downflow chlorinator unit, whereby the quenching sprays prevent reactor wall buildup.

    Abstract translation: 本发明涉及特别含有大于约0.3重量％的碱金属和/或碱土金属作为氧化物的细金属矿石的夹带下流氯化方法。 该方法包括在氯化步骤之后的淬火步骤，其中氯化产物通过液体冷却流体喷雾图案淬火，其适于防止碱和/或碱土金属物质固化到反应器壁上。 本发明的氯化器单元防止由于存在液体或粘性颗粒而导致的氯化过程的破坏，并且其包含设置在夹带下流式氯化器单元中的氯化区下方的骤冷喷雾装置，由此骤冷喷雾防止反应器壁积聚。

    Process for the production of Ge by reduction of GeCl4 with liquid metal
    8.
    发明授权
    Process for the production of Ge by reduction of GeCl4 with liquid metal 有权
    通过用液态金属还原GeCl4来生产Ge的方法

    公开(公告)号：US07682593B2

    公开(公告)日：2010-03-23

    申请号：US11663795

    申请日：2005-09-16

    Applicant: Eric Robert ,  Tjakko Zijlema

    Inventor： Eric Robert ,  Tjakko Zijlema

    IPC: C01G19/08 ,  C22B25/00 ,  C22B41/00 ,  C01D3/14

    CPC classification number: C22B41/00 ,  C22B5/04 ,  Y02P10/212

    Abstract: The invention relates to the manufacture of high purity germanium for the manufacture of e.g. infra red optics, radiation detectors and electronic devices. GeCl4 is converted to Ge metal by contacting gaseous GeCl4 with a liquid metal M containing one of Zn, Na and Mg, thereby obtaining a Ge-bearing alloy and a metal M chloride, which is removed by evaporation or skimming. The Ge-bearing alloy is then purified at a temperature above the boiling point of metal M. This process does not require complicated technologies and preserves the high purity of the GeCl4 in the final Ge metal, as the only reactant is metal M, which can be obtained in very high purity grades and continuously recycled.

    Abstract translation: 本发明涉及用于制造例如高纯度锗的制造方法。 红外光学，辐射探测器和电子设备。 通过使气体GeCl4与含有Zn，Na和Mg中的一种的液态金属M接触，将GeCl 4转化为Ge金属，由此得到含Ge的合金和金属氯化物，通过蒸发或撇去除去。 然后在高于金属M沸点的温度下纯化含Ge合金。该方法不需要复杂的技术，并且保留了GeCl4在最终的Ge金属中的高纯度，因为唯一的反应物是金属M，它可以 可以获得非常高的纯度等级并持续回收。

    Production of anhydrous stannic chloride from aqueous solution
    10.
    发明授权
    Production of anhydrous stannic chloride from aqueous solution 失效
    从水溶液生产无水氯化钠

    公开(公告)号：US3642647A

    公开(公告)日：1972-02-15

    申请号：US3642647D

    申请日：1969-01-17

    Applicant: M & T PRODUCTS OF CANADA LTD

    Inventor： GOULDEN PETER DERRICK

    IPC: C01G19/08

    CPC classification number: C01G19/08

    Abstract: A PROCESS FOR THE DEHYDRATING OF AQUEOUS SOLUTIONS CONTAINING TETRAVALENT TIN AND CHLORIDE IONS BY TREATMENT THEREOF WITH SULFURIC ACID OR OLEUM TO FORM AN UPPER PHASE CONTAINING SULFURIC ACID AND A LOWER PHASE CONSISTING OF ANHYDROUS STANNIC CHLORIDE AND REMOVING AND RECOVERING THE LOWER PHASE AS AN ANHYDROUS STANNIC CHLORIDE PRODUCT.

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