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    METHOD FOR PREPARING POLY (ETHER KETONE KETONES)
    2.
    发明申请
    METHOD FOR PREPARING POLY (ETHER KETONE KETONES) 有权
    制备聚（酮基酮）的方法

    公开(公告)号：US20120263953A1

    公开(公告)日：2012-10-18

    申请号：US13383171

    申请日：2010-07-09

    Applicant: Ian Towle

    Inventor： Ian Towle

    IPC: C08G65/00

    CPC classification number: C08G61/127 ,  A61L27/18 ,  B33Y70/00 ,  C08G2261/3442 ,  C08G2261/45 ,  C08L65/00 ,  C08L71/12 ,  D01F6/665 ,  Y10T428/2982 ,  C08L71/00

    Abstract: A method of preparing a poly (ether ketone ketone) consisting essentially of the repeat unit: —Ar—O—Ar—C(═O)—Ar—C(═O)— wherein each Ar is independently an aromatic moiety is provided. The method may comprise the step of polymerising a monomer system in a reaction medium comprising: (a) a Lewis acid; and (b) a controlling agent comprising an aromatic carboxylic acid, an aromatic sulphonic acid, or a derivative thereof.

    Abstract translation: 制备基本上由重复单元组成的聚（醚酮酮）的方法：-Ar-O-Ar-C（= O）-Ar-C（= O）），其中每个Ar独立地为芳族部分。 该方法可以包括在反应介质中聚合单体体系的步骤，包括：（a）路易斯酸; 和（b）包含芳族羧酸，芳族磺酸或其衍生物的控制剂。

    Process for the production of fibers from poly(etheretherketone)-type polymers
    5.
    发明授权
    Process for the production of fibers from poly(etheretherketone)-type polymers 失效
    用于由聚（醚醚酮）型聚合物生产纤维的方法

    公开(公告)号：US4904426A

    公开(公告)日：1990-02-27

    申请号：US175716

    申请日：1988-03-31

    Applicant: Richard A. Lundgard ,  Henry N. Beck

    Inventor： Richard A. Lundgard ,  Henry N. Beck

    IPC: B01D67/00 ,  B01D69/08 ,  B01D71/52 ,  C08J3/09 ,  D01D5/247 ,  D01F6/66

    CPC classification number: D01F6/665 ,  B01D67/0009 ,  B01D67/003 ,  B01D69/08 ,  B01D71/52 ,  C08J3/091 ,  D01D5/247 ,  B01D2323/08 ,  B01D2323/12 ,  C08J2371/00

    Abstract: A process for preparing microporous poly(etheretherketone)-type fibers comprising forming an extrusion mixture of at least one unsulphonated poly(etheretherketone)-type polymer and a solvent comprising at least one organic compound consisting predominantly of carbon and hydrogen, wherein the organic compound has a molecular weight of between about 160 and 450, contains at least one six membered aromatic ring structure, possesses a boiling point of between about 240 and 480 degrees Celsius, and is capable of dissolving at least about 10 weight percent of the poly(etheretherketone)-type polymer present at the extrusion temperature, extruding to form solid or hollow fibers, conveying the fibers through at least one quench zone, conveying the fibers through at least one leach zone, and drying the fibers, wherein the fibers so formed possess interconnecting or non-interconnecting pores.

    Abstract translation: 一种制备微孔聚（醚醚酮）型纤维的方法，包括形成至少一种未磺化聚（醚醚酮）型聚合物和包含至少一种主要由碳和氢组成的有机化合物的溶剂的挤出混合物，其中有机化合物具有 约160至450之间的分子量含有至少一个六元芳族环结构，其沸点介于约240至480摄氏度之间，并且能够溶解至少约10重量％的聚（醚醚酮） 以挤出温度存在，挤出以形成固体或中空纤维，将纤维输送通过至少一个骤冷区，将纤维输送通过至少一个浸出区，并干燥纤维，其中如此形成的纤维具有互连或 非互连孔。

    Process of making an aromatic polyetherketone fiber product
    6.
    发明授权
    Process of making an aromatic polyetherketone fiber product 失效
    制备芳香族聚醚酮纤维制品的方法

    公开(公告)号：US4849148A

    公开(公告)日：1989-07-18

    申请号：US107845

    申请日：1987-10-06

    Applicant: Martin H. G. Deeg

    Inventor： Martin H. G. Deeg

    IPC: D01F6/78 ,  C08G67/00 ,  C08G67/02 ,  D01D1/06 ,  D01D1/10 ,  D01F6/66 ,  D01F6/76

    CPC classification number: D01D1/106 ,  D01F6/665

    Abstract: Filaments are produced from polymers having an inherent viscosity of at least 0.7 measured in concentrated sulfuric acid and containing in the polmer chain at least 50 percent of the repeating units. ##STR1## by melting the polymer and heating the melt to a temperature of from about 20.degree. C. to about 80.degree. C. above the melting point of the polymer, passing the melt through a filter pack having a filtering area of at least about 8 in.sup.2 and a total volume of at least about 1.2 in.sup.3 per pound of polymer extruded per hour, and containing inert, irregularly shaped particles having a mesh size of about 25 to 140 to provide a pressure drop at least about 800 psig., and extruding the melt through spinning openings of desired shape to form filaments. The process is capable of producing fibers and yarns having a dpf of about 15 to 100, a tenacity of about 1 to 2 grams per denier, an elongation at break of about 50 to 160 percent and a modulus of about 20 to 30 grams per denier.

    Abstract translation: 长丝由浓硫酸中测定的特性粘度至少为0.7的聚合物制成，并且在聚合物链中含有至少50％的重复单元。 通过熔融聚合物并将熔体加热至高于聚合物熔点的约20℃至约80℃的温度，使熔体通过具有至少约 8英寸2，总体积为每磅聚合物挤出每小时至少约1.2英寸3，并且包含具有约25至140的筛孔尺寸的惰性，不规则形状的颗粒，以提供至少约800psig的压降，并且挤出 通过所需形状的纺丝开口熔化以形成长丝。 该方法能够生产具有约15至100 dpf的纤维和纱线，约1至2克/旦尼尔的韧度，约50至160％的断裂伸长率和约20至30克每旦旦的模量 。

    HIGH MELTING POINT RESIN FIBERS AND NONWOVEN FABRIC
    7.
    发明申请
    HIGH MELTING POINT RESIN FIBERS AND NONWOVEN FABRIC 审中-公开

    公开(公告)号：US20170298535A1

    公开(公告)日：2017-10-19

    申请号：US15517075

    申请日：2015-08-26

    Applicant: DAICEL CORPORATION

    Inventor： Takahiro TEI ,  Aya YOKOYAMA

    IPC: D01D5/00 ,  D04H1/728 ,  D01F6/66 ,  D04H3/016

    CPC classification number: D01D5/0092 ,  D01D5/0023 ,  D01D5/08 ,  D01F6/665 ,  D01F6/76 ,  D04H1/728 ,  D04H3/016

    Abstract: Provided are: a high-melting-point resin fiber having heat resistance and solvent resistance, offering excellent workability/formability, and having a diameter of 4 μm or less; and a nonwoven fabric including the high-melting-point resin fiber. Also provided is a method for efficiently producing a high-melting-point resin fiber having a diameter of 4 μm or less, via laser melt electrospinning. The high-melting-point resin fiber according to the present invention includes a resin having a melting point of 250° C. or higher and has a diameter of 4 μm or less. In the high-melting-point resin fiber, the resin having a melting point of 250° C. or higher is preferably a PEEK. The fiber preferably has a degree of crystallinity of 30% or less.

    Fiber or foil from polymers with high Tg and process for their manufacture
    10.
    发明授权
    Fiber or foil from polymers with high Tg and process for their manufacture 失效
    具有高Tg聚合物的纤维或箔片及其制造方法

    公开(公告)号：US08637583B2

    公开(公告)日：2014-01-28

    申请号：US13124078

    申请日：2009-10-16

    Applicant: Frank Hermanutz ,  Mark G. Reichmann

    Inventor： Frank Hermanutz ,  Mark G. Reichmann

    IPC: C08G75/23 ,  B29C55/28

    CPC classification number: D01D5/06 ,  D01F6/665 ,  D01F6/74 ,  D01F6/76

    Abstract: A process for the manufacture of a fiber or foil comprising at least one optionally functionalized polymer with a high Tg selected from the group consisting of poly(aryl ether sulfone) (PAES), poly(aryl ether ketone) (PAEK) and aromatic polyimide, comprising the steps of (aa) providing a solution comprising at least 45 wt. % of the polymer, and at least 20 wt. %, of at least one halogen-free organic solvent (S1) for the polymer, both wt % based upon the weight of the solution; (bb) pushing the solution through a nozzle; and (cc) introducing the solution into a coagulation bath comprising: (cc1) at least one liquid (L1) in which the polymer is insoluble, and optionally (cc2) at least one organic solvent (S2) for the polymer, identical to or different from the organic solvent (S1), to form a fiber or foil. A fiber or foil obtained by this process as well as to fibers or foils with specific porosity features and/or mechanical properties.

    Abstract translation: 一种纤维或箔的制造方法，其包含至少一种选自聚（芳基醚砜）（PAES），聚（芳基醚酮）（PAEK）（PAEK）和芳族聚酰亚胺）的高Tg的任选官能化聚合物， 包括以下步骤：（aa）提供包含至少45重量％ ％的聚合物，和至少20wt。 ％，为聚合物的至少一种无卤素有机溶剂（S1），均为基于溶液重量的wt％; （bb）通过喷嘴推动溶液; 和（cc）将溶液引入凝结浴，其包括：（cc1）至少一种其中聚合物不溶的液体（L1）和任选的（cc2）聚合物的至少一种有机溶剂（S2），与 与有机溶剂（S1）不同，形成纤维或箔。 通过该方法获得的纤维或箔以及具有特定孔隙特征和/或机械性能的纤维或箔。

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