公开(公告)号：US20130145685A1

公开(公告)日：2013-06-13

申请号：US13520480

申请日：2010-12-21

申请人： Holger Thielert

发明人： Holger Thielert

IPC分类号： B01D21/26

CPC分类号： B01D21/262 ,  C10C1/00

摘要： A device for separating a solid matter-containing, liquid and pumpable tar suspension from a coking reaction with direct use of the separated solid matter contained therein. The device consists of a centrifuge, which is arranged in the upper inner region of a carbon-storing container, and the centrifuge is equipped with a feed nozzle for solid matter-containing, liquid tar and with a discharge nozzle for liquid tar centrifugate. In the lower part, the centrifuge is equipped with an outlet for the solid matter contained in the tar, whereby the tar-containing solid matter obtained from the tar suspension does not have to be delivered or transported. Also disclosed is a method is for separating a solid matter-containing, liquid and pumpable tar suspension with delivery-free use of the separated solid matter contained therein using the device and to the use of the coal mixed with the solid matter.

摘要翻译： 一种用于从焦化反应中分离含固体物质，液体和可泵送的焦油悬浮液的装置，其直接使用其中包含的分离的固体物质。 该装置由离心机组成，该离心机布置在储碳容器的上部内部区域中，离心机配有含固体物质，液体焦油的进料喷嘴和用于液体焦油离心液的排出喷嘴。 在下部，离心机配备有用于焦油中固体物质的出口，由此从焦油悬浮液获得的含焦油固体物质不必被输送或输送。 还公开了一种用于使用该装置分离含固体物质，液体和可泵送的焦油悬浮液的方法，其中无需使用其中包含的分离的固体物质以及与固体物质混合的煤的使用。

公开(公告)号：US5656041A

公开(公告)日：1997-08-12

申请号：US658423

申请日：1996-06-05

申请人： Kevin L. Hylton

发明人： Kevin L. Hylton

IPC分类号： C10C1/00 ,  C10C1/20 ,  C10L5/48 ,  C10L5/00

CPC分类号： C10L5/48 ,  C10C1/00 ,  C10C1/20

摘要： In a process for detoxifying a coal-tar deposit, effective amounts of carbon and a calcium oxide containing substance are added at a mixing station to at least a portion of the coal-tar deposit. The reaction mixture thus formed is mixed at a temperature of about 70.degree. F. to 130.degree. F. for a time sufficient to detoxify it and convert it into a non-hazardous reaction product. The coal-tar deposit may be either a substantially homogeneous coal-tar or a heterogeneous coal-tar contaminated substrate. The mixing station site may be either subsurface or surface and may include a container. The non-hazardous reaction product may be separated into small particles, suitable as fuel, and large particles, suitable as safe fill.

摘要翻译： 在用于解燃煤焦油沉积物的过程中，将有效量的碳和含氧化钙的物质在混合站中加入到至少一部分煤焦油沉积物中。 将如此形成的反应混合物在约70°F至130°F的温度下混合足够的时间以使其解毒并将其转化为无害的反应产物。 煤焦油沉积物可以是基本均匀的煤焦油或异质煤焦油污染的底物。 混合站位置可以是地下或表面，并且可以包括容器。 非危险反应产物可以分成适合作为燃料的小颗粒，和适合作为安全填充物的大颗粒。

公开(公告)号：US5607770A

公开(公告)日：1997-03-04

申请号：US451537

申请日：1995-05-26

申请人： Irwin C. Lewis ,  Ronald A. Howard

发明人： Irwin C. Lewis ,  Ronald A. Howard

IPC分类号： C04B35/532 ,  C04B35/83 ,  C08L95/00 ,  C10C1/00 ,  B32B9/00

CPC分类号： C10C1/00 ,  C04B35/532 ,  C04B35/83 ,  C08L95/00 ,  Y10S428/902 ,  Y10T428/30 ,  Y10T442/2984

摘要： A unitary composite structure having improved flexural strength and a reduced coefficient of thermal expansion comprising a heterogeneous combination of a carbonaceous reinforcing material interbonded with a matrix material, wherein the said matrix material is a poorly graphitizing carbonaceous pitch containing polymerized and cross-linked aromatic components is disclosed. Graphite electrodes comprised of the poorly graphitized pitch matrix material acting as a binder and/or an impregnant are also disclosed. Processes for the preparation of the poorly graphitizing pitch, the composite structure, and particularly the graphite electrodes are disclosed as well.

摘要翻译： 具有改进的弯曲强度和降低的热膨胀系数的整体复合结构，其包括与基质材料相互结合的碳质增强材料的不均匀组合，其中所述基体材料是含有聚合和交联的芳族组分的不良石墨化碳质沥青是 披露 还公开了由作为粘合剂和/或浸渍剂的不良石墨化沥青基体材料构成的石墨电极。 还公开了用于制备不良石墨化间距，复合结构，特别是石墨电极的方法。

公开(公告)号：US5182011A

公开(公告)日：1993-01-26

申请号：US616836

申请日：1990-11-21

申请人： Masatoshi Tsuchitani ,  Makoto Tamura ,  Kiyotaka Suzuki ,  Shuji Okada ,  Ryoichi Nakajima ,  Sakae Naito

发明人： Masatoshi Tsuchitani ,  Makoto Tamura ,  Kiyotaka Suzuki ,  Shuji Okada ,  Ryoichi Nakajima ,  Sakae Naito

IPC分类号： C10C1/00 ,  C10C3/00

CPC分类号： C10C3/00 ,  C10C1/00

摘要： Commercially attractive continuous processes for the preparation of mesophase pitches for manufacturing high-performance carbon fibers are disclosed. One feature resides in that conversion of a pitch into a mesophase pitch is conducted continuously by using a unique continuous dispersion-heat-treating apparatus. The other feature resides in that the raw material for hydrogenation treatment which is a pretreatment preceeding to the final heat treatment for the production of a mesophase pitch, is prepared by using a heavy oil or pitch having substantially no BTX-insoluble material as the starting raw material, subjecting the raw material to a simple four-step treatment of (1) a continuous heat treatment in a tubular heater, (2) a distillation operation, (3) a BTX-solvent extraction and (4) a distillation operation; while recycling a soluble component obtained in the step (4) to the heat treatment of step (1) and recovering a BTX-solvent insoluble component formed in step (3) as the material for the hydrogenation treatment. This feature can provide a significant increase in the yield of a mesophase pitch. Furthermore, unexpectedly, the recycle of the soluble component into the heat treatment of step (1) is helpful to improve the characteristics of the ultimate products, i.e., carbon fibers or graphite fibers. Combination of the first and the second features, of course, can provide a better commercial success. In fact, the process of the present invention can provide a carbon fiber having a tensile strength of more than 300 kg/mm.sup.2 and a graphite fiber having a tensile strength of more than 400 kg/mm.sup.2 and a modulus of elasticity of more than 60 ton/mm.sup.2. Processes with minor modifications to the above are also disclosed.

摘要翻译： 公开了用于制备用于制造高性能碳纤维的中间相沥青的商业上有吸引力的连续方法。 一个特征在于，通过使用独特的连续分散热处理装置连续地进行沥青转化为中间相沥青。 另一个特征在于，通过使用基本上不含BTX不溶性材料的重油或沥青作为起始原料，制备作为用于生产中间相沥青的最终热处理之前的预处理的氢化处理原料 材料，对原料进行简单的四步处理（1）在管式加热器中的连续热处理，（2）蒸馏操作，（3）BTX-溶剂萃取和（4）蒸馏操作; 同时将步骤（4）中获得的可溶组分再循环到步骤（1）的热处理中，并回收步骤（3）中形成的BTX-溶剂不溶组分作为氢化处理材料。 该特征可以显着提高中间相沥青的产率。 此外，意想不到的是，将可溶组分再循环到步骤（1）的热处理中有助于改善最终产物即碳纤维或石墨纤维的特性。 结合第一和​​第二功能，当然可以提供更好的商业成功。 事实上，本发明的方法可以提供拉伸强度大于300kg / mm 2的碳纤维和拉伸强度大于400kg / mm 2的石墨纤维和大于60吨的弹性模量 / mm2。 还公开了对上述的微小修改的处理。

公开(公告)号：US4589975A

公开(公告)日：1986-05-20

申请号：US686651

申请日：1984-12-27

申请人： Kozo Yudate ,  Yukihiro Ohsugi ,  Mamoru Kamishita ,  Ken Nagasawa

发明人： Kozo Yudate ,  Yukihiro Ohsugi ,  Mamoru Kamishita ,  Ken Nagasawa

IPC分类号： C10C3/04 ,  C10C1/00 ,  D01F9/15 ,  C10C3/00 ,  C10C3/02 ,  D01F9/12

CPC分类号： C10C1/00

摘要： A method of producing a precursor pitch for use in the production of carbon fibers, which comprises hydrogenating a soft or middle tar pitch to obtain a hydrogenated pitch containing no free carbon and high molecular weight components and then subjecting it to a heat treatment. In this method, the hydrogenation is carried out in the presence of tetralin at a temperature of 400.degree.-450.degree. C., and the heat treatment after the removal of solvent insoluble components and solvent is carried out in an inert gas atmosphere at a temperature of 450.degree.-500.degree. C. and under a reduced pressure of 0.1-10 Torr.

摘要翻译： 一种生产用于生产碳纤维的前体沥青的方法，其包括将软或中焦油沥青加氢以获得不含游离碳和高分子量组分的氢化沥青，然后进行热处理。 在该方法中，在四氢化萘存在下，在400〜-450℃的温度下进行氢化，除去溶剂不溶性成分和溶剂后的热处理在惰性气体气氛中，在温度 450℃-500℃，减压0.1-10托。

公开(公告)号：US4429170A

公开(公告)日：1984-01-31

申请号：US398068

申请日：1982-07-14

申请人： Robert L. Lovell

发明人： Robert L. Lovell

IPC分类号： C10C1/04 ,  C10C1/00 ,  C10C1/20 ,  C07C37/74 ,  C07C37/68

CPC分类号： C10C1/00

摘要： A process is disclosed for purifying the tar acid mixture that is obtained from the Lurgi process of coal gasification. The tar acid is treated with dilute aqueous sulfuric acid solution to form non-volatile tar base salts from the tar base component and to hydrolyze the neutral oil component and then distilling the tar acid component off from the non-volatile tar base salts and the hydrolysis products of the neutral oil component.

摘要翻译： 公开了一种用于纯化从煤气化的Lurgi方法获得的焦油酸混合物的方法。 用稀硫酸水溶液处理焦油酸，从焦油基础组分中形成非挥发性焦油碱盐，并水解中性油组分，然后将焦油酸组分从非挥发性焦油碱盐中蒸馏出来，水解 产品的中性油组分。

公开(公告)号：US2936282A

公开(公告)日：1960-05-10

申请号：US2936282D

IPC分类号： B01D15/08 ,  C10C1/00 ,  G01N25/14

CPC分类号： C10C1/00 ,  B01D15/08 ,  B01D15/1871 ,  B01D15/426 ,  G01N25/14

公开(公告)号：US2838447A

公开(公告)日：1958-06-10

申请号：US39748753

申请日：1953-12-10

申请人： ALLIED CHEM & DYE CORP

发明人： VINCENT SAVERCOOL JOHN

IPC分类号： C10C1/00

CPC分类号： C10C1/00

公开(公告)号：US2775550A

公开(公告)日：1956-12-25

申请号：US42367654

申请日：1954-04-16

申请人： KOPPERS CO INC

发明人： HARLOW EARL V

IPC分类号： C10C1/00

CPC分类号： C10C1/00

公开(公告)号：US2683107A

公开(公告)日：1954-07-06

申请号：US25001551

申请日：1951-10-05

申请人： GREAT LAKES CARBON CORP

发明人： HARRISVILLE JUEL LESLIE

IPC分类号： C10C1/00 ,  C10L5/14 ,  C25C7/02 ,  D01F11/14

CPC分类号： D01F11/14 ,  C10C1/00 ,  C10L5/14 ,  C25C7/025