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    Halogenated alkoxysilane intermediate compounds and their preparation
    5.
    发明授权
    Halogenated alkoxysilane intermediate compounds and their preparation 失效
    卤代烷氧基硅烷中间体化合物及其制备方法

    公开(公告)号：US3960913A

    公开(公告)日：1976-06-01

    申请号：US616437

    申请日：1975-09-24

    申请人： Karl O. Knollmueller

    发明人： Karl O. Knollmueller

    IPC分类号： C10M105/76 ,  C07F7/08 ,  C07F7/12 ,  C07F7/18 ,  C10N40/08 ,  C07F7/04

    CPC分类号： C07F7/0861 ,  C07F7/1808

    摘要： Halogenated alkoxysilane intermediate compounds are described having the formula RSi[OSi(OR').sub.3 ].sub.2 X wherein X is a halogen, R is hydrogen, an alkyl, alkenyl, aryl or aralkyl group and each R' is independently selected from the same group as R with the proviso that at least a majority of R' radicals are sterically hindered alkyl groups having at least 3 carbon atoms. The preparation of these compounds is also described.

    摘要翻译： 描述了具有式RSi [OSi（OR'）3] 2X的卤化烷氧基硅烷中间体化合物，其中X是卤素，R是氢，烷基，烯基，芳基或芳烷基，并且每个R'独立地选自与 R，条件是至少大部分R'基团是具有至少3个碳原子的空间位阻烷基。 还描述了这些化合物的制备。

    Chlorine, hydroxy and alkoxy endblocked trimethylsiloxysiloxanes
    6.
    发明授权
    Chlorine, hydroxy and alkoxy endblocked trimethylsiloxysiloxanes 失效
    氯，羟基和烷氧基封端的三甲基甲硅烷氧基硅氧烷

    公开(公告)号：US3308148A

    公开(公告)日：1967-03-07

    申请号：US30521663

    申请日：1963-08-28

    申请人： DOW CORNING

    发明人： HAHN JAMES R ,  LENTZ CHARLES W

    IPC分类号： B27K3/15 ,  C07F7/08 ,  C07F7/12 ,  C07F7/18 ,  C07F7/21 ,  C08G77/16 ,  C08G77/18 ,  C08G77/38 ,  C23F15/00

    CPC分类号： C23F15/00 ,  C07F7/0858 ,  C07F7/0861 ,  C07F7/0867 ,  C07F7/0896 ,  C07F7/12 ,  C07F7/1808 ,  C07F7/21 ,  C08G77/16 ,  C08G77/18 ,  C08G77/38

    摘要： The invention comprises siloxanes of the formula wherein X is a halogen atom or an alkoxy or hydroxyl radical and n is zero or an integer. The halogen-terminated siloxanes can be made by halogenating the corresponding H-containing siloxanes (which can be made by co-hydrolysis and condensation of [(CH3)3SiO]2Si(OCH3)2 and [(CH3)3SiO]2H.SiOCH3), and the hydroxylate and alkoxylated siloxanes can be obtained from the halogenated siloxanes by hydrolysis and alcoholysis respectively. Examples describe the preparation of {[CH3)3SiO]2XSi}2O, in which X is (1) Cl, (2, 3) -OH and (4) -OCH3, -OC2H5, -OCH(CH3)2 and -OC4H9; Example (5) describes the preparation of siloxanes of the above general formula in which n is 1, 2, 3, 4, 5, 10, 15, 25, 50, 100 and 1500, and X is Cl, -OH, or alkoxy as specified in Example (4). Uses.-Fluid springs, hydraulic fluids and lubricants or as protective coatings for metals, wood and glass. The H-containing siloxanes can be made as follows:

    摘要翻译： 本发明包括式的硅氧烷，其中X是卤素原子或烷氧基或羟基，n是0或整数。 卤素封端的硅氧烷可以通过卤化相应的含H的硅氧烷（其可以通过共[C 3] 3 SiO] 2 Si（OCH 3）2和[（CH 3）3 SiO] 2H.SiOCH 3） ，羟基化和烷氧基化硅氧烷可以分别通过水解和醇解由卤化硅氧烷获得。 实例描述了{[CH 3）3 SiO] 2 XSi} 2 O的制备，其中X是（1）Cl，（2,3）-OH和（4）-OCH 3，-OC 2 H 5，-OCH（CH 3）2和-OC 4 H 9 ; 实施例（5）描述了上述通式的硅氧烷的制备，其中n为1,2,3,4,5,10,15,25,50,100和1500，X为Cl，-OH或烷氧基 如实施例（4）所述。 用途 - 流体弹簧，液压油和润滑剂或金属，木材和玻璃的保护涂层。 含H的硅氧烷可如下制备：

    Method for the preparation of alkoxysilane cluster compounds
    7.
    发明授权
    Method for the preparation of alkoxysilane cluster compounds 失效
    烷氧基硅烷簇化合物的制备方法

    公开(公告)号：US4077993A

    公开(公告)日：1978-03-07

    申请号：US791358

    申请日：1977-04-27

    申请人： Karl O. Knollmueller

    发明人： Karl O. Knollmueller

    IPC分类号： C07F7/04 ,  C07F7/02 ,  C07F7/18

    CPC分类号： C07F7/1808 ,  C07F7/025

    摘要： An improved method is disclosed for preparing alkoxysilane cluster compounds having the formula:RSi[OSi(OR').sub.3 ].sub.3wherein R is hydrogen, an alkyl, alkenyl, aryl or aralkyl group and each R' is independently selected from alkyl, alkenyl, aryl and aralkyl with the proviso that at least a majority of the R' radicals are sterically hindered alkyl groups having at least 3 carbon atoms. The improved preparation method involves reacting a substituted trihalosilane with a trialkoxysilanol in the presence of a critical amount of an acceptor base in a solvent reaction medium while maintaining the reactor temperature within a select range.

    摘要翻译： 公开了一种用于制备具有下式的烷氧基硅烷簇化合物的改进方法：