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1.发明授权公开(公告)号：US12098078B1
公开(公告)日：2024-09-24
申请号：US18408250
申请日：2024-01-09
Inventor： Khaled Masoud Mohamed Masoud
CPC classification number: C01C1/026 , C01C1/024 , G01N30/7206 , G01N2030/025
Abstract: A method of supplying ammonia to a gas chromatography-chemical ionization tandem mass spectrometry (GC/CI-MS/MS) includes the steps of: providing ammonium carbonate and diethanolamine in a reaction vessel; heating the reaction vessel to a temperature of 50-60° C. to decompose the ammonium carbonate to form ammonia, carbon dioxide and water; absorbing the carbon dioxide and water by the diethanolamine to form diethanolamine carbonate; and supplying the ammonia to the GC/CI-MS/MS. Another method of supplying ammonia to a gas chromatography-chemical ionization tandem mass spectrometry (GC/CI-MS/MS) includes the steps of: providing ammonium carbonate and a mixture of monoethanolamine and diethanolamine in a reaction vessel; reacting the ammonium carbonate with the monoethanolamine to form ammonia and monoethanolamine carbonate; and supplying the ammonia to the GC/CI-MS/MS.
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公开(公告)号：US20150284256A1
公开(公告)日：2015-10-08
申请号：US14246513
申请日：2014-04-07
Applicant: The Boeing Company
Inventor： Jason M. Siegel , Wen-teh Chen , Steven J. Adam
Abstract: A system for ammonia distillation may include a condenser to condense ammonia vapor into liquid anhydrous ammonia, a flush tank to receive a flushed portion of the liquid anhydrous ammonia, a collection tank to receive a collected portion of the liquid anhydrous ammonia, and a corrosion inhibitor dispenser to transfer a corrosion inhibitor to the collected portion of the liquid anhydrous ammonia to form corrosion-inhibiting liquid anhydrous ammonia.
Abstract translation: 用于氨蒸馏的系统可以包括用于将氨蒸汽冷凝成液体无水氨的冷凝器，用于接收液体无水氨的冲洗部分的冲洗槽，用于接收液体无水氨的收集部分的收集罐，以及腐蚀抑制剂 分配器将腐蚀抑制剂转移到液体无水氨的收集部分以形成腐蚀抑制液体无水氨。
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3.发明申请公开(公告)号：US20120145949A1
公开(公告)日：2012-06-14
申请号：US12973434
申请日：2010-12-20
Applicant: Jiarong Zhan , Li Zhou
Inventor： Jiarong Zhan , Li Zhou
IPC: C09K13/00
CPC classification number: C01C1/162 , C01C1/024 , C01P2004/62 , C01P2006/80
Abstract: The present invention relates to a method for producing of electronic grade aqueous ammonium fluoride solution. The industrial grade liquid ammonia is used as the raw material, when it is heated, the ammonia gas will be released. The organic gas impurities in the ammonia gas are removed by activated charcoal, and the oxygen is removed by deoxidizer, and then the high-purity ammonia gas is gotten. The high-purity hydrofluoric acid absorbs and reacts with the high-purity ammonia gas to obtain the electronic grade aqueous ammonium fluoride solution. The product has high-purity and stable quality, and it can be used in producing of electronic products directly. The method for producing of electronic grade ammonium aqueous fluoride solution provided by the present invention is suitable for continuous production on a large scale because of its simple operation.
Abstract translation: 本发明涉及电子级氟化铵水溶液的制造方法。 工业级液氨用作原料，加热时氨气将被释放。 通过活性炭除去氨气中的有机气体杂质，通过脱氧剂除去氧气，然后得到高纯度氨气。 高纯度氢氟酸吸收并与高纯氨气反应，得到电子级氟化铵水溶液。 该产品具有高纯度，质量稳定，可直接用于电子产品的生产。 本发明提供的电子级氟化铵水溶液的制造方法由于操作简单，适合大规模连续生产。
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公开(公告)号：US20110033361A1
公开(公告)日：2011-02-10
申请号：US12936375
申请日：2009-03-26
Applicant: Roland Bou Chedid , Gabriele Iffland , Jürgen Ciprian , Johann-Peter Melder , Frank-Friedrich Pape
Inventor： Roland Bou Chedid , Gabriele Iffland , Jürgen Ciprian , Johann-Peter Melder , Frank-Friedrich Pape
IPC: C01C1/00 , C01B21/087
Abstract: The present invention relates to a method for depleting halide ions from liquid ammonia, wherein the liquid ammonia is brought into contact with a strongly basic ion exchanger, where the basic structure of the strongly basic ion exchanger is a covalently crosslinked polymer matrix. Furthermore, the present invention relates to the use of an ammonia obtainable according to the invention as starting material in the production of amines.
Abstract translation: 本发明涉及从液氨中消耗卤离子的方法，其中液态氨与强碱性离子交换剂接触，其中强碱性离子交换剂的基本结构是共价交联的聚合物基体。 此外，本发明涉及根据本发明可获得的氨作为制备胺的原料的用途。
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公开(公告)号：US07297181B2
公开(公告)日：2007-11-20
申请号：US11009510
申请日：2004-12-13
Applicant: Derong Zhou , John P. Borzio , Mindi Xu , Hwa-Chi Wang , Tran Vuong
Inventor： Derong Zhou , John P. Borzio , Mindi Xu , Hwa-Chi Wang , Tran Vuong
CPC classification number: B01D53/261 , B01D53/02 , C01C1/024 , Y10S203/17
Abstract: An ammonia purification system includes a hydrocarbon removal station that removes hydrocarbons from gaseous ammonia via adsorption, a moisture removal station that removes water from gaseous ammonia via adsorption, and a distillation station including a distillation column connected with a condenser to facilitate removal of impurities from ammonia and condensation of gaseous ammonia to form a purified liquid ammonia product. The system further includes a storage tank to receive purified ammonia, a remote station connected with the storage tank, and a vaporizer connected with the storage tank. The vaporizer is configured to receive and vaporize liquid ammonia from the storage tank and deliver gaseous ammonia back to the storage tank so as to facilitate pumping of the ammonia to the remote station based upon a vapor pressure established within the storage tank.
Abstract translation: 氨净化系统包括通过吸附从气态氨除去烃的除烃站，通过吸附从气态氨除去水的除湿站，以及包括与冷凝器连接的蒸馏塔以便于从氨除去杂质的蒸馏站 和气态氨的缩合形成纯化的液氨产物。 该系统还包括用于接收净化氨的储罐，与储罐连接的远程站以及与储存罐连接的蒸发器。 蒸发器被配置为从储罐接收和蒸发液氨，并将气态氨返回到储罐，以便于基于在储罐内建立的蒸汽压力将氨泵送到远程站。
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Patent Agency Ranking
公开(公告)号：US07108737B2
公开(公告)日：2006-09-19
申请号：US10472846
申请日：2002-03-04
Applicant: Ewald Neumann , Wolfgang Himmler , Werner Büttner , Harald Fritsch , Hans-Jürgen Schmidt , Martin Hostalek
Inventor： Ewald Neumann , Wolfgang Himmler , Werner Büttner , Harald Fritsch , Hans-Jürgen Schmidt , Martin Hostalek
CPC classification number: B01D53/1418 , B01D53/229 , C01B7/0706 , C01B7/195 , C01C1/024
Abstract: The present invention relates to a novel process for the preparation of high-purity chemicals with an extremely low particle count, such as ammonia gas, hydrogen fluoride and hydrogen chloride, which are also used as aqueous solutions in semiconductor technology the corrosive gas is enriched with an absorbent which is miscible with the gas and in which impurities present in the gas are soluble, and the gas is subsequently subjected to membrane filtration.
Abstract translation: 本发明涉及一种用于制备具有极低的颗粒数的高纯度化学品的新方法，例如氨气，氟化氢和氯化氢，它们也用作半导体技术中的水溶液，腐蚀性气体富含 与气体混溶并且气体中存在的杂质可溶的吸收剂，随后对气体进行膜过滤。
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7.发明申请公开(公告)号：US20050260108A1
公开(公告)日：2005-11-24
申请号：US11130505
申请日：2005-05-17
Applicant: Thomas Del Prato , Harold Spicer
Inventor： Thomas Del Prato , Harold Spicer
CPC classification number: C01C1/086 , B01D53/79 , C01C1/024 , C01P2006/80
Abstract: A system and method for generating, purifying, and using ultra-pure ammonia on-site, such as at a semiconductor manufacturing facility. The system includes an ammonia generation system configured to generate ammonia including carbon dioxide, water, and other impurities. A purification system is provided with the generation system in the manufacturing facility and is linked to the output of the generation system. The purification system processes the effluent from the ammonia generation system to remove substantially all of the carbon dioxide, water, and other impurities to produce an outlet stream of ultra-pure ammonia. The system further includes a point of use system provided at the same manufacturing facility to utilize the outlet stream of ultra-pure ammonia.
Abstract translation: 用于生产，净化和使用现场超纯氨的系统和方法，例如在半导体制造设备。 该系统包括氨生成系统，其被配置为产生包括二氧化碳，水和其它杂质的氨。 净化系统在制造设施中具有发电系统，并与发电系统的输出相连接。 净化系统处理来自氨生成系统的流出物以除去基本上所有的二氧化碳，水和其它杂质，以产生超纯氨的出口流。 该系统还包括设置在同一制造设施处以利用超纯氨出口流的使用点系统。
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公开(公告)号：US06892473B1
公开(公告)日：2005-05-17
申请号：US10730505
申请日：2003-12-08
Applicant: Robert Ling Chiang , Roger Dean Whitley , Dingiun Wu , Chun Christine Dong , Madhukar Bhaskara Rao
Inventor： Robert Ling Chiang , Roger Dean Whitley , Dingiun Wu , Chun Christine Dong , Madhukar Bhaskara Rao
IPC: B01J19/00 , B01D53/28 , B01J8/00 , B01J19/02 , B01J20/04 , B01J20/32 , C01B21/04 , C01B23/00 , C01C1/02 , F26B3/00
CPC classification number: B01D53/28 , B01J20/041 , B01J20/08 , B01J20/28057 , B01J20/3078 , B01J20/3204 , B01J20/3236 , B01J2220/42 , B01J2220/56 , C01B21/0455 , C01B23/0057 , C01B2210/0042 , C01B2210/0062 , C01C1/024
Abstract: This invention relates to an improvement in a process for removing water from a hydride gas, and particularly ammonia, by contacting the hydride gas with a drying agent under conditions for effecting removal of the water. The improvement for significantly reducing the water content to trace levels in said hydride gas resides in the use of at least Group 1 metal oxide and at least one Group 2 metal oxide as a drying agent.
Abstract translation: 本发明涉及通过在有效去除水分的条件下使氢化物气体与干燥剂接触而从氢化物气体，特别是氨中除去水的方法。 在所述氢化物气体中显着降低水含量至痕量水平的改进在于使用至少第1族金属氧化物和至少一种第2族金属氧化物作为干燥剂。
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公开(公告)号：US20040089152A1
公开(公告)日：2004-05-13
申请号：US10472846
申请日：2003-09-26
Inventor： Ewald Neumann , Wolfgang Himmler , Werner Buttner , Harald Fritsch , Hans-Jurgen Schmidt , Martin Hostalek
IPC: B01D047/00
CPC classification number: B01D53/1418 , B01D53/229 , C01B7/0706 , C01B7/195 , C01C1/024
Abstract: The present invention relates to a novel process for the preparation of high-purity chemicals with an extremely low particle count, such as ammonia gas, hydrogen fluoride and hydrogen chloride, which are also used as aqueous solutions in semiconductor technology the corrosive gas is enriched with an absorbent which is miscible with the gas and in which impurities present in the gas are soluble, and the gas is subsequently subjected to membrane filtration.
Abstract translation: 本发明涉及一种用于制备具有极低的颗粒数的高纯度化学品的新方法，例如氨气，氟化氢和氯化氢，它们也用作半导体技术中的水溶液，腐蚀性气体富含 与气体混溶并且气体中存在的杂质可溶的吸收剂，随后对气体进行膜过滤。
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10.发明授权公开(公告)号：US06706093B2
公开(公告)日：2004-03-16
申请号：US09847126
申请日：2001-05-02
Applicant: Abraham Benderly , Michael Stanley DeCourcy , Ronald Eugene Myers
Inventor： Abraham Benderly , Michael Stanley DeCourcy , Ronald Eugene Myers
IPC: B01D5314
CPC classification number: B01J8/006 , B01J19/002 , B01J19/02 , B01J2219/00247 , B01J2219/00252 , B01J2219/0204 , B01J2219/0209 , B01J2219/0245 , B01J2219/0286 , C01C1/024 , C01C1/12
Abstract: A method which reduces iron contamination of a system which receives ammonia from an ammonia recovery process by one or more of the following techniques: a) Physically separating iron oxide, iron containing colloidal particles, and liquid droplets from the gas stream; b) Preventing AC from depositing on piping via elimination of condensation, thereby preventing corrosion of the piping; or c) Installing piping and equipment that is not susceptible to corrosive attack by AC, thereby eliminating the source of iron contamination.
Abstract translation: 一种通过一种或多种以下技术从氨回收过程中减少接收氨的系统的铁污染的方法：a）从气流中物理分离氧化铁，含铁的胶体颗粒和液滴; b）防止AC 通过消除冷凝而沉积在管道上，从而防止管道腐蚀; orc）安装不受AC腐蚀性侵害的管道和设备，从而消除铁污染源。
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