Perovskite film layer, device and preparation method for effectively improving efficiency of light-emitting device

    公开(公告)号:US11158830B2

    公开(公告)日:2021-10-26

    申请号:US16771230

    申请日:2018-12-05

    摘要: The disclosure discloses a perovskite film layer, a device and a preparation method for effectively improving the efficiency of perovskite optoelectronics. The perovskite film layer consists of a layer with discontinuous, irregularly distributed perovskite crystal grains and an organic insulating layer with a low refractive index embedded between the perovskite crystal grains. The perovskite crystal grains form a plurality of convex portions, and the organic insulating layer forms a plurality of concave portions between the convex portions. By adding an excess of an alkylammonium salt and/or an organic molecule with a specific functional group to perovskite precursor solution, a concave-convex film layer structure is spontaneously formed, and an upper charge transport layer and an electrode form pleated concave-convex structures. Such a special perovskite thin film structure formed by a simple solution method can effectively improve the light-outcoupling efficiency and enhance the performance of the perovskite light-emitting device.

    METHOD FOR PREPARING COMPOSITE METAL OXIDE HOLLOW FIBRE

    公开(公告)号:US20200062657A1

    公开(公告)日:2020-02-27

    申请号:US16466066

    申请日:2017-05-10

    摘要: The invention relates to a method for preparing a composite metal oxide hollow fibre. A certain stoichiometry of composite metal oxide raw material and a polymer binding agent are added to an organic solvent, and mixed mechanically to obtain an evenly dispersed spinning solution having a suitable viscosity. After defoaming treatment, the spinning solution is extruded through a spinneret and, after undergoing a certain dry spinning process, enters an external coagulation bath; during this period, a phase inversion process occurs and composite metal oxide hollow fibre blanks are formed. The blanks are immersed in the external coagulation bath and the organic solvent is displaced; after natural drying, the blanks undergo a heat treatment process; during this period, polymer burn off, in situ reaction, and in situ sintering processes occur to obtain the composite metal oxide hollow fibre.

    NUCLEOTIDE PRODUCTION PROCESS
    3.
    发明申请

    公开(公告)号:US20170130254A1

    公开(公告)日:2017-05-11

    申请号:US15127373

    申请日:2014-03-26

    IPC分类号: C12P19/30

    CPC分类号: C12P19/30 C12Y301/11005

    摘要: A nucleotide production process comprises: decomposing an RNA by using a nuclease P1 so as to obtain nucleotides AMP, GMP, CMP and UMP, converting part or all of the nucleotide AMP into a nucleotide IMP by using adenosine deaminase, separating the obtained nucleotide by using an ion exchange resin, and then performing concentration and crystallization to obtain purified nucleotides AMP, GMP, CMP, UMP and IMP or obtain purified nucleotides GMP, CMP, UMP and IMP. The whole biocatalysis production of nucleotides is implemented by using a double-enzyme catalysis method, and high-purity nucleotides are obtained by using an ion resin separation technology and a solvent crystallization method; and the production process is simple and environmentally-friendly, and has low costs, high product safety and purity.

    Preparation method of lycopene intermediate 3-methyl-4,4-dialkoxy-1-butaldehyde
    7.
    发明授权
    Preparation method of lycopene intermediate 3-methyl-4,4-dialkoxy-1-butaldehyde 有权
    番茄红素中间体3-甲基-4,4-二烷氧基-1-丁醛的制备方法

    公开(公告)号:US08993810B2

    公开(公告)日:2015-03-31

    申请号:US14369137

    申请日:2012-12-10

    IPC分类号: C07C45/00 C07C45/30 C07C41/22

    摘要: Disclosed is a preparation method of the lycopene intermediate 3-methyl-4,4-dialkoxy-1-butaldehyde. The preparation method comprises the following steps: (1) reacting 2-methyl-3,3-dialkoxy-1-halopropane with magnesium powder in the solvent of anhydrous tetrahydrofuran at a temperature of 45˜65° C. to generate a mixture of Grignard reagents under the protection of an inert gas; and (2) adding N,N-disubstituted carboxamide to the mixture of Grignard reagents and reacting at a temperature of 10° C.˜35° C. to obtain 3-methyl-4,4-dialkoxy-1-butaldehyde. The process route of the present invention is simple and direct, the operation is easy, the conditions are mild and the yield is good, and thus the invention has commercial value.

    摘要翻译: 公开了番茄红素中间体3-甲基-4,4-二烷氧基-1-丁醛的制备方法。 制备方法包括以下步骤:(1)在45〜65℃的温度下,将2-甲基-3,3-二烷氧基-1-卤代丙烷与镁粉末在无水四氢呋喃的溶剂中反应,生成格利雅 在惰性气体保护下的试剂; 和(2)将N,N-二取代的甲酰胺加入到格氏试剂混合物中,并在10℃〜35℃的温度下反应,得到3-甲基-4,4-二烷氧基-1-丁醛。 本发明的工艺路线简单直接,操作容易,条件温和,产量好,因此本发明具有商业价值。

    MEDIUM AND HIGH-TEMPERATURE CARBON-AIR CELL
    8.
    发明申请
    MEDIUM AND HIGH-TEMPERATURE CARBON-AIR CELL 有权
    中高碳气囊

    公开(公告)号:US20150050579A1

    公开(公告)日:2015-02-19

    申请号:US14387942

    申请日:2013-03-26

    IPC分类号: H01M8/12 H01M8/00 H01M8/10

    摘要: The present invention relates to a medium and high-temperature carbon-air cell, which include a solid oxide fuel cell, a CO2 separation membrane and a carbon fuel. The solid oxide fuel cell is a tubular solid oxide fuel cell with one end closed, the carbon fuel is placed inside the tubular solid oxide fuel cell, and the CO2 separation membrane is sealed at the open end of the solid oxide fuel cell. In the carbon-air cell, with carbon as fuel and oxygen in the air as an oxidizing gas, electrochemical reactions occur. The carbon-air cell of the present invention has a novel structural design, and can achieve electricity generation with the solid oxide fuel cell without externally charging a gas, and at the same time, CO2 generated inside the solid oxide fuel cell can be discharged from the system through the CO2 separation membrane in time.

    摘要翻译: 本发明涉及一种中高温碳空气电池,其包括固体氧化物燃料电池,CO 2分离膜和碳燃料。 固体氧化物型燃料电池是一端封闭的管状固体氧化物型燃料电池,碳素燃料配置在管状固体氧化物型燃料电池内,CO 2分离膜密封在固体氧化物型燃料电池的开放端。 在碳 - 空气池中,作为燃料的碳和空气中的氧作为氧化气体,发生电化学反应。 本发明的碳 - 空气电池具有新的结构设计,并且可以在不从外部充入气体的状态下实现固体氧化物型燃料电池的发电,同时可以在固体氧化物型燃料电池内产生的CO 2从 系统通过CO2分离膜及时。

    ANTI-COLLISION DEVICE MADE OF BUFFERING ENERGY-ABSORBING TYPE WEB-ENHANCED COMPOSITE MATERIAL
    9.
    发明申请
    ANTI-COLLISION DEVICE MADE OF BUFFERING ENERGY-ABSORBING TYPE WEB-ENHANCED COMPOSITE MATERIAL 审中-公开
    缓冲能量吸收型增强复合材料的抗碰撞装置

    公开(公告)号:US20140130725A1

    公开(公告)日:2014-05-15

    申请号:US14126497

    申请日:2011-12-30

    IPC分类号: E01F15/14 B63B59/02

    摘要: An anti-collision device made of a buffering energy-absorbing type web-enhanced composite material, including an anti-collision unit. The anti-collision unit includes a housing and a filling material body located in the housing, and the housing is a solid housing formed of a composite material surface layer or a sandwiched housing formed of a composite material surface layer internally filled with a sandwiched material, and the sandwiched material; the filling material body includes a space lattice body and an energy consuming material, the space lattice body is formed of fiber webs arranged in the housing in a single-layered unidirectional, single-layered bidirectional, multi-layered unidirectional or multi-layered multi-directional manner, and the energy consuming material is located between the fiber webs and/or between the fiber webs and inner walls of the housing.

    摘要翻译: 一种由缓冲能量吸收型网状增强复合材料制成的防碰撞装置,包括防撞单元。 防撞单元包括位于壳体中的壳体和填充材料体,并且壳体是由复合材料表面层或由内部填充有夹层材料的复合材料表面层形成的夹层壳体形成的实心壳体, 和夹层材料; 填充材料体包括空间格子体和能量消耗材料,空间格子体由布置在壳体中的单层单向,单层双向,多层单向或多层多层单层多层多层结构的纤维网形成, 并且能量消耗材料位于纤维幅材之间和/或位于纤维幅材和壳体的内壁之间。

    Cleaning process of producing lactic acid
    10.
    发明授权
    Cleaning process of producing lactic acid 有权
    生产乳酸的清洗工艺

    公开(公告)号:US08545685B2

    公开(公告)日:2013-10-01

    申请号:US13127307

    申请日:2009-04-20

    IPC分类号: B01D61/42 B01D61/58

    摘要: Provided is a cleaning process of producing lactic acid. Firstly saccharification liquid is prepared through saccharated materials, then fermented with nutritive materials and lactic acid bacteria, and liquid alkali is used to adjust the pH. The fermentation broth is filtrated with porous membrane, and the lactic acid bacteria in the interception liquid are then reintroduced into the porous membrane for recycling. The permeate from porous membrane is subjected to nanofiltration to be decolored and purified. The concentrated solution from nanofiltration and the cleaning liquid from fermentation tank and its affiliated equipment are filtrated and sterilized by using ceramic membrane, and then are reintroduced into the fermentation unit for recycling. The permeate from nanofiltration is then subjected to bipolar electrodialysis system to prepare lactic acid, and the liquid alkali produced at the same time is reintroduced into the fermentation tank for recycling. The lactic acid is finally concentrated by using vacuum distillation. The process recycles the bacteria in the liquid alkali and matured fermentation broth, and is characterized by low material consumption and emission, low pollution, reduced cost and cleanness and environmentally protection of the whole production process.

    摘要翻译: 提供了生产乳酸的清洗方法。 首先通过糖化物质制备糖化液,然后用营养物质和乳酸菌发酵,并使用液态碱调节pH值。 用多孔膜过滤发酵肉汤,然后将拦截液中的乳酸菌重新引入多孔膜进行再循环。 将来自多孔膜的渗透物进行纳滤,进行脱色和纯化。 来自纳滤的浓缩溶液和来自发酵罐及其附属设备的清洗液通过陶瓷膜过滤灭菌,然后重新引入发酵单元进行再循环。 然后将来自纳滤的渗透物进行双极电渗析系统以制备乳酸,同时产生的液碱再次引入发酵罐中进行再循环。 最后通过真空蒸馏浓缩乳酸。 该工艺循环利用液态碱和成熟发酵液中的细菌,其特点是材料消耗低,污染少,成本低廉,整个生产过程的清洁和环保。