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公开(公告)号：US4383047A
公开(公告)日：1983-05-10
申请号：US234521
申请日：1981-02-17
IPC分类号： G01N30/02 , B01D15/08 , B01D15/36 , B01J41/20 , B01J47/00 , G01N30/56 , G01N30/96 , B01J41/06
CPC分类号： B01D15/363 , B01J20/2803 , B01J20/3221 , B01J41/20 , B01J47/006 , G01N30/56 , G01N30/96 , B01J2220/54
摘要： An improved pellicular type (agglomerated) anion-exchange chromatographic packing composition which comprises:Component A, a substrate which consists essentially of particles of insoluble synthetic resin, having cation-exchanging sites at least on their available surfaces, the Component A particles being of a diameter of between about 5 to 75 microns and of low porosity relative to Component B microparticles, described below, andComponent B, which consists essentially of microparticles of insoluble synthetic resin, having a volume average diameter of less than about 900 and greater than about 50 Angstroms, the microparticles having anion-exchanging sites, at least on their outer surfaces, which attract available cation sites of Component A, wherein the microparticles of Component B are attached as a monolayer to the available surfaces of the Component A particles.
摘要翻译： 改进的薄膜型（聚集）阴离子交换色谱填充组合物，其包含：组分A，基本上由至少在其可用表面上具有阳离子交换位点的不溶性合成树脂颗粒组成的底物，组分A颗粒为 直径为约5至75微米且相对于下文所述的组分B微粒为低孔隙率，组分B主要由体积平均直径小于约900且大于约50的不溶性合成树脂微粒组成 埃，至少在其外表面上具有阴离子交换位点的微粒，其吸引组分A的可用阳离子位点，其中组分B的微粒作为单层附着到组分A颗粒的可用表面上。
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公开(公告)号：US4519905A
公开(公告)日：1985-05-28
申请号：US626569
申请日：1984-07-02
IPC分类号： B01D15/08 , B01J20/286 , B01J41/20 , G01N30/56 , G01N30/96
CPC分类号： B01J20/286 , B01J20/3221 , B01J41/20 , G01N30/56 , G01N30/96 , B01J2220/54 , B01J2220/58
摘要： An improved chromatographic analytical column, the column containing a pellicular type (agglomerated) anion-exchange packing, comprising:Component A, which comprises a pressure packed bed of substrate particles of insoluble synthetic resin, having cation-exchanging sites at least on their available surfaces, the Component A particles being of low porosity relative to Component B microparticles, described below, andComponent B, derived by agglomerating microparticles of insoluble synthetic resin onto the pressure packed bed of Component A particles, the microparticles having a volume average diameter of less than about 1,500 and greater than about 50 Angstroms and having anion-exchanging sites, at least on their outer surfaces, which attract available cation sites of Component A, wherein the microparticles of Component B are attached as a monolayer to the available surfaces of the Component A particles.
摘要翻译： 一种改进的色谱分析柱，该柱包含薄膜型（聚集）阴离子交换填料，其包含：组分A，其包含不溶性合成树脂的基质颗粒的压力填充床，至少在其可用表面上具有阳离子交换位点 组分A颗粒相对于下述组分B微粒具有低孔隙率，以及组分B，其通过将不溶性合成树脂的微粒聚集到组分A颗粒的加压填充床上而得到，微粒的体积平均直径小于 至少在其外表面上具有阴离子交换位点，其吸引组分A的可用阳离子位点，其中组分B的微粒以单层的形式附着到组分A的可用表面上 粒子。
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3.发明授权High performance anion-exchange chromatographic packing composition consisting of low porosity synthetic resin gel particle substrate coated with liquid water-soluble aminated resin 失效高性能阴离子交换色谱填料组合物由低孔隙率合成树脂凝胶颗粒基体组成，涂有液体水溶性胺化树脂
公开(公告)号：US4927539A
公开(公告)日：1990-05-22
申请号：US262074
申请日：1988-10-24
CPC分类号： B01D15/363 , B01J20/3221 , B01J41/20 , B01J47/006 , B01J2220/54
摘要： An anion-exchange chromatographic packing composition which comprises:a substrate which consists essentially of particles having cation-exchanging sites at least on their available surfaces, the particles being of a diameter of between about 1 to about 75 microns; anda liquid coating which consists essentially of a hydrophilic, water soluble, film forming resin having anion-exchanging sites which attract available cation-exchanging sites of the substrate, wherein the liquid coating is retained by electrostatic bonds on the available surfaces of the substrate particles. The invention further includes a chromatographic column and process using the described packing composition.
摘要翻译： 阴离子交换色谱填料组合物，其包含：基本上由至少在其可用表面上具有阳离子交换位点的颗粒组成的颗粒，所述颗粒直径在约1至约75微米之间; 以及液体涂层，其基本上由亲水的，水溶性的成膜树脂组成，其具有阴离子交换位点，其吸引基材的可用的阳离子交换位点，其中液体涂层由基材颗粒的可用表面上的静电键保持 。 本发明还包括色谱柱和使用所述包装组合物的方法。
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4.发明授权
公开(公告)号：US4048288A
公开(公告)日：1977-09-13
申请号：US558403
申请日：1975-03-14
CPC分类号： C01D3/26 , Y02P20/149
摘要： By providing about 1 percent of an extremely finely divided powder, e.g. less than about 60 microns, disposed throughout a body of sodium chloride particles, the salt particles can be heated without caking to temperatures higher than otherwise obtainable without experiencing caking. Suitable powders include those binary oxides, carbonates, sulfates, phosphates and hydroxides of Group II and Group IV elements, which are solids within the temperature range to be encountered.
摘要翻译： 通过提供约1％的极细粉末，例如 小于约60微米，设置在整个氯化钠颗粒体内，盐颗粒可以被加热而不会结块到高于其他可获得的温度，而不会经历结块。 合适的粉末包括II族和IV族元素的二元氧化物，碳酸盐，硫酸盐，磷酸盐和氢氧化物，它们是在遇到的温度范围内的固体。
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5.发明授权Size separation of particles contained within a material by the use of nonaqueous hydrodynamic chromatography 失效通过使用非水性流体动力学色谱法在材料中包含的颗粒的尺寸分离
公开(公告)号：US5372721A
公开(公告)日：1994-12-13
申请号：US139324
申请日：1993-10-19
CPC分类号： G01N30/0005 , G01N15/02 , G01N2030/001 , G01N2030/885
摘要： A method is disclosed for determining the distribution according to size of particles which make up a noncontinuous phase dispersed within a matrix which is not completely soluble in an aqueous solution. The method involves dissolving the matrix containing the particles in an essentially nonaqueous liquid causing the particles to be suspended. The suspension is then eluted through a separating medium which sorts the particles according to size. A detector monitors the effluent from the separating medium and creates a record of the data. This record is then compared to data obtained from known standards in order to estimate the size distribution in the sample.
摘要翻译： 公开了一种根据构成分散在不完全溶于水溶液的基体内的非连续相的颗粒尺寸来确定分布的方法。 该方法包括将含有颗粒的基质溶解在基本上非水性的液体中，导致颗粒被悬浮。 然后将悬浮液通过分离介质洗脱，根据尺寸对颗粒进行排序。 检测器监测来自分离介质的流出物，并创建数据记录。 然后将该记录与从已知标准获得的数据进行比较，以估计样品中的尺寸分布。
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公开(公告)号：US4532043A
公开(公告)日：1985-07-30
申请号：US523818
申请日：1983-08-15
CPC分类号： G01N30/74 , G01N2030/001 , G01N2030/027 , G01N2030/625 , G01N30/38 , G01N33/44
摘要： The molecular weight and molecular weight distribution of diverse ultra-high molecular weight water soluble polymers is rapidly determined based on apparent size by passage of extremely dilute samples of the polymer (1-250 ppm) through a column of nonporous packing whereby separation into molecular weight (apparent size) fractions is obtained predominantly based on flow (i.e., hydrodynamic chromatography). Detection of the extremely dilute sample polymer is accomplished, e.g., by tagging the polymer with a fluorescent agent and using a flow-through fluorometer detector. The molecular weight characterization of the polymers is determined independent or less dependent of the composition of the polymer by analyzing the sample in its nonionized form.
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公开(公告)号：US4854700A
公开(公告)日：1989-08-08
申请号：US207699
申请日：1988-06-15
CPC分类号： G01N30/74 , G01N30/6047
摘要： A column holder for on-column photometric detection capillary liquid chromatography incorporating a body and a pair of straight edges attached to the body. The straight edges can be conveniently made from a razor blade. The body has two passageways through it that are transverse and intersecting. The first passageway is dimensioned so that a capillary column can be slipped into it or removed from it by hand. The other passageway is for the passage of a light beam from a liquid chromatography photometric detector. The straight edges are slightly separated to form an optical slit in front of the capillary column and are securely clamped to the body of the column holder. A capillary column can be removed from the column holder and be replaced with another capillary column without damaging it and without the necessity of repositioning the slit.
摘要翻译： 用于柱内光度检测毛细管液相色谱柱的柱保持器，其包含主体和附接到身体的一对直边。 直边可以方便地用剃刀刀片制成。 身体有两条通过它的横向和相交的通道。 第一个通道的尺寸设计使得毛细管柱可以滑入其中或用手从其中移除。 另一个通道用于通过来自液相色谱测光检测器的光束。 直边缘稍微分开，在毛细管柱前面形成一个光学狭缝，并牢固地夹在柱保持器的主体上。 毛细管柱可以从柱保持器中取出，并用另一个毛细管柱替换，而不会损坏毛细管柱，无需重新定位狭缝。
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8.发明授权
公开(公告)号：US4038188A
公开(公告)日：1977-07-26
申请号：US558402
申请日：1975-03-14
摘要： A body of particles of sodium chloride (1) initially containing sodium sulfate and/or sodium carbonate, and/or (2) exposed to compounds capable of reacting in situ with the sodium chloride and/or with each other to form sodium sulfate and/or sodium carbonate, is maintained free from caking at temperatures within the range of from about 610.degree. C to at least about 700.degree. C by maintaining such a body substantially free from sodium sulfate and/or sodium carbonate. One or more compounds, at least one of which contains calcium ion, are provided in the system to react with any sodium sulfate and sodium carbonate present in the system initially, and with any compounds in the system which would otherwise react to form sodium sulfate and/or sodium carbonate. One aspect of this invention enables the operation of a fluidized bed reactor at more efficient operating temperatures than previously attainable in the incineration of organic matter contained in an aqueous sodium chloride brine over a bed of sodium chloride fluidized by gases from the combustion of sulfur-containing fossil fuels and fuel oils.
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9.发明授权Size separation of particles contained within a material by the use of nonaqueous hydrodynamic chromatography 失效通过使用非水性流体动力学色谱法在材料中包含的颗粒的尺寸分离
公开(公告)号：US5183604A
公开(公告)日：1993-02-02
申请号：US825353
申请日：1992-01-24
CPC分类号： G01N30/0005 , G01N15/02 , G01N2030/001 , G01N2030/885
摘要： A method is disclosed for determining the distribution according to size of particles which make up a noncontinuous phase dispersed within a matrix which is not completely soluble in an aqueous solution. The method involves dissolving the matrix containing the particles in an essentially nonaqueous liquid causing the particles to be suspended. The suspension is then eluted through a separating medium which sorts the particles according to size. A detector monitors the effluent from the separating medium and creates a record of the data. This record is then compared to data obtained from known standards in order to estimate the size distribution in the sample.
摘要翻译： 公开了一种根据构成分散在不完全溶于水溶液的基体内的非连续相的颗粒尺寸来确定分布的方法。 该方法包括将含有颗粒的基质溶解在基本上非水性的液体中，导致颗粒被悬浮。 然后将悬浮液通过分离介质洗脱，根据尺寸对颗粒进行排序。 检测器监测来自分离介质的流出物，并创建数据记录。 然后将该记录与从已知标准获得的数据进行比较，以估计样品中的尺寸分布。
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公开(公告)号：US4113471A
公开(公告)日：1978-09-12
申请号：US746981
申请日：1976-12-02
CPC分类号： C22B3/10 , C22B11/04 , Y02P10/234
摘要： A process for extracting non-ferrous metal values from an oxide ore. The process comprises leaching the ore with a solution containing at least one alkali metal chloride or alkaline earth chloride salt in the presence of an oxygen-containing gas at a temperature and pressure sufficient to solubilize the non-ferrous metal values into the solution of the metal chloride salt.
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