Zero thermal expansion, low heat transfer, variable temperature sample assembly for probe microscopy
    2.
    发明授权
    Zero thermal expansion, low heat transfer, variable temperature sample assembly for probe microscopy 有权
    零热膨胀,低热传递,可变温度样品组件用于探针显微镜

    公开(公告)号:US08763161B2

    公开(公告)日:2014-06-24

    申请号:US13622623

    申请日:2012-09-19

    CPC classification number: G01Q30/10 Y10S977/871

    Abstract: A variable temperature assembly for scanning probe microscopy (SPM) is described which minimizes or eliminates motion of the sample caused by the thermal expansion or contraction of the sample holder assembly and platform/scanning stage on which the assembly is mounted, and minimizes heating or cooling of the platform/stage. In heater form, the variable temperature assembly includes a thin boron nitride puck with one or more high-resistivity wires embedded along an underside of the puck. The puck is suspended from its polished top surface by posts that are secured to the microscope stage. All thermal expansion of the puck occurs in the downward direction, away from the SPM probe-sample interface, thus eliminating relative motion between the probe tip and sample surface. The top surface of the puck remains stationary as a result of the unique geometry of the posts and the puck-post attachment configuration described herein.

    Abstract translation: 描述了用于扫描探针显微镜(SPM)的可变温度组件,其最小化或消除了由安装组件的样品架组件和平台/扫描台的热膨胀或收缩引起的样品的运动,并使加热或冷却最小化 的平台/舞台。 在加热器形式中,可变温度组件包括具有沿着盘的下侧嵌入的一个或多个高电阻率线的薄氮化硼圆盘。 圆盘通过固定在显微镜台上的柱子从其抛光的顶部表面悬挂下来。 圆盘的所有热膨胀发生在向下的方向上,远离SPM探针 - 样品界面,从而消除了探针尖端和样品表面之间的相对运动。 由于柱的独特几何结构和本文所述的固定柱附件结构,圆盘的顶部表面保持静止。

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