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    Rheology modification of polymers prepared using metallocenes
    3.
    发明授权
    Rheology modification of polymers prepared using metallocenes 有权
    使用金属茂制备的聚合物的流变改性

    公开(公告)号：US06528136B1

    公开(公告)日：2003-03-04

    申请号：US09140603

    申请日：1998-08-26

    申请人： Thoi H. Ho ,  Wendy D. Hoenig ,  Che-I Kao ,  Michael E. Rowland ,  Clark H. Cummins ,  Michael J. Mullins ,  H. Craig Silvis

    发明人： Thoi H. Ho ,  Wendy D. Hoenig ,  Che-I Kao ,  Michael E. Rowland ,  Clark H. Cummins ,  Michael J. Mullins ,  H. Craig Silvis

    IPC分类号： B29D2200

    CPC分类号： C08L23/02 ,  C08G81/02 ,  C08K5/43 ,  C08L23/04 ,  C08L23/06 ,  C08L23/08 ,  C08L23/0815 ,  C08L23/0838 ,  C08L23/0853 ,  C08L23/16 ,  C08L2205/22 ,  C08L2312/00 ,  C08L2314/06 ,  Y10T428/1334 ,  Y10T428/1352 ,  Y10T428/1386 ,  Y10T428/139 ,  Y10T428/31913 ,  Y10T428/31917 ,  C08L2666/04

    摘要： The invention includes a process of preparing a coupled polymer comprising heating an admixture containing (1) at least one polyolefin comprising ethylene and optionally at least one comonomer which is selected from alpha olefins having at least 3 carbon atoms, dienes and combinations thereof said polyolefin having a molecular weight distribution of less than or equal to about 3 and (2) a coupling amount at least one poly(sulfonyl azide) to at least the decomposition temperature of the poly(sulfonyl azide) for a period sufficient for decomposition of at least about 80 weight percent of the poly(sulfonyl azide) and sufficient to result in a coupled polymer; particularly where the polyolefin is the product of polymerization of ethylene and optionally at least one other alpha-olefin in the presence of a single site catalyst (transition metal like Va or Cr, metallocene or constrained geometry). The amount of poly(sulfonyl azide) is preferably from about 0.01 to about 5 weight percent of the polyolefin. The poly(sulfonyl azide)and polyolefin preferably react at a temperature at least the decomposition temperature and greater than about 150° C. The invention also includes any composition made by the process of the invention and any article made from the composition as well as processes for making the articles, particularly melt processing (especially where the article is formed from a melt of a composition of the invention), more preferably selected by molding, blow molding or extrusion blow molding the composition. The invention also includes the use of a composition of the invention in any of these processes.

    摘要翻译： 本发明包括一种制备偶联聚合物的方法，包括加热含有（1）至少一种包含乙烯和任选至少一种选自具有至少3个碳原子的α-烯烃的共聚单体的聚烯烃，二烯及其组合的混合物的混合物，所述聚烯烃具有 小于或等于约3的分子量分布和（2）偶联量至少一种聚（磺酰基叠氮化物）至少达到聚（磺酰基叠氮化物）的分解温度足够分解至少约 80重量％的聚（磺酰基叠氮化物）并且足以产生偶联的聚合物; 特别是当聚烯烃是在单中心催化剂（过渡金属如Va或Cr，金属茂或约束几何形式）存在下乙烯和任选的至少一种其它α-烯烃聚合的产物时。 聚（磺酰基叠氮化物）的量优选为聚烯烃的约0.01至约5重量％。 聚（磺酰基叠氮化物）和聚烯烃优选在至少分解温度和大于约150℃的温度下进行反应。本发明还包括通过本发明的方法制备的任何组合物和由组合物制成的任何制品以及工艺 用于制造制品，特别是熔融加工（特别是在由本发明的组合物的熔体形成制品的情况下），更优选通过模制，吹塑或挤出吹塑该组合物来选择。 本发明还包括在任何这些方法中使用本发明的组合物。

    Finishing design to increase the polymer content in an olefin solution polymerization process
    4.
    发明授权
    Finishing design to increase the polymer content in an olefin solution polymerization process 有权
    精加工设计，以提高烯烃溶液聚合过程中的聚合物含量

    公开(公告)号：US06420516B1

    公开(公告)日：2002-07-16

    申请号：US09555915

    申请日：2000-06-06

    申请人： Li-Min Tau ,  Robert O. Swindoll ,  Che-I Kao ,  Pradeep Jain

    发明人： Li-Min Tau ,  Robert O. Swindoll ,  Che-I Kao ,  Pradeep Jain

    IPC分类号： C08F610

    CPC分类号： C08F6/003 ,  B01J2219/1942 ,  C08F6/10 ,  C08L23/00

    摘要： The polymer recovery capacity of solution polymerization units is increased by flashing a polymer solution exiting olefin polymerization reactors to produce a concentrated polymer solution having a reduced temperate and a solids content from 10 percent to 40 percent by weight. Flashing of the polymer solution preferably occurs at a temperature at least 20° C. higher than the crystallization temperature of the concentrated polymer solution The concentrated polymer solution can be prepared adiabatically and can be subsequently finished in conventional polymer recovery units without increasing the risk of gel formation.

    摘要翻译： 通过闪烁离开烯烃聚合反应器的聚合物溶液来提高溶液聚合单元的聚合物回收能力，以产生具有降低的温度和10至40重量％的固体含量的浓缩聚合物溶液。 聚合物溶液的闪烁优选在比浓缩的聚合物溶液的结晶温度高至少20℃的温度下发生。聚合的聚合物溶液可以绝热制备，随后在常规聚合物回收装置中完成，而不增加凝胶的风险 形成。

    Process of rheology modification of polymers
    6.
    发明授权
    Process of rheology modification of polymers 有权
    聚合物流变改性工艺

    公开(公告)号：US06552129B2

    公开(公告)日：2003-04-22

    申请号：US10013152

    申请日：2001-12-10

    申请人： David A. Babb ,  Che-I Kao ,  Wendy D. Hoenig ,  Michael E. Rowland ,  Clark H. Cummins ,  H. Craig Silvis ,  Michael J. Mullins ,  Thoi H. Ho

    发明人： David A. Babb ,  Che-I Kao ,  Wendy D. Hoenig ,  Michael E. Rowland ,  Clark H. Cummins ,  H. Craig Silvis ,  Michael J. Mullins ,  Thoi H. Ho

    IPC分类号： C08F800

    CPC分类号： C08L23/02 ,  C08G81/02 ,  C08K5/43 ,  C08L23/04 ,  C08L23/06 ,  C08L23/08 ,  C08L23/0815 ,  C08L23/0838 ,  C08L23/0853 ,  C08L23/16 ,  C08L2205/22 ,  C08L2312/00 ,  C08L2314/06 ,  Y10T428/1334 ,  Y10T428/1352 ,  Y10T428/1386 ,  Y10T428/139 ,  Y10T428/31913 ,  Y10T428/31917 ,  C08L2666/04

    摘要： The invention includes a process of reacting a poly(sulfonyl azide) with a polymer comprising steps (a) forming a first admixture of a first amount of a first polymer or in a liquid which does not require removal from the polymer and a poly(sulfonyl azide); (b) then forming a second admixture of the first admixture with a second amount of at least one second polymer; and (c) heating the second admixture at least to the decomposition temperature of the coupling agent for a time sufficient to result in coupling of polymer chains. The invention further includes all compositions obtainable by processes of the invention as well as blends of those compositions with one or more polymers of compositions different from the first or second polymer or the product of a process of the invention. Additionally the invention includes articles made from compositions of the invention, and shaping those articles particularly by processes which comprise shaping the compositions in a melted state into an article, more preferably when the process comprises thermoforming, injection molding, extrusion, casting, blow molding, foaming or blowing as well as the use of the compositions in those processes.

    摘要翻译： 本发明包括使聚（磺酰基叠氮化物）与聚合物反应的方法，包括步骤（a）形成第一量的第一聚合物的第一混合物或不需要从聚合物中除去的液体和聚（磺酰基 叠氮化物）; （b）然后形成第一混合物与第二量的至少一种第二聚合物的第二混合物; 和（c）至少加热第二混合物至偶联剂的分解温度足以导致聚合物链偶联的时间。 本发明还包括可通过本发明的方法获得的所有组合物以及这些组合物与一种或多种不同于第一或第二聚合物或本发明方法的产物的组合物的一种或多种聚合物的共混物。 另外，本发明包括由本发明的组合物制成的制品，特别是通过包括将熔融状态的组合物成型成制品的方法成型，更优选当该方法包括热成型，注射成型，挤出，铸造，吹塑成型， 发泡或吹塑以及在这些方法中使用组合物。

    Hybrid Electret
    8.
    发明申请
    Hybrid Electret 审中-公开
    混合驻极体

    公开(公告)号：US20110095626A1

    公开(公告)日：2011-04-28

    申请号：US12908046

    申请日：2010-10-20

    申请人： Hsi-Hsin SHIH ,  Che-I Kao ,  Chien-Tsung Wu ,  Po-Tsun Chen

    发明人： Hsi-Hsin SHIH ,  Che-I Kao ,  Chien-Tsung Wu ,  Po-Tsun Chen

    IPC分类号： B32B27/00

    CPC分类号： H01G7/028 ,  H01G7/021

    摘要： This invention discloses a hybrid electret. The hybrid electret comprises at least a first dielectric layer and at least a second dielectric layer, and the first dielectric layer and the second layer are alternatively stacked. The first dielectric layer comprises at least a polymer and the second dielectric layer comprises at least a polymer, and the polymer of the first dielectric layer differs from the polymer of the second dielectric layer.

    摘要翻译： 本发明公开了一种混合驻极体。 混合驻极体至少包括第一电介质层和至少第二电介质层，并且第一电介质层和第二层交替堆叠。 第一电介质层至少包含聚合物，第二电介质层至少包含聚合物，第一电介质层的聚合物与第二电介质层的聚合物不同。

    Process of rheology modification of polymers
    9.
    发明授权
    Process of rheology modification of polymers 有权
    聚合物流变改性工艺

    公开(公告)号：US06359073B1

    公开(公告)日：2002-03-19

    申请号：US09694649

    申请日：2000-10-23

    申请人： David A. Babb ,  Che-I Kao ,  Wendy D. Hoenig ,  Michael E. Rowland ,  Clark H. Cummins ,  H. Craig Silvis ,  Michael J. Mullins ,  Thoi H. Ho

    发明人： David A. Babb ,  Che-I Kao ,  Wendy D. Hoenig ,  Michael E. Rowland ,  Clark H. Cummins ,  H. Craig Silvis ,  Michael J. Mullins ,  Thoi H. Ho

    IPC分类号： C08F800

    CPC分类号： C08L23/02 ,  C08G81/02 ,  C08K5/43 ,  C08L23/04 ,  C08L23/06 ,  C08L23/08 ,  C08L23/0815 ,  C08L23/0838 ,  C08L23/0853 ,  C08L23/16 ,  C08L2205/22 ,  C08L2312/00 ,  C08L2314/06 ,  Y10T428/1334 ,  Y10T428/1352 ,  Y10T428/1386 ,  Y10T428/139 ,  Y10T428/31913 ,  Y10T428/31917 ,  C08L2666/04

    摘要： The invention includes a process of reacting a poly(sulfonyl azide) with a polymer comprising steps (a) forming a first admixture of a first amount of a first polymer or in a liquid which does not require removal from the polymer and a poly(sulfonyl azide); (b) then forming a second admixture of the first admixture with a second amount of at least one second polymer; and (c) heating the second admixture at lest to the decomposition temperature of the coupling agent for a time sufficient to result in coupling of polymer chains. The invention further includes all compositions obtainable by processes of the invention as well as blends of those compositions with one or more polymers of compositions different from the first or second polymer or the product of a process of the invention. Additionally the invention includes articles made from compositions of the invention, and shaping those articles particularly by processes which comprise shaping the compositions in a melted state into an article, more preferably when the process comprises thermoforming, injection molding, extrusion, casting, blow molding, foaming or blowing as well as the use of the compositions in those processes.

    摘要翻译： 本发明包括使聚（磺酰基叠氮化物）与聚合物反应的方法，包括步骤（a）形成第一量的第一聚合物的第一混合物或不需要从聚合物中除去的液体和聚（磺酰基 叠氮化物）; （b）然后形成第一混合物与第二量的至少一种第二聚合物的第二混合物; 和（c）加热第二混合物至少达到偶联剂的分解温度足以导致聚合物链偶联的时间。 本发明还包括可通过本发明的方法获得的所有组合物以及这些组合物与一种或多种不同于第一或第二聚合物或本发明方法的产物的组合物的一种或多种聚合物的共混物。 另外，本发明包括由本发明的组合物制成的制品，并且特别通过包括将熔融状态的组合物成型成制品的方法成型那些制品，更优选当该方法包括热成型，注射成型，挤出，浇铸，吹塑成型， 发泡或吹塑以及在这些方法中使用组合物。

    Production of alkali metal phenates
    10.
    发明授权
    Production of alkali metal phenates 失效
    生产碱金属酚盐

    公开(公告)号：US4272635A

    公开(公告)日：1981-06-09

    申请号：US60945

    申请日：1979-07-26

    申请人： Sanford A. Siegel ,  Masao Yoshimine ,  Che-I Kao

    发明人： Sanford A. Siegel ,  Masao Yoshimine ,  Che-I Kao

    IPC分类号： C07C37/66 ,  C07C37/70 ,  C07C39/44 ,  C07C39/24 ,  C07C39/36

    CPC分类号： C07C37/66 ,  C07C37/70

    摘要： A molten substituted phenol and an aqueous caustic solution are reacted at temperatures from 170.degree. C. to 190.degree. C. under superatmospheric pressure to form an aqueous solution of an alkali metal phenate. By employing a rapid drying process such as flashing the water vapor from the reactor to cool the mixture, alkali metal phenate solids are produced with low levels of toxic by-products.

    摘要翻译： 熔融取代的苯酚和苛性碱水溶液在超大气压下在170℃至190℃的温度下反应，形成碱金属酚盐的水溶液。 通过采用快速干燥方法，例如将来自反应器的水蒸气闪蒸以冷却混合物，产生具有低水平的有毒副产物的碱金属酚盐固体。