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公开(公告)号：US20130035406A1
公开(公告)日：2013-02-07
申请号：US13197342
申请日：2011-08-03
IPC分类号： C07C27/06
CPC分类号： C07C41/09 , C07C43/043 , Y02P20/132
摘要： This invention discloses a method for making a dimethylether (DME) product from a synthesis gas (syngas) in the presence of a catalyst in a fluid pluralized bed reactor operating in the gas phase. The reactions generate a significant amount of heat and the heat management is balanced between supplying quench recycle syngas to the pluralized sections along the reactor and also by controlling the preheat temperature of the reactant streams. Gas phase fluidization of the catalyst is controlled so that the pluralized reactive zones are maintained in a backmix configuration.
摘要翻译： 本发明公开了一种在气相中操作的流体多元床反应器中在催化剂存在下由合成气（合成气）制备二甲醚（DME）产物的方法。 反应产生大量的热量，并且在沿着反应器的多个部分供应骤冷循环合成气之间以及通过控制反应物流的预热温度来平衡热管理。 控制催化剂的气相流化，使得多个反应区域保持在回混构造。
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公开(公告)号：US08791165B2
公开(公告)日：2014-07-29
申请号：US13197342
申请日：2011-08-03
CPC分类号： C07C41/09 , C07C43/043 , Y02P20/132
摘要： This invention discloses a method for making a dimethylether (DME) product from a synthesis gas (syngas) in the presence of a catalyst in a fluid pluralized bed reactor operating in the gas phase. The reactions generate a significant amount of heat and the heat management is balanced between supplying quench recycle syngas to the pluralized sections along the reactor and also by controlling the preheat temperature of the reactant streams. Gas phase fluidization of the catalyst is controlled so that the pluralized reactive zones are maintained in a backmix configuration.
摘要翻译： 本发明公开了一种在气相中操作的流体多元床反应器中在催化剂存在下由合成气（合成气）制备二甲醚（DME）产物的方法。 反应产生大量的热量，并且在沿着反应器的多个部分供应骤冷循环合成气之间以及通过控制反应物流的预热温度来平衡热管理。 控制催化剂的气相流化，使得多个反应区域保持在回混构造。
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公开(公告)号：US20140364654A1
公开(公告)日：2014-12-11
申请号：US13913821
申请日：2013-06-10
申请人： SARABJIT S. RANDHAVA , Richard L. Kao , Todd L. Harvey , Bradley S. Novak , Jorge Romero Zabaleta
发明人： SARABJIT S. RANDHAVA , Richard L. Kao , Todd L. Harvey , Bradley S. Novak , Jorge Romero Zabaleta
IPC分类号： C07C41/09
CPC分类号： C07C41/09 , C01B3/384 , C01B2203/0233 , C01B2203/0405 , C01B2203/061 , C01B2203/0822 , C01B2203/0827 , C01B2203/0894 , C01B2203/1241 , C07C29/1518 , Y02P20/127 , Y02P20/128 , C07C31/04 , C07C43/043
摘要： Disclosed herein is a process for monetization of natural gas by producing fuel grade dimethyl ether (DME). The process includes three reactive stages with the first reactive stage being the conversion of natural gas into syngas, the second reactive stage being the conversion of syngas into crude methanol and the third reactive stage being the production of fuel grade dimethyl ether. The management and optimization of the water and steam circuits is important to maintain net overall system efficiency and mitigation of any liquid effluents.
摘要翻译： 本文公开了通过生产燃料级二甲醚（DME）来获得天然气货币化的方法。 该方法包括三个反应阶段，第一个反应阶段是将天然气转化为合成气，第二个反应阶段是将合成气转化为粗甲醇，第三个反应阶段是生产燃料级二甲醚。 水和蒸汽回路的管理和优化对于保持净整体系统效率和减轻任何液体流出物都很重要。
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公开(公告)号：US08546454B2
公开(公告)日：2013-10-01
申请号：US13190678
申请日：2011-07-26
IPC分类号： C07C27/00
CPC分类号： C07C41/01 , C01B3/382 , C01B3/48 , C01B2203/0233 , C01B2203/0244 , C01B2203/0283 , C01B2203/0415 , C01B2203/043 , C01B2203/0475 , C01B2203/0485 , C01B2203/0495 , C01B2203/06 , C01B2203/0894 , C01B2203/1258 , C01B2203/142 , C01B2203/147 , C10J3/463 , C10J2300/0916 , C10J2300/0993 , C10J2300/1656 , C10K1/003 , C10K3/006 , Y02P20/132 , Y02P20/145 , C07C43/043
摘要： Disclosed herein is a process for the production of fuel grade DME from carbonaceous fuels, including a pressurized multi-stage progressively expanding fluidized bed gasifier and an oxyblown autothermal reformer to produce a synthesis gas (syngas) with desirable hydrogen to carbon monoxide molar ratio, which then undergoes gas-phase DME one-step direct synthesis in a fluid pluralized bed reactor over an attrition resistant bifunctional catalyst. The crude DME thus obtained is purified in a two column distillation unit to produce a fuel grade DME having a purity greater than 99.98 mole %.
摘要翻译： 本文公开了一种用于从含碳燃料生产燃料级DME的方法，包括加压多级逐步膨胀的流化床气化器和氧气自热重整器，以产生具有所需氢气与一氧化碳摩尔比的合成气（合成气），其中 然后在耐磨损双功能催化剂上在流体多元床反应器中进行气相DME一步直接合成。 由此获得的粗DME在双塔蒸馏装置中纯化以产生纯度大于99.98摩尔％的燃料级DME。
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公开(公告)号：US20130030063A1
公开(公告)日：2013-01-31
申请号：US13190678
申请日：2011-07-26
IPC分类号： C07C27/06
CPC分类号： C07C41/01 , C01B3/382 , C01B3/48 , C01B2203/0233 , C01B2203/0244 , C01B2203/0283 , C01B2203/0415 , C01B2203/043 , C01B2203/0475 , C01B2203/0485 , C01B2203/0495 , C01B2203/06 , C01B2203/0894 , C01B2203/1258 , C01B2203/142 , C01B2203/147 , C10J3/463 , C10J2300/0916 , C10J2300/0993 , C10J2300/1656 , C10K1/003 , C10K3/006 , Y02P20/132 , Y02P20/145 , C07C43/043
摘要： Disclosed herein is a process for the production of fuel grade DME from carbonaceous fuels, including a pressurized multi-stage progressively expanding fluidized bed gasifier and an oxyblown autothermal reformer to produce a synthesis gas (syngas) with desirable hydrogen to carbon monoxide molar ratio, which then undergoes gas-phase DME one-step direct synthesis in a fluid pluralized bed reactor over an attrition resistant bifunctional catalyst. The crude DME thus obtained is purified in a two column distillation unit to produce a fuel grade DME having a purity greater than 99.98 mole %.
摘要翻译： 本文公开了一种用于从含碳燃料生产燃料级DME的方法，包括加压多级逐步膨胀的流化床气化器和氧气自热重整器，以产生具有所需氢气与一氧化碳摩尔比的合成气（合成气），其中 然后在耐磨损双功能催化剂上在流体多元床反应器中进行气相DME一步直接合成。 由此获得的粗DME在双塔蒸馏装置中纯化以产生纯度大于99.98摩尔％的燃料级DME。
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