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公开(公告)号：US11499947B2
公开(公告)日：2022-11-15
申请号：US16470392
申请日：2018-02-22
Applicant: SHIMADZU CORPORATION
Inventor： Isao Sawamura , Akira Aono
Abstract: A sample introduction device 10 includes a tube holding section 21 and a sample removing mechanism 40. The sample removing mechanism 40 removes a sample 6 in a sample tube 2 held by the tube holding section 21. Thus, in the sample introduction device 10, the sample 6 in the sample tube 2 held by the tube holding section 21 can be automatically removed. As a result, the operator no longer needs to perform an operation of taking out the sample 6 from the sample tube 2. Thus, a work load on the operator can be reduced.
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公开(公告)号：US10852218B2
公开(公告)日：2020-12-01
申请号：US15778355
申请日：2015-12-15
Applicant: SHIMADZU CORPORATION
Inventor： Akira Aono , Isao Sawamura
Abstract: A sample introduction device includes a tube holding unit 10, a tube heating unit 20, and a movement mechanism 30. The tube holding unit 10 holds a sample tube 1. The tube heating unit 20 comes into contact with the sample tube 1 held in the tube holding unit 10 and heats the sample tube 1 to desorb sample components in the sample tube 1. The tube holding unit 10 and the tube heating unit 20 are attached to the movement mechanism 30 so as to be able to move separately. The movement mechanism 30 includes a nut 32 which can be attached to and detached from the tube holding unit 10 and the tube heating unit 20, and a support shaft 31 which supports the nut 32 such that the nut 32 can move.
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公开(公告)号：US10712246B2
公开(公告)日：2020-07-14
申请号：US15143702
申请日：2016-05-02
Applicant: SHIMADZU CORPORATION
Inventor： Akira Aono
Abstract: A carrier gas flow path of at least from a trap to an analyzing portion is shared between a state wherein a sample component is trapped within the trap and a state wherein the sample component is not trapped within the trap. In this case, even after the sample has been introduced into the analyzing portion through the carrier gas flow path, there is a time interval over which the carrier gas flows within the carrier gas flow path. This makes it possible, through the carrier gas that flows within the carrier gas flow path afterward, to remove the sample component from within the flow path, despite there being a sample component within the carrier gas flow path at the time of sample introduction, thus making it possible to prevent the sample component from remaining within the flow path after sample introduction.
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公开(公告)号：US10119926B2
公开(公告)日：2018-11-06
申请号：US15032348
申请日：2013-12-02
Applicant: SHIMADZU CORPORATION
Inventor： Akira Aono
Abstract: A heat retention start timing of each sample container is determined based on a room temperature detected by a room temperature sensor, and a starting temperature and an ending temperature of each sample at a time of programmed temperature analysis that are stored in an analysis condition storage section. Since cooling speed of each sample container varies depending on the room temperature, the cooling time (A12, B12, C12, . . . ) of each sample container may be predicted based on the ending temperature of each sample at the time of programmed temperature analysis, the starting temperature of a next sample at the time of the programmed temperature analysis, and the room temperature. By determining the heat retention start timing of each sample container according to the cooling time (A12, B12, C12, . . . ) of each sample container predicted in the above manner, a margin time (A13, B13, C13, . . . ) after the cooling time may be prevented from becoming unnecessarily long. Accordingly, the processing performance may be improved compared to a conventional configuration where the heat retention start timings of sample containers are shifted by fixed time intervals.
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公开(公告)号：US09588088B2
公开(公告)日：2017-03-07
申请号：US13966765
申请日：2013-08-14
Applicant: SHIMADZU CORPORATION
Inventor： Akira Aono
CPC classification number: G01N30/20 , G01N1/2214 , G01N2030/025 , G01N2030/085 , G01N2030/207
Abstract: In a gas sample analysis device including a metering tube, sample gas supply channel, carrier gas supply channel, evacuation channel and collection tube, there is provided a first channel switching valve which switches between a load state in which the metering tube is interposed between said sample gas supply channel and the evacuation channel and an injection state in which the metering tube is interposed between the sample gas supply channel and gas analysis device; and a second channel switching valve which, in the load state or injection state, switches between a collection tube interposition state in which the collection tube is interposed between the sample gas supply channel and the metering tube or between the metering tube and the gas analysis device, and a collection tube shunt state in which the collection tube is not interposed.
Abstract translation: 在包括计量管，样品气体供给通道，载气供给通道，排气通道和收集管的气体样品分析装置中，设置有第一通道切换阀，其在计量管介于所述 样品气体供给通道和排气通道以及计量管插入在样品气体供给通道和气体分析装置之间的注入状态; 以及第二通道切换阀，所述第二流路切换阀在所述负荷状态或注入状态下，在收集管插入状态之间切换，在所述收集管插入状态中，所述收集管插入在所述样品气体供给流路和所述计量管之间，或者在所述计量管与所述气体分析装置 ，收集管未插入收集管分流状态。
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Patent Agency Ranking
公开(公告)号：US20140326045A1
公开(公告)日：2014-11-06
申请号：US14358744
申请日：2012-11-16
Applicant: Shimadzu Corporation , GL Sciences Incorporation
Inventor： Shinji Fukumoto , Hiroshi Yamauchi , Akira Aono , Manabu Shimomura , Yoshiyuki Takei , Tadashi Mimura , Akira Suzuki , Masahiro Furuno
CPC classification number: G01N30/06 , B01D3/346 , G01N1/14 , G01N1/24 , G01N30/7206 , G01N2001/4066 , G01N2030/025 , G01N2030/065
Abstract: The present invention provides a method and apparatus for rapidly extracting the analyte existing in the liquid phase in analyzing an analyse “having a large partition coefficient in gas-liquid equilibrium”, “having a high water solubility”, or “having a low olfactory threshold” by a gas-liquid contact extraction method, and further provides, a method and apparatus for unmanned continuous sample introduction of the analyte to a GC or the like for a long time. In the present invention, using a gas-liquid contact extractor to which a sample liquid is continuously introduced from above and a purge gas from beneath, the analyte in the sample liquid is extracted by gas-liquid contact between the sample liquid and the purge gas. A discharge pipe is connected to the bottom of the gas-liquid contact extractor, the pipe having a liquid sump through which the sample liquid is discharged, while blocking the outflow of the purge gas from the liquid sump.
Abstract translation: 本发明提供一种方法和装置，用于在分析“气 - 液平衡中的分配系数大”，“具有高水溶性”或“低嗅觉阈值”的分析中快速提取存在于液相中的分析物 “，并且还提供了用于将分析物无间连续样品长时间引入GC等的方法和装置。 在本发明中，使用从上方连续引入样品液体的气液接触提取器和来自下方的吹扫气体，通过样品液体和吹扫气体之间的气液接触来提取样品液体中的分析物 。 排气管连接到气 - 液接触提取器的底部，管具有液体槽，样品液通过该液槽排出，同时阻止吹扫气体从液槽中流出。
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公开(公告)号：US12222336B2
公开(公告)日：2025-02-11
申请号：US17641679
申请日：2020-11-18
Applicant: SHIMADZU CORPORATION
Inventor： Akira Aono , Shota Hata , Naru Maruoka , Hideki Sato
Abstract: A switching mechanism 110 can perform switching to a pressurized state in which gas is supplied from a pipe 203 to an insertion tube 101, or a derivation state in which gas in a head space 23 that is pressurized is derived from the insertion tube 101 to the pipe 207 via a collection unit 104. The switching mechanism 110 includes a discharge valve 103 that puts the insertion tube 101 and the pipe 207 into a non-communication state in the pressurized state and puts the insertion tube 101 and the pipe 207 into a communication state in the derivation state. A resistance pipe 206 supplies gas to a channel between the collection unit 104 and the discharge valve 103 in the derivation state.
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公开(公告)号：US10955389B2
公开(公告)日：2021-03-23
申请号：US16077068
申请日：2016-03-07
Applicant: SHIMADZU CORPORATION
Inventor： Akira Aono , Isao Sawamura
Abstract: A sample introduction device 100 includes a heating unit 102, an ultraviolet irradiation unit 103, and a sample supply part 106. The heating unit 102 vaporizes a sample 22 by heating externally a container 2 in which the sample 22 is enclosed. The ultraviolet irradiation unit 103 causes ultraviolet rays to pass through the container 2 and irradiates the sample 22 with the ultraviolet rays. The sample supply part 106 supplies the sample vaporized in the container 2 to a gas chromatograph 1 side.
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公开(公告)号：US09347919B2
公开(公告)日：2016-05-24
申请号：US14358744
申请日：2012-11-16
Applicant: Shimadzu Corporation , GL Sciences Incorporation
Inventor： Shinji Fukumoto , Hiroshi Yamauchi , Akira Aono , Manabu Shimomura , Yoshiyuki Takei , Tadashi Mimura , Akira Suzuki , Masahiro Furuno
CPC classification number: G01N30/06 , B01D3/346 , G01N1/14 , G01N1/24 , G01N30/7206 , G01N2001/4066 , G01N2030/025 , G01N2030/065
Abstract: The present invention provides a method and apparatus for rapidly extracting the analyte existing in the liquid phase in analyzing an analyte “having a large partition coefficient in gas-liquid equilibrium”, “having a high water solubility”, or “having a low olfactory threshold” by a gas-liquid contact extraction method, and further provides, a method and apparatus for unmanned continuous sample introduction of the analyte to a GC or the like for a long time. In the present invention, using a gas-liquid contact extractor to which a sample liquid is continuously introduced from above and a purge gas from beneath, the analyte in the sample liquid is extracted by gas-liquid contact between the sample liquid and the purge gas. A discharge pipe is connected to the bottom of the gas-liquid contact extractor, the pipe having a liquid sump through which the sample liquid is discharged, while blocking the outflow of the purge gas from the liquid sump.
Abstract translation: 本发明提供一种方法和装置，用于在分析“气 - 液平衡分配系数大”，“具有高水溶性”或“具有低嗅觉阈值”的分析物中快速提取存在于液相中的分析物 “，并且还提供了用于将分析物无间连续样品长时间引入GC等的方法和装置。 在本发明中，使用从上方连续引入样品液体的气液接触提取器和来自下方的吹扫气体，通过样品液体和吹扫气体之间的气液接触来提取样品液体中的分析物 。 排气管连接到气 - 液接触提取器的底部，管具有液体槽，样品液通过该液槽排出，同时阻止吹扫气体从液槽中流出。
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公开(公告)号：US09274030B2
公开(公告)日：2016-03-01
申请号：US14169733
申请日：2014-01-31
Applicant: SHIMADZU CORPORATION
Inventor： Akira Aono
CPC classification number: G01N1/2202 , G01N30/12 , G01N2001/2282 , G01N2030/025 , G01N2030/128
Abstract: A sample introduction device having a channel configuration which allows recapture of samples and in which thorough purging is performed so that no sample components remain inside the channel. In the trap capture process, a first six-way switching valve is placed in state where ports a-f, b-c and d-e are connected, a second six-way switching valve is placed in state where ports a-b, c-d and e-f are connected, and an electromagnetic valve is opened. Carrier gas is introduced through a carrier gas channel, and is discharged via the first six-way valve-sample channel-second six-way switching valve-trap channel-second six-way switching valve-channel-first six-way valve-discharge channel. Carrier gas is also introduced through the path going through the electronic control flow controller, so the operation of stabilization of the analysis channel continues to be performed.
Abstract translation: 具有通道结构的样品引入装置，其允许重新捕获样品，并且进行彻底清洗，使得通道内不残留样品成分。 在陷阱捕获过程中，将第一六通切换阀置于端口af，bc和de连接的状态，将第二六通切换阀置于端口ab，cd和ef连接的状态， 电磁阀打开。 载气通过载气通道引入，并通过第一六通阀样通道 - 第二六通切换阀 - 捕集通道 - 第二六通切换阀 - 通道 - 第一六通阀 - 排出 渠道。 载气也通过电子控制流量控制器的路径引入，因此继续执行分析通道的稳定运行。
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