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公开(公告)号：US10273340B2
公开(公告)日：2019-04-30
申请号：US15791864
申请日：2017-10-24
Applicant: PBI Performance Products, Inc.
Inventor： John B. Hopkins, Jr. , Karin M. Hudson , Gregory S. Copeland , Michael Gruender
Abstract: A porous polybenzimidazole (PBI) particulate resin is disclosed. This resin is easily dissolved at ambient temperatures and pressures. The resin is made by: dissolving a virgin PBI resin in a highly polar solvent; precipitating the dissolved PBI in a bath; and drying the precipitated PBI, the dried precipitated PBI being porous. The porous PBI resin may be dissolved by: mixing a porous PBI resin with a highly polar solvent at ambient temperatures and pressures to form a solution.
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公开(公告)号：US20180044493A1
公开(公告)日：2018-02-15
申请号：US15791864
申请日：2017-10-24
Applicant: PBI Performance Products, Inc.
Inventor： John B. Hopkins, JR. , Karin M. Hudson , Gregory S. Copeland , Michael Gruender
CPC classification number: C08J9/00 , C08J3/096 , C08J3/097 , C08J3/11 , C08J9/28 , C08J2201/0542 , C08J2205/04 , C08J2379/04 , Y10T428/2982
Abstract: A porous polybenzimidazole (PBI) particulate resin is disclosed. This resin is easily dissolved at ambient temperatures and pressures. The resin is made by: dissolving a virgin PBI resin in a highly polar solvent; precipitating the dissolved PBI in a bath; and drying the precipitated PBI, the dried precipitated PBI being porous. The porous PBI resin may be dissolved by: mixing a porous PBI resin with a highly polar solvent at ambient temperatures and pressures to form a solution.
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3.发明申请公开(公告)号：US20140309377A1
公开(公告)日：2014-10-16
申请号：US14316892
申请日：2014-06-27
Applicant: PBI Performance Products, Inc.
Inventor： Bobby G. Dawkins , Michael Gruender , Gregory S. Copeland , Tim Hsu
CPC classification number: C08L79/04 , B29C47/0004 , B29C47/0023 , B29C47/6087 , B29C47/786 , B29C47/802 , B29C47/82 , B29C47/822 , B29C47/827 , B29C47/862 , B29C47/92 , C08G65/4012 , C08G73/22 , C08G2261/3442 , C08G2650/40 , C08J3/005 , C08J2365/00 , C08J2371/00 , C08J2379/04 , C08L65/00 , C08L71/00 , C08L2666/22
Abstract: A process for producing a solution blend of a polybenzimidazole (PBI) and a polyetherketoneketone (PEKK). The PBI is mixed with sulfuric acid at a temperature between 40° C. and 80° C. for 30 minutes to 2 hours to produce a PBI solution then cooled to room temperature to form a cooled PBI solution. Then PEKK is added to the cooled PBI solution to form a mixture and that mixture is stirred from 30 minutes to 2 hours at room temperature to form a stirred mixture. The stirred mixture is poured into an excess of water being stirred swiftly to form an aqueous mixture. The aqueous mixture is filtered to produce a blend. The blend is washed with water and dried. The resulting blend can yield a blend in all proportion from 1/99 PBI/PEKK to 99/1 PBI/PEKK.
Abstract translation: 一种制备聚苯并咪唑（PBI）和聚醚酮酮（PEKK）的溶液共混物的方法。 将PBI在40℃至80℃的温度下与硫酸混合30分钟至2小时以产生PBI溶液，然后冷却至室温以形成冷却的PBI溶液。 然后将PEKK加入到冷却的PBI溶液中以形成混合物，并将该混合物在室温下搅拌30分钟至2小时以形成搅拌的混合物。 将搅拌的混合物倒入过量的水中，迅速搅拌以形成含水混合物。 将含水混合物过滤以产生共混物。 将混合物用水洗涤并干燥。 所得共混物可以以1/99 PBI / PEKK至99/1 PBI / PEKK的所有比例产生共混物。
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公开(公告)号：US09827532B2
公开(公告)日：2017-11-28
申请号：US14986779
申请日：2016-01-04
Applicant: PBI Performance Products, Inc.
Inventor： Yan Wang , Michael Gruender , Tai-shung Chung
IPC: B01D39/00 , B01D39/14 , B01D67/00 , B01D15/00 , B29C44/04 , B01D33/21 , B01D61/36 , C08G73/18 , B01D71/64 , B01D63/02 , B01D63/08 , C02F1/44
CPC classification number: B01D61/366 , B01D61/362 , B01D63/02 , B01D63/08 , B01D67/0006 , B01D67/0083 , B01D67/0093 , B01D71/64 , B01D2323/30 , B01D2325/30 , C08G73/18
Abstract: A pervaporation membrane may be an acid-resistant polybenzidimazole (PBI) membrane. The acid-resistant PBI membrane may be a PBI membrane chemically modified by a process selected from the group consisting of sulfonation, phosphonation, cross-linking, N-substitution, and/or combinations thereof. The membrane may be thermally stabilized. A method for the dehydration of an acid material may include the steps of: contacting an acidic aqueous solution with a membrane of an acid-resistant polybenzidimazole; taking away a permeate stream rich in water; and taking away a concentrate steam rich in the acid material. The acidic aqueous solution may be acetic acid.
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Patent Agency Ranking
公开(公告)号：US20160114291A1
公开(公告)日：2016-04-28
申请号：US14986779
申请日：2016-01-04
Applicant: PBI Performance Products, Inc.
Inventor： Yan Wang , Michael Gruender , Tai-shung Chung
CPC classification number: B01D61/366 , B01D61/362 , B01D63/02 , B01D63/08 , B01D67/0006 , B01D67/0083 , B01D67/0093 , B01D71/64 , B01D2323/30 , B01D2325/30 , C08G73/18
Abstract: A pervaporation membrane may be an acid-resistant polybenzidimazole (PBI) membrane. The acid-resistant PBI membrane may be a PBI membrane chemically modified by a process selected from the group consisting of sulfonation, phosphonation, cross-linking, N-substitution, and/or combinations thereof. The membrane may be thermally stabilized. A method for the dehydration of an acid material may include the steps of: contacting an acidic aqueous solution with a membrane of an acid-resistant polybenzidimazole; taking away a permeate stream rich in water; and taking away a concentrate steam rich in the acid material. The acidic aqueous solution may be acetic acid.
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公开(公告)号：USRE46720E1
公开(公告)日：2018-02-20
申请号：US15212512
申请日：2016-07-18
Applicant: PBI Performance Products, Inc.
Inventor： Yan Wang , Michael Gruender , Tai-Shung Chung
CPC classification number: B01D61/366 , B01D61/362 , B01D63/02 , B01D63/08 , B01D67/0006 , B01D67/0083 , B01D67/0093 , B01D71/64 , B01D2323/30 , B01D2325/30 , C08G73/18
Abstract: A pervaporation membrane may be an acid-resistant polybenzidimazole (PBI) membrane. The acid-resistant PBI membrane may be a PBI membrane chemically modified by a process selected from the group consisting of sulfonation, phosphonation, cross-linking, N-substitution, and/or combinations thereof. The membrane may be thermally stabilized. A method for the dehydration of an acid material may include the steps of: contacting an acidic aqueous solution with a membrane of an acid-resistant polybenzidimazole; taking away a permeate stream rich in water; and taking away a concentrate steam rich in the acid material. The acidic aqueous solution may be acetic acid.
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公开(公告)号：US09828479B2
公开(公告)日：2017-11-28
申请号：US13934265
申请日：2013-07-03
Applicant: PBI Performance Products, Inc.
Inventor： John B. Hopkins, Jr. , Karin M. Hudson , Gregory S. Copeland , Michael Gruender
CPC classification number: C08J9/00 , C08J3/096 , C08J3/097 , C08J3/11 , C08J9/28 , C08J2201/0542 , C08J2205/04 , C08J2379/04 , Y10T428/2982
Abstract: A porous polybenzimidazole (PBI) particulate resin is disclosed. This resin is easily dissolved at ambient temperatures and pressures. The resin is made by: dissolving a virgin PBI resin in a highly polar solvent; precipitating the dissolved PBI in a bath; and drying the precipitated PBI, the dried precipitated PBI being porous. The porous PBI resin may be dissolved by: mixing a porous PBI resin with a highly polar solvent at ambient temperatures and pressures to form a solution.
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公开(公告)号：US09156983B2
公开(公告)日：2015-10-13
申请号：US14316892
申请日：2014-06-27
Applicant: PBI Performance Products, Inc.
Inventor： Bobby G. Dawkins , Michael Gruender , Gregory S. Copeland , Tim Hsu
IPC: C08L65/00 , C08L79/00 , C08L79/04 , C08G65/40 , C08J3/00 , C08L71/00 , B29C47/60 , B29C47/80 , B29C47/92 , B29C47/00 , B29C47/82
CPC classification number: C08L79/04 , B29C47/0004 , B29C47/0023 , B29C47/6087 , B29C47/786 , B29C47/802 , B29C47/82 , B29C47/822 , B29C47/827 , B29C47/862 , B29C47/92 , C08G65/4012 , C08G73/22 , C08G2261/3442 , C08G2650/40 , C08J3/005 , C08J2365/00 , C08J2371/00 , C08J2379/04 , C08L65/00 , C08L71/00 , C08L2666/22
Abstract: A process for producing a solution blend of a polybenzimidazole (PBI) and a polyetherketoneketone (PEKK). The PBI is mixed with sulfuric acid at a temperature between 40° C. and 80° C. for 30 minutes to 2 hours to produce a PBI solution then cooled to room temperature to form a cooled PBI solution. Then PEKK is added to the cooled PBI solution to form a mixture and that mixture is stirred from 30 minutes to 2 hours at room temperature to form a stirred mixture. The stirred mixture is poured into an excess of water being stirred swiftly to form an aqueous mixture. The aqueous mixture is filtered to produce a blend. The blend is washed with water and dried. The resulting blend can yield a blend in all proportion from 1/99 PBI/PEKK to 99/1 PBI/PEKK.
Abstract translation: 一种制备聚苯并咪唑（PBI）和聚醚酮酮（PEKK）的溶液共混物的方法。 将PBI在40℃至80℃的温度下与硫酸混合30分钟至2小时以产生PBI溶液，然后冷却至室温以形成冷却的PBI溶液。 然后将PEKK加入到冷却的PBI溶液中以形成混合物，并将该混合物在室温下搅拌30分钟至2小时以形成搅拌的混合物。 将搅拌的混合物倒入过量的水中，迅速搅拌以形成含水混合物。 将含水混合物过滤以产生共混物。 将混合物用水洗涤并干燥。 所得共混物可以以1/99 PBI / PEKK至99/1 PBI / PEKK的所有比例产生共混物。
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公开(公告)号：US20130331470A1
公开(公告)日：2013-12-12
申请号：US13934265
申请日：2013-07-03
Applicant: PBI Performance Products Inc.
Inventor： John B. Hopkins, JR. , Karin M. Hudson , Gregory S. Copeland , Michael Gruender
IPC: C08J9/00
CPC classification number: C08J9/00 , C08J3/096 , C08J3/097 , C08J3/11 , C08J9/28 , C08J2201/0542 , C08J2205/04 , C08J2379/04 , Y10T428/2982
Abstract: A porous polybenzimidazole (PBI) particulate resin is disclosed. This resin is easily dissolved at ambient temperatures and pressures. The resin is made by: dissolving a virgin PBI resin in a highly polar solvent; precipitating the dissolved PBI in a bath; and drying the precipitated PBI, the dried precipitated PBI being porous. The porous PBI resin may be dissolved by: mixing a porous PBI resin with a highly polar solvent at ambient temperatures and pressures to form a solution.
Abstract translation: 公开了一种多孔聚苯并咪唑（PBI）颗粒树脂。 该树脂在环境温度和压力下容易溶解。 树脂通过以下方法制备：将未处理的PBI树脂溶解在高极性溶剂中; 将溶解的PBI沉淀在浴中; 并干燥沉淀的PBI，干燥的沉淀PBI是多孔的。 可以通过在环境温度和压力下将多孔PBI树脂与高极性溶剂混合以形成溶液来溶解多孔PBI树脂。
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