POLYMER-MEDIATED PARTICLE COARSENING WITHIN HOLLOW SILICA SHELL NANOREACTORS

    公开(公告)号:US20230286047A1

    公开(公告)日:2023-09-14

    申请号:US18118031

    申请日:2023-03-06

    IPC分类号: B22F9/26 B22F1/054 B22F1/16

    摘要: A method of forming a nanoparticle can include admixing an aqueous solution into an oil-phase to thereby form an emulsion of droplets of the aqueous solution in the oil phase, the aqueous solution comprising a nanostructure precursor and a polymer, adding a silane precursor and catalyst to form a silica shell around each of the droplets to nanoreactors; annealing at a first temperature below the decomposition temperature of the polymer to aggregate the nanostructure precursor within the nanoreactor; and annealing at a second temperature above the decomposition temperature of the polymer to convert the aggregated nanostructure precursor to the nanostructure and decompose the polymer.