Method of forming a protective coating on a surface of a ceramic substrate

    公开(公告)号:US11236023B2

    公开(公告)日:2022-02-01

    申请号:US16183276

    申请日:2018-11-07

    摘要: A method for forming a protective coating on a surface of a ceramic substrate includes combining a rare-earth oxide, alumina, and silica to form a powder, etching the surface of the ceramic substrate, applying the powder on the etched surface in an amount of from about 0.001 to about 0.1 g/cm2 to reduce capture of bubbles from off-gassing of the ceramic substrate, heating the powder for a time of from about 5 to about 60 minutes to a temperature at or above the melting point such that the powder melts and forms a molten coating on the surface that has a minimized number of bubbles, and cooling the molten coating to ambient temperature to form the protective coating disposed on and in direct contact with the surface of the ceramic substrate such that the protective coating has a thickness of less than about 1 mil.

    HEAT EXCHANGERS, HEAT EXCHANGER TUBES, AND ADDITIVE MANUFACTURING COLD SPRAY PROCESSES FOR PRODUCING THE SAME

    公开(公告)号:US20190234697A1

    公开(公告)日:2019-08-01

    申请号:US15882160

    申请日:2018-01-29

    摘要: Methods are disclosed for fabricating heat exchangers and Heat Exchanger (HX) tubes, as are heat exchangers fabricated in accordance with such methods. In embodiments, the method includes the steps or processes of obtaining a Non-Equilibrium Alloy (NEA) feedstock powder comprised of an alloy matrix throughout which at least one minority constituent is dispersed. The first minority constituent precipitates from the alloy matrix when the NEA feedstock powder is exposed to temperatures exceeding a critical temperature threshold (TCRITICAL) for a predetermined time period. A cold spray process is carried-out to at least partially form the HX tubes from the NEA feedstock powder; and the HX tubes are subsequently installed in the heat exchanger. The HX tubes are exposed to a maximum temperature (TSPRAY_MAX) during the cold spray process, which is maintained below TCRITICAL to substantially preserve the non-equilibrium state of the NEA feedstock powder through cold spray deposition.