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公开(公告)号：US11951072B2
公开(公告)日：2024-04-09
申请号：US16653974
申请日：2019-10-15
申请人： CORNING INCORPORATED
发明人： Dana Craig Bookbinder , Theresa Chang , Paul Stephen Danielson , Steven Edward DeMartino , Andrei Gennadyevich Fadeev , Robert Michael Morena , Santona Pal , John Stephen Peanasky , Robert Anthony Schaut , Christopher Lee Timmons , Natesan Venkataraman , Ronald Luce Verkleeren
IPC分类号： A61J1/14 , A61J1/06 , B32B17/06 , B65D1/02 , B65D1/40 , B65D23/02 , B65D23/08 , B65D25/14 , B65D25/34 , B65D65/42 , C03B23/04 , C03C15/02 , C03C17/00 , C03C17/22 , C03C17/30 , C03C17/32 , C03C17/34 , C03C17/42 , C03C21/00 , C09D179/08
CPC分类号： A61J1/1468 , A61J1/065 , B32B17/06 , B65D1/0207 , B65D1/0215 , B65D1/40 , B65D23/02 , B65D23/0814 , B65D23/0821 , B65D25/14 , B65D25/34 , B65D65/42 , C03B23/04 , C03C15/02 , C03C17/005 , C03C17/22 , C03C17/30 , C03C17/32 , C03C17/3405 , C03C17/42 , C03C21/002 , C09D179/08 , C03C2217/78 , C03C2218/111 , Y10T428/13 , Y10T428/131 , Y10T428/1317 , Y10T428/24802 , Y10T428/315
摘要： A coated glass pharmaceutical package includes a glass body having a Type 1 chemical durability according to USP 660, at least a class A2 base resistance or better according to ISO 695, and at least a type HGB2 hydrolytic resistance or better according to ISO 719, the glass body having an interior surface and an exterior surface and a wall extending therebetween. A lubricous coating having a thickness of less than or equal to 90 nm may be positioned on at least a portion of the exterior surface of the glass body but not on any portion of the interior surface. The portion of the coated glass package with the lubricous coating comprises a coefficient of friction that is at least 20% less than an uncoated glass package and the coefficient of friction does not increase by more than 30% after undergoing a depyrogenation cycle including exposure to a temperature of 250° C. for a time period of 30 minutes. A horizontal compression strength of the coated glass package is at least 10% greater than an uncoated glass package and the horizontal compression strength is not reduced by more than 20% after undergoing the depyrogenation cycle including exposure to a temperature of 250° C. for a time period of 30 minutes and then being abraded. The lubricous coating comprises a polymer.
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公开(公告)号：US11786441B2
公开(公告)日：2023-10-17
申请号：US16024825
申请日：2018-06-30
申请人： CORNING INCORPORATED
发明人： Andrei Gennadyevich Fadeev , Theresa Chang , Dana Craig Bookbinder , Santona Pal , Chandan Kumar Saha , Steven Edward DeMartino , Christopher Lee Timmons , John Stephen Peanasky
CPC分类号： A61J1/1468 , B65D23/0821 , C03C17/005 , C03C17/30 , C03C17/32 , C03C17/42 , C03C21/002 , C03C2217/78 , Y10T428/1321 , Y10T428/24926 , Y10T428/265
摘要： Coated pharmaceutical packages are disclosed. The coated pharmaceutical packages may Include a glass body formed from borosilicate glass that meets Type 1 criteria according to USP or alkali aluminosilicate glass having a Class HGA 1 hydrolytic resistance when tested according to the ISO 720-1985 testing standard. A low-friction coating comprising a polymer may be positioned on a portion of the exterior surface. A coefficient of friction of an abraded area of the portion of the exterior surface with the low-friction coating may be less than 0.7 after exposure to a temperature of 260° C. for 30 minutes and abrasion under a load of at least 10 N and does not have observable damage. A retained strength of the coated glass article in horizontal compression does not decrease by more than 20% after the temperature exposure and the abrasion.
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公开(公告)号：US10786431B2
公开(公告)日：2020-09-29
申请号：US16185828
申请日：2018-11-09
申请人： CORNING INCORPORATED
发明人： Theresa Chang , Paul Stephen Danielson , Steven Edward DeMartino , Andrei Gennadyevich Fadeev , Robert Michael Morena , Santona Pal , John Stephen Peanasky , Robert Anthony Schaut , Christopher Lee Timmons , Natesan Venkataraman , Ronald Luce Verkleeren
IPC分类号： A61J1/14 , B65D23/08 , C03C17/22 , B65D25/14 , B65D1/40 , C03C17/00 , C03C21/00 , B65D23/02 , C03C17/34 , A61J1/06 , C03C15/02 , B65D1/02 , B65D25/34 , B32B17/06 , C03C17/30 , C03C17/32 , C03C17/42 , C09D179/08 , B65D65/42
摘要： A delamination resistant glass pharmaceutical container may include a glass body comprising a borosilicate glass having a Type 1 chemical durability according to USP . At least an inner surface of the glass body may have a delamination factor less than or equal to 10. A thermally stable coating may be positioned around at least a portion of the outer surface of the glass body. The thermally stable coating may be an outermost coating on the outer surface of the glass body and the outer surface of the glass body with the thermally stable coating has a coefficient of friction less than or equal to 0.7. The thermally stable coating comprising at least one of a metal nitride coating, a metal oxide coating, a metal sulfide coating, SiO2, diamond-like carbon, graphene, and a carbide coating.
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公开(公告)号：US20200268608A1
公开(公告)日：2020-08-27
申请号：US16870657
申请日：2020-05-08
申请人： CORNING INCORPORATED
发明人： Andrei Gennadyevich Fadeev , Theresa Chang , Dana Craig Bookbinder , Santona Pal , Chandan Kumar Saha , Steven Edward DeMartino , Christopher Lee Timmons , John Stephen Peanasky
IPC分类号： A61J1/14 , B65D65/42 , A61J1/00 , B65D23/08 , C03C17/00 , C03C21/00 , B65D25/14 , C03C17/30 , C03C17/32 , C09D179/08 , C03C17/42 , B65D25/34
摘要： According to embodiments, a method of making a coated pharmaceutical container, may include: forming a glass tube; forming the glass tube into a pharmaceutical container comprising an interior surface and an exterior surface; and applying a coating to the exterior surface. The coating may have a coefficient of friction less than or equal to 0.7 relative to a second pharmaceutical container when tested in a vial-on-vial testing jig under a normal load of 30 N. The coated pharmaceutical container may be thermally stable after depyrogenation at a temperature of at least 260° C. for 30 minutes in air.
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5.发明授权公开(公告)号：US10684265B2
公开(公告)日：2020-06-16
申请号：US15693693
申请日：2017-09-01
申请人： CORNING INCORPORATED
发明人： Robert Scott Burkhalter , Andrei Gennadyevich Fadeev , John Stephen Peanasky , David Charles Sauer
摘要： A method for measuring volatile organic compounds includes loading glass containers into an oven, heating the oven, purging the oven with dry clean air, collecting a volumetric portion of an oven exhaust, trapping volatile organic compounds from the volumetric portion, and measuring the volatile organic compounds trapped in the trap. The one or more glass containers are in-tact while measuring the VOCs of the coated glass container. An apparatus includes an oven having an interior volume that is capable of holding one or more in-tact glass containers, a flow meter fluidly connected to the first trap, and a pump fluidly connected to the flow meter. The first trap collects volatile organic compounds from a volumetric portion of the oven exhaust gas. The pump controls a flow rate of the volumetric portion of the oven exhaust gas across the first trap.
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公开(公告)号：US20190084875A1
公开(公告)日：2019-03-21
申请号：US16185819
申请日：2018-11-09
申请人： CORNING INCORPORATED
发明人： Theresa Chang , Paul Stephen Danielson , Steven Edward DeMartino , Andrei Gennadyevich Fadeev , Robert Michael Morena , Santona Pal , John Stephen Peanasky , Robert Anthony Schaut , Christopher Lee Timmons , Natesan Venkataraman , Ronald Luce Verkleeren
IPC分类号： C03C17/42 , B65D25/14 , B65D1/02 , B65D25/34 , B65D65/42 , A61J1/14 , B65D23/08 , B65D23/02 , C03C21/00 , C03C17/00 , B65D1/40 , C03C15/02 , C09D179/08 , C03C17/32 , C03C17/30 , B32B17/06 , C03C17/34
摘要： Glass pharmaceutical packages comprising glass containers are disclosed. In embodiments, a coated glass pharmaceutical package includes a glass container formed from one of a borosilicate glass composition that meets Type 1 criteria according to USP or an alkali aluminosilicate glass having a Class HGA 1 hydrolytic resistance when tested according to the ISO 720-1985 testing standard. A lubricous coating may be positioned on at least a portion of the exterior surface of the glass container. The portion of the coated glass pharmaceutical package with the lubricous coating has a coefficient of friction that is at least 20% less than an uncoated glass pharmaceutical package. A horizontal compression strength of the portion of the coated glass pharmaceutical package with the lubricous coating may be at least 10% greater than an uncoated glass pharmaceutical package.
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公开(公告)号：US20190076331A1
公开(公告)日：2019-03-14
申请号：US16185493
申请日：2018-11-09
申请人： CORNING INCORPORATED
发明人： Andrei Gennadyevich Fadeev , Theresa Chang , Dana Craig Bookbinder , Santona Pal , Chandan Kumar Saha , Steven Edward DeMartino , Christopher Lee Timmons , John Stephen Peanasky
IPC分类号： A61J1/14 , B65D65/42 , B65D23/08 , C09D179/08 , B65D25/14 , C03C21/00 , C03C17/42 , C03C17/00 , B65D25/34 , C03C17/32 , C03C17/30 , A61J1/00
摘要： Coated glass pharmaceutical packages are disclosed. According to embodiments, a coated glass pharmaceutical package may include a glass container formed from one of a borosilicate glass composition that meets Type 1 criteria according to USP or an alkali aluminosilicate glass having a Class HGA 1 hydrolytic resistance when tested according to the ISO 720-1985 testing standard. A low-friction coating may be bonded to the exterior surface of the glass container. The low-friction coating may include a polymer. The exterior surface of the glass container with the low-friction coating may have a coefficient of friction of less than or equal to 0.7. The coated glass pharmaceutical package may be thermally stable after depyrogenation in air at a temperature of at least about 260° C. for 30 minutes.
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公开(公告)号：US20180171162A1
公开(公告)日：2018-06-21
申请号：US15834802
申请日：2017-12-07
申请人： Corning Incorporated
摘要： An aqueous formulation and method of making an ultraviolet light blocking coating from an aqueous formulation having from greater than or equal to 15 wt % to less than or equal to 65 wt % water, from greater than or equal to 30 wt % to less than or equal to 70 wt % metal oxide particles, and from greater than or equal to 5 wt % to less than or equal to 35 wt % aminoalkylsilsesquioxane oligomers. An optical device including a housing, a lens element, potting material positioned between the lens element and the housing, and an ultraviolet light blocking coating positioned between the lens element and the potting material. The ultraviolet light blocking coating has from greater than or equal to 30 wt % to less than or equal to 90 wt % metal oxide particles and from greater than or equal to 10 wt % to less than or equal to 70 wt % silsesquioxane.
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公开(公告)号：US09763852B2
公开(公告)日：2017-09-19
申请号：US13780740
申请日：2013-02-28
申请人： Corning Incorporated
发明人： Andrei Gennadyevich Fadeev , Theresa Chang , Dana Craig Bookbinder , Santona Pal , Chandan Kumar Saha , Steven Edward DeMartino , Christopher Lee Timmons , John Stephen Peanasky
IPC分类号： A61J1/00 , B65D25/14 , C03C17/30 , A61J1/14 , B65D23/08 , B65D65/42 , C03C17/32 , C03C17/42 , C03C17/00 , C03C21/00 , C09D179/08
CPC分类号： A61J1/1468 , A61J1/00 , B65D23/0814 , B65D23/0821 , B65D25/14 , B65D25/34 , B65D65/42 , C03C17/005 , C03C17/30 , C03C17/32 , C03C17/42 , C03C21/002 , C03C2217/78 , C03C2218/111 , C09D179/08 , Y10T428/1321 , Y10T428/24942
摘要： Low-friction coatings and glass articles with low-friction coatings are disclosed. According to one embodiment, a coated glass article may include a glass body comprising a first surface and a low-friction coating positioned on at least a portion of the first surface of the glass body. The low-friction coating may include a polymer chemical composition. The coated glass article may be thermally stable at a temperature of at least about 260° C. for 30 minutes. A light transmission through the coated glass article may be greater than or equal to about 55% of a light transmission through an uncoated glass article for wavelengths from about 400 nm to about 700 nm. The low-friction coating may have a mass loss of less than about 5% of its mass when heated from a temperature of 150° C. to 350° C. at a ramp rate of about 10° C./minute.
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公开(公告)号：US09744099B2
公开(公告)日：2017-08-29
申请号：US15331113
申请日：2016-10-21
申请人： Corning Incorporated
发明人： Andrei Gennadyevich Fadeev , Theresa Chang , Dana Craig Bookbinder , Santona Pal , Chandan Kumar Saha , Steven Edward DeMartino , Christopher Lee Timmons , John Stephen Peanasky
IPC分类号： A61J1/00 , B65D65/42 , B65D23/08 , B65D25/14 , C03C17/30 , C03C17/32 , C09D179/08 , C03C17/00 , C03C17/42 , C03C21/00 , A61J1/14
CPC分类号： A61J1/1468 , A61J1/00 , B65D23/0814 , B65D23/0821 , B65D25/14 , B65D25/34 , B65D65/42 , C03C17/005 , C03C17/30 , C03C17/32 , C03C17/42 , C03C21/002 , C03C2217/78 , C03C2218/111 , C09D179/08 , Y10T428/1321 , Y10T428/24942
摘要： A coated glass pharmaceutical package may include a body formed from borosilicate glass that meets the Type 1 criteria according to USP . The body may have an interior surface and an exterior surface. A low-friction coating having a thickness of less than 100 microns may be positioned on at least a portion of the exterior surface. The portion of the exterior surface with the low-friction coating may have a coefficient of friction that is at least 20% less than an uncoated glass pharmaceutical package formed from the same glass composition and the coefficient of friction may not increase by more than 30% after undergoing a depyrogenation cycle at a temperature of from 250° C. to 400° C. for a time period of from 30 seconds to 72 hours.
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