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公开(公告)号：US10676451B2
公开(公告)日：2020-06-09
申请号：US16315345
申请日：2017-07-19
发明人： Joaquim Henrique Teles , Marvin Kramp , Christian Mueller , Nicolai Tonio Woerz , Bernd Metzen , Tobias Keller , Dominic Riedel , Heiner Schelling , Markus Weber , Daniel Urbanczyk , Andrei-Nicolae Parvulescu , Ulrike Wegerle , Ulrich Mueller , Meinolf Weidenbach , Werner J. Witzl
IPC分类号： C07D301/32 , B01D3/14 , C07D303/04
摘要： Disclosed is a process for purifying propylene oxide. A stream S0 containing propylene oxide, acetonitrile, water, and an organic compound containing one or more of acetone and propionaldehyde is provided. Propylene oxide is separated from S0 by subjecting S0 to distillation in a first distillation unit, obtaining a gaseous top stream S1c enriched in propylene oxide, a liquid bottom stream S1a enriched in acetonitrile and water, and a side stream S1b containing propylene oxide and enriched in the carbonyl compound; reacting the carbonyl compound in S1b with an organic compound containing an amino group to obtain a reaction product; separating propylene oxide from the reaction product in a second distillation unit, obtaining a gaseous top stream S3a enriched in propylene oxide and a liquid bottoms stream S3b enriched in the reaction product; and introducing stream S3a into the first distillation unit.
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公开(公告)号：US10435381B2
公开(公告)日：2019-10-08
申请号：US16318221
申请日：2017-07-19
发明人： Joaquim Henrique Teles , Marvin Kramp , Christian Mueller , Nicolai Tonio Woerz , Bernd Metzen , Tobias Keller , Dominic Riedel , Heiner Schelling , Markus Weber , Daniel Urbanczyk , Andrei-Nicolae Parvulescu , Ulrike Wegerle , Ulrich Mueller , Meinolf Weidenbach , Werner J. Witzl , Karsten Luecke
IPC分类号： C07D301/32 , C07D301/12 , C07D303/04 , B01D3/00 , B01D3/14 , B01D5/00 , B01D3/40 , B01J29/08
摘要： The present invention is related to a process for preparing propylene oxide, comprising (i) providing a stream comprising propene, hydrogen peroxide or a source of hydrogen peroxide, water, and an organic solvent; (ii) passing the liquid feed stream provided in (i) into an epoxidation zone comprising an epoxidation catalyst comprising a titanium zeolite, and subjecting the liquid feed stream to epoxidation reaction conditions in the epoxidation zone, obtaining a reaction mixture comprising propene, propylene oxide, water, and the organic solvent; (iii) removing an effluent stream from the epoxidation zone, the effluent stream comprising propylene oxide, water, organic solvent, and propene; (iv) separating propene from the effluent stream by distillation, comprising (iv.1) subjecting the effluent stream to distillation conditions in a distillation unit, obtaining a gaseous top stream S0 enriched in propene compared to the effluent stream subjected to distillation conditions, and a liquid bottoms stream S01 enriched in propylene oxide, water and organic solvent compared to the effluent stream subjected to distillation conditions; (iv.2) returning a condensed portion of the stream S0 to an upper part of the distillation unit.
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公开(公告)号：US10189946B2
公开(公告)日：2019-01-29
申请号：US15121940
申请日：2014-12-12
申请人： BASF SE
发明人： Christoph Mueller , Thomas Reissner , Ansgar Gereon Altenhoff , Andreas Kunst , Christian Mueller
摘要： The present invention relates to a process for preparing polyamines having a mean molecular weight of ≥203 g/mol, in which the deviation from the mean molecular weight per ° C. of change in the reaction temperature is
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公开(公告)号：US11180467B2
公开(公告)日：2021-11-23
申请号：US16500313
申请日：2018-04-13
申请人： BASF SE
发明人： Nicolai Tonio Woerz , Ulrich Mueller , Andrei-Nicolae Parvulescu , Dominic Riedel , Marvin Kramp , Daniel Urbanczyk , Ulrike Wegerle , Christian Mueller , Bernd Metzen , Markus Weber , Joaquim Henrique Teles
IPC分类号： C07D301/32 , C07D301/19 , C07D301/12
摘要： The invention relates to a process for preparing propylene oxide, comprising (i) providing a stream comprising propene, propane, hydrogen peroxide or a source of hydrogen peroxide, water, and an organic solvent; (ii) passing the liquid feed stream provided in (i) into an epoxidation zone comprising an epoxidation catalyst comprising a titanium zeolite, and subjecting the liquid feed stream to epoxidation reaction conditions in the epoxidation zone, obtaining a reaction mixture comprising propene, propane, propylene oxide, water, and the organic solvent; (iii) removing an effluent stream from the epoxidation zone, the effluent stream comprising propene, propane, propylene oxide, water, and the organic solvent; (iv) separating propene and propane from the effluent stream by distillation, comprising subjecting the effluent stream to distillation conditions in a distillation unit, obtaining a gaseous stream (S1) which is enriched in propene and propane compared to the effluent stream subjected to distillation conditions, and a liquid bottoms stream (S2) which is enriched in propylene oxide, water and organic solvent compared to the effluent stream subjected to distillation conditions; (v) separating propane from the stream (S1) in a separation zone, comprising subjecting the stream (S1) to washing conditions in a scrubber, wherein a solvent mixture comprising organic solvent and water is added as entraining agent, obtaining a bottoms stream (S3), which comprises organic solvent, water and at least 70 weight-% of the propene comprised in (S1); and a gaseous top stream (S4), which comprises at least 5 weight-% of the propane comprised in stream (S1).
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公开(公告)号：US11351525B2
公开(公告)日：2022-06-07
申请号：US16462430
申请日：2017-12-20
申请人： BASF SE
发明人： Andrei-Nicolae Parvulescu , Ulrich Mueller , Hans-Juergen Luetzel , Georg Uhl , Joaquim Henrique Teles , Dominic Riedel , Daniel Urbanczyk , Ulrike Wegerle , Markus Weber , Nicolai Tonio Woerz , Christian Mueller , Ruediger Schmitt , Xiana Romani Fernandez , Harald Wuerz
摘要： Use of an acid-treated titanium-containing zeolitic material having framework type MWW for preparing a composition having a relative plasticity of less than 1.
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公开(公告)号：US11110442B2
公开(公告)日：2021-09-07
申请号：US16997038
申请日：2020-08-19
申请人： BASF SE
发明人： Andrei-Nicolae Parvulescu , Ulrich Mueller , Hans-Juergen Luetzel , Joaquim Henrique Teles , Dominic Riedel , Daniel Urbanczyk , Ulrike Wegerle , Markus Weber , Nicolai Tonio Woerz , Christian Mueller
IPC分类号： B01J29/89 , B01J29/70 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/08 , C01B39/02 , C01B39/06 , C01B39/12 , C07D301/12
摘要： A process for preparing a molding comprising zinc and a titanium-containing zeolitic material having framework type MWW, comprising (i) providing a molding comprising a titanium-containing zeolitic material having framework type MWW; (ii) preparing an aqueous suspension comprising a zinc source and the molding comprising a titanium-containing zeolitic material having framework type MWW prepared in (i); (iii) heating the aqueous suspension prepared in (ii) under autogenous pressure to a temperature of the liquid phase of the aqueous suspension in the range of from 100 to 200° C., obtaining an aqueous suspension comprising a molding comprising zinc and a titanium-containing zeolitic material having framework type MWW; (iv) separating the molding comprising zinc and a titanium-containing zeolitic material having framework type MWW from the liquid phase of the suspension obtained in (iii).
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公开(公告)号：US11291980B2
公开(公告)日：2022-04-05
申请号：US16461134
申请日：2017-12-20
申请人： BASF SE
发明人： Andrei-Nicolae Parvulescu , Ulrich Mueller , Hans-Juergen Luetzel , Georg Uhl , Joaquim Henrique Teles , Dominic Riedel , Daniel Urbanczyk , Ulrike Wegerle , Markus Weber , Nicolai Tonio Woerz , Christian Mueller
摘要： A process for preparing an extrudable composition comprising a titanium-containing zeolitic material having framework type MWW, the process comprising providing a titanium-containing zeolitic material having framework type MWW, having a water absorption capacity of at least 11 weight-%, subjecting the titanium-containing zeolitic material having framework type MWW an acid treatment, optionally incorporating zinc in the acid-treated titanium-containing zeolitic material having framework type MWW; preparing a composition comprising the titanium-containing zeolitic material having framework type MWW obtained from (ii) or (iii), a precursor of a silica binder, water, and a kneading agent, wherein the composition does not comprise a polyethylene oxide.
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公开(公告)号：US20210253861A1
公开(公告)日：2021-08-19
申请号：US17270972
申请日：2019-08-27
申请人： BASF SE
发明人： Donald Charles Mente , Gustavo E. Leon , Gene Michael Scheffler , Christian Mueller , Stephan Weinkoetz
摘要： A lignocellulosic composite article includes a plurality of lignocellulosic pieces and an adhesive system disposed on the plurality of lignocellulosic pieces for bonding the plurality of lignocellulosic pieces. The adhesive system comprises a binder component and an additive component. The binder component comprises a diphenylmethane diisocyanate (MDI), a polymeric diphenylmethane diisocyanate (pMDI), and combinations thereof. The additive component comprises an amine compound and water. The amine compound can be imidazole. The additive component is useful for reducing the amount of press time required during manufacture of the composite article.
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公开(公告)号：US10780432B2
公开(公告)日：2020-09-22
申请号：US16470834
申请日：2018-01-18
申请人： BASF SE
发明人： Andrei-Nicolae Parvulescu , Ulrich Mueller , Hans-Juergen Luetzel , Joaquim Henrique Teles , Dominic Riedel , Daniel Urbanczyk , Ulrike Wegerle , Markus Weber , Nicolai Tonio Woerz , Christian Mueller
IPC分类号： B01J29/89 , B01J29/70 , B01J35/02 , B01J35/10 , B01J37/00 , C01B39/02 , C01B39/06 , C01B39/12 , C07D301/12 , B01J37/08
摘要： A process for preparing a molding comprising zinc and a titanium-containing zeolitic material having framework type MWW, comprising (i) providing a molding comprising a titanium-containing zeolitic material having framework type MWW; (ii) preparing an aqueous suspension comprising a zinc source and the molding comprising a titanium-containing zeolitic material having framework type MWW prepared in (i); (iii) heating the aqueous suspension prepared in (ii) under autogenous pressure to a temperature of the liquid phase of the aqueous suspension in the range of from 100 to 200° C., obtaining an aqueous suspension comprising a molding comprising zinc and a titanium-containing zeolitic material having framework type MWW; (iv) separating the molding comprising zinc and a titanium-containing zeolitic material having framework type MWW from the liquid phase of the suspension obtained in (iii).
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公开(公告)号：US10544116B2
公开(公告)日：2020-01-28
申请号：US16315680
申请日：2017-07-19
申请人： BASF SE
发明人： Joaquim Henrique Teles , Marvin Kramp , Christian Mueller , Nicolai Tonio Woerz , Bernd Metzen , Tobias Keller , Dominic Riedel , Markus Weber , Daniel Urbanczyk , Andrei-Nicolae Parvulescu , Ulrike Wegerle , Ulrich Mueller
IPC分类号： C07D301/12 , C07D301/32 , C07D303/04
摘要： Disclosed herein is a process for purifying propylene oxide, including the steps of: (i) providing a stream S0 containing propylene oxide, acetonitrile, water, and an organic compound containing a carbonyl group —C(═O)—; and (ii) separating propylene oxide from the stream S0 by subjecting the stream S0 to distillation conditions in a distillation column to obtain a gaseous top stream S1c which is enriched in propylene oxide compared to the stream S0, a liquid bottoms stream S1a which is enriched in acetonitrile and water compared to the stream S0, and a side stream S1b containing propylene oxide which is enriched in the carbonyl compound compared to the stream S0.
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