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    REACTOR FOR CARRYING OUT A REACTION BETWEEN TWO NON-MISCIBLE FLUIDS OF DIFFERENT DENSITIES
    1.
    发明申请
    REACTOR FOR CARRYING OUT A REACTION BETWEEN TWO NON-MISCIBLE FLUIDS OF DIFFERENT DENSITIES 有权

    公开(公告)号：US20210275987A1

    公开(公告)日：2021-09-09

    申请号：US17274148

    申请日：2019-09-03

    Applicant: BASF SE

    Inventor： Oliver BEY ,  Peter ZEHNER ,  Mathias SCHELWIES ,  Rocco PACIELLO ,  Martin HAUBNER ,  Guenter WEGNER ,  Gerd TEBBEN ,  Gunnar HEYDRICH ,  Georg SEEBER ,  Michael ACKER

    IPC: B01J19/26 ,  C07C45/62 ,  B01J19/24 ,  B01J19/00

    Abstract: A reactor for performing a reaction between two immiscible fluids of different density, comprising an interior formed by a cylindrical, vertically oriented elongate shell, a bottom and a cap, wherein the interior is divided by internals into a backmixed zone, a zone of limited backmixing preferably arranged below the backmixed zone and a plug-flow zone which are at least consecutively traversable by one of the fluids, wherein the backmixed zone comprises at least one inlet and the plug-flow zone comprises an outlet and the backmixed zone comprises at least one mixing apparatus selected from a stirrer, a jet nozzle and means for injecting the fluid of lower density, a first cylindrical internal element which in the interior extends in the longitudinal direction of the reactor, which delimits the zone of limited backmixing from the plug-flow zone and which comprises a first passage to the backmixed zone and a second passage to the plug-flow zone, a second internal element which delimits the backmixed zone from the plug-flow zone such that there is no direct fluid connection between the backmixed zone and the plug-flow zone, and backmixing-preventing third internal elements in the form of random packings, structured packings or liquid-permeable trays arranged in the zone of limited backmixing. The reactor allows an optimal residence time distribution in the reaction of the two immiscible fluids of different density. The invention further relates to a process for performing a continuous reaction in the reactor.

    REACTOR FOR CARRYING OUT A GAS-LIQUID TWO-PHASE HIGH-PRESSURE REACTION WITH A FOAMING MEDIUM
    2.
    发明申请
    REACTOR FOR CARRYING OUT A GAS-LIQUID TWO-PHASE HIGH-PRESSURE REACTION WITH A FOAMING MEDIUM 有权

    公开(公告)号：US20210371361A1

    公开(公告)日：2021-12-02

    申请号：US17274135

    申请日：2019-09-03

    Applicant: BASF SE

    Inventor： Oliver BEY ,  Peter ZEHNER ,  Michael ACKER ,  Rocco PACIELLO ,  Mathias SCHELWIES ,  Martin HAUBNER ,  Guenter WEGNER ,  Gerd TEBBEN ,  Gunnar HEYDRICH ,  Georg SEEBER

    IPC: C07C29/141 ,  B01J19/00 ,  B01J19/24 ,  B01J19/26 ,  B01J19/30 ,  B01J19/32 ,  B01J31/20 ,  B01J3/04

    Abstract: A reactor for performing a gas/liquid biphasic high-pressure reaction with a foaming medium, comprising an interior formed by a cylindrical, vertically oriented elongate shell, a bottom and a cap, wherein the interior is divided by internals into a backmixed zone and a zone of limited backmixing, wherein the backmixed zone and the zone of limited backmixing are consecutively traversable by the reaction mixture, wherein the backmixed zone comprises means for introducing gas and liquid and a gas outlet and also comprises at least one mixing apparatus selected from a stirrer, a jet nozzle and means for injecting the gas, and the zone of limited backmixing comprises a reaction product outlet, a first cylindrical internal element which in the interior extends in the longitudinal direction of the reactor and which delimits the zone of limited backmixing from the backmixed zone, backmixing-preventing second internal elements in the form of random packings, structured packings or liquid-permeable trays arranged in the zone of limited backmixing and a riser tube whose lower end is arranged within the backmixed zone and whose upper end opens into the zone of limited backmixing so that liquid from the backmixed zone can ascend into the zone of limited backmixing via the riser tube, wherein flow into the zone of limited backmixing enters from below. The reactor is configured such that the high-pressure reaction space is optimally utilized and contamination of workup steps or subsequent reactions arranged downstream of the high-pressure reaction with foam is substantially avoided. The invention further relates to a process for performing a continuous gas/liquid biphasic high-pressure reaction in the reactor.

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