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1.发明授权Method for producing 3,4-dihydro-1,2,3-oxathiazin-4-one-2,2-dioxide compound or salt thereof 失效制备3,4-二氢-1,2,3-氧杂噻嗪-4-酮-2,2-二氧化物化合物或其盐的方法公开(公告)号：US07662957B2
公开(公告)日：2010-02-16
申请号：US12373922
申请日：2007-08-02
申请人： Akira Saito , Yuki Ishiguro , Yasushi Yamamoto
发明人： Akira Saito , Yuki Ishiguro , Yasushi Yamamoto
IPC分类号： C07D291/06
CPC分类号： C07D291/06
摘要： A high quality 3,4-dihydro-1,2,3-oxathiazin-4-one-2,2-dioxide compound or a salt thereof is obtained easily and efficiently.When the compound represented by the following formula (2)[Formula 2] (wherein, R1, R2, and R3 are hydrogen atom or an organic group inert to the reaction, and X is hydrogen atom) or a salt thereof is produced by cyclization of a mixture of β-ketoamide-N-sulfonic acid represented by the following formula (1) [Formula 1] or a salt thereof and an inert solvent and a mixture of acid anhydride and an inert solvent, and by subsequent hydrolysis of the product, a step of (A) hydrolyzing the reaction product obtained by the cyclization by mixing with an aqueous solution of sulfuric acid so as a concentration of sulfuric acid in an aqueous phase after the hydrolysis would become 30% by weight or more, and then separating an organic phase and an aqueous phase, or a step of (B) washing the organic phase liquid after the hydrolysis with an aqueous solution of sulfuric acid with a concentration of 30% by weight or more is at least carried out.
摘要翻译： 可以容易且有效地获得高质量的3,4-二氢-1,2,3-氧杂噻嗪-4-酮-2,2-二氧化物或其盐。 当由下式（2）[式2]（其中，R1，R2和R3是氢原子或对反应惰性的有机基团，X是氢原子）表示的化合物或其盐是通过环化 的由下式（1）[式1]表示的β-酮酰胺-N-磺酸或其盐和惰性溶剂和酸酐与惰性溶剂的混合物的混合物，然后通过产物水解 通过与水溶液中的硫酸水溶液混合后水解得到的反应产物水解后的水相中，将水解产生的反应产物水解成为30重量％以上， 有机相和水相的步骤，或者（B）用浓度为30重量％以上的硫酸水溶液进行水解后的有机相液体的洗涤至少进行。
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2.发明申请METHOD FOR PRODUCING 3,4-DIHYDRO-1,2,3-OXATHIAZIN-4-ONE-2,2-DIOXIDE COMPOUND OR SALT THEREOF 失效生产3,4-二氢-1,2,3-氧杂环辛烷-4-酮-2,2-二氧化物或其盐的方法公开(公告)号：US20090318685A1
公开(公告)日：2009-12-24
申请号：US12373922
申请日：2007-08-02
申请人： Akira Saito , Yuki Ishiguro , Yasushi Yamamoto
发明人： Akira Saito , Yuki Ishiguro , Yasushi Yamamoto
IPC分类号： C07D291/06
CPC分类号： C07D291/06
摘要： A high quality 3,4-dihydro-1,2,3-oxathiazin-4-one-2,2-dioxide compound or a salt thereof is obtained easily and efficiently.When the compound represented by the following formula (2) (wherein, R1, R2, and R3 are hydrogen atom or an organic group inert to the reaction, and X is hydrogen atom) or a salt thereof is produced by cyclization of a mixture of β-ketoamide-N-sulfonic acid represented by the following formula (1) or a salt thereof and an inert solvent and a mixture of acid anhydride and an inert solvent, and by subsequent hydrolysis of the product, a step of (A) hydrolyzing the reaction product obtained by the cyclization by mixing with an aqueous solution of sulfuric acid so as a concentration of sulfuric acid in an aqueous phase after the hydrolysis would become 30% by weight or more, and then separating an organic phase and an aqueous phase, or a step of (B) washing the organic phase liquid after the hydrolysis with an aqueous solution of sulfuric acid with a concentration of 30% by weight or more is at least carried out.
摘要翻译： 可以容易且有效地获得高质量的3,4-二氢-1,2,3-氧杂噻嗪-4-酮-2,2-二氧化物或其盐。 当下式（2）表示的化合物（其中，R1，R2和R3为氢原子或对反应为惰性的有机基团，X为氢原子）或其盐时，通过使 由下式（1）表示的β-酮酰胺-N-磺酸或其盐和惰性溶剂以及酸酐和惰性溶剂的混合物，随后水解产物，（A）水解 通过与硫酸水溶液在水解后的水相中与硫酸的浓度混合而获得的反应产物将成为30重量％以上，然后分离有机相和水相， 或（B）用浓度为30重量％以上的硫酸水溶液进行水解后的有机相液体洗涤的工序至少进行。
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公开(公告)号：US08858735B2
公开(公告)日：2014-10-14
申请号：US13147510
申请日：2010-02-01
申请人： Masaaki Kondo , Shinichi Suzuki , Toshimasa Tomokiyo , Koichi Nishizawa , Takayuki Suzuki , Yuki Ishiguro , Hideyuki Kai
发明人： Masaaki Kondo , Shinichi Suzuki , Toshimasa Tomokiyo , Koichi Nishizawa , Takayuki Suzuki , Yuki Ishiguro , Hideyuki Kai
CPC分类号： C21D8/0278 , C21D1/673 , C21D2221/00 , C23C2/06 , C23C2/28
摘要： A high-strength quenched formed article has a zinc plating layer which is formed at a post-quenching formed steel sheet surface, and which contains 30 g/m2 or more of a phase that contains 5% or more by mass but 30% or less by mass of Fe, and which also contains 0.15% or more by mass but less than 2% by mass of at least one of Al and Si in a separate fashion or a composite fashion, and contains Zn, which makes up substantially a rest portion of the zinc plating layer, and an inevitable impurity, wherein the high-strength quenched formed article has a high-strength portion having a post-quenching-formation tensile strength of 1000 MPa or more, and a low-strength portion having a post-quenching-formation tensile strength of 800 MPa or less.
摘要翻译： 高强度淬火成型体具有在后淬火成形钢板表面形成的镀锌层，其含有30g / m 2以上含有5质量％以上且30质量％以下的相 的Fe，并且其还含有0.15％以上且小于2质量％的Al和Si中的至少一种，以单独的方式或复合形式，并且含有Zn，其基本上构成休止部分 的镀锌层和不可避免的杂质，其中高强度骤冷成形体具有淬火后形成抗拉强度为1000MPa以上的高强度部分， 淬火形成抗拉强度在800MPa以下。
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公开(公告)号：US20100285328A1
公开(公告)日：2010-11-11
申请号：US12811222
申请日：2009-05-14
摘要： A current density changing portion is formed in a heating process on an upper base side with respect to a center portion of a flat metal plate in a direction of current flow, by passing current from a lower base side to the upper base side of the flat metal plate which is rectangular when viewed from above. As a result, a quenchable portion is formed on the upper base side with respect to the center portion of the flat metal plate in the direction of current flow, and a non-quenchable portion is formed on the lower base side with respect to the center portion of the flat metal plate in the direction of current flow. The flat metal plate is press-formed after the heating process, so a complex die cooling structure is not necessary during press-forming, which enables the die cost to be reduced.
摘要翻译： 电流密度变化部分在电流流动方向上相对于平板状金属板的中心部分在上基底侧进行加热处理，通过使电流从下基底侧向平底部的上基底侧 从上方看矩形的金属板。 结果，在电流流动方向上相对于平板状金属板的中心部分的上基部侧形成有淬火部，相对于中心在下基部侧形成非淬火部 平坦金属板的一部分在电流方向上。 在加热过程之后压制平板金属板，因此在压制成型期间不需要复杂的模具冷却结构，从而能够降低模具成本。
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公开(公告)号：US20110303328A1
公开(公告)日：2011-12-15
申请号：US13147510
申请日：2010-02-01
申请人： Masaaki Kondo , Shinichi Suzuki , Toshimasa Tomokiyo , Koichi Nishizawa , Takayuki Suzuki , Yuki Ishiguro , Hideyuki Kai
发明人： Masaaki Kondo , Shinichi Suzuki , Toshimasa Tomokiyo , Koichi Nishizawa , Takayuki Suzuki , Yuki Ishiguro , Hideyuki Kai
CPC分类号： C21D8/0278 , C21D1/673 , C21D2221/00 , C23C2/06 , C23C2/28
摘要： A high-strength quenched formed article has a zinc plating layer which is formed at a post-quenching formed steel sheet surface, and which contains 30 g/m2 or more of a phase that contains 5% or more by mass but 30% or less by mass of Fe, and which also contains 0.15% or more by mass but less than 2% by mass of at least one of Al and Si in a separate fashion or a composite fashion, and contains Zn, which makes up substantially a rest portion of the zinc plating layer, and an inevitable impurity, wherein the high-strength quenched formed article has a high-strength portion having a post-quenching-formation tensile strength of 1000 MPa or more, and a low-strength portion having a post-quenching-formation tensile strength of 800 MPa or less.
摘要翻译： 高强度淬火成型体具有在后淬火成形钢板表面形成的镀锌层，其含有30g / m 2以上含有5质量％以上且30质量％以下的相 的Fe，并且其还含有0.15％以上且小于2质量％的Al和Si中的至少一种，以单独的方式或复合形式，并且含有Zn，其基本上构成休止部分 的镀锌层和不可避免的杂质，其中高强度骤冷成形体具有淬火后形成抗拉强度为1000MPa以上的高强度部分， 淬火形成抗拉强度在800MPa以下。
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公开(公告)号：US09003857B2
公开(公告)日：2015-04-14
申请号：US12811222
申请日：2009-05-14
摘要： A current density changing portion is formed in a heating process on an upper base side with respect to a center portion of a flat metal plate in a direction of current flow, by passing current from a lower base side to the upper base side of the flat metal plate which is rectangular when viewed from above. As a result, a quenchable portion is formed on the upper base side with respect to the center portion of the flat metal plate in the direction of current flow, and a non-quenchable portion is formed on the lower base side with respect to the center portion of the flat metal plate in the direction of current flow. The flat metal plate is press-formed after the heating process, so a complex die cooling structure is not necessary during press-forming, which enables the die cost to be reduced.
摘要翻译： 电流密度变化部分在电流流动方向上相对于平板状金属板的中心部分在上基底侧进行加热处理，通过使电流从下基底侧向平底部的上基底侧 从上方看矩形的金属板。 结果，在电流流动方向上相对于平板状金属板的中心部分的上基部侧形成有淬火部，相对于中心在下基部侧形成非淬火部 平坦金属板的一部分在电流方向上。 在加热过程之后压制平板金属板，因此在压制成型期间不需要复杂的模具冷却结构，从而能够降低模具成本。
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