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1.发明授权Electrochemical method and apparatus for producing and separating ferrate (VI) compounds 失效用于生产和分离高铁酸盐（VI）化合物的电化学方法和装置公开(公告)号：US06946078B2
公开(公告)日：2005-09-20
申请号：US10084020
申请日：2002-02-27
申请人： Zoran Minevski , Jason Maxey , Carl Nelson , Dylan Taylor
发明人： Zoran Minevski , Jason Maxey , Carl Nelson , Dylan Taylor
CPC分类号： C25B15/00 , C22B3/22 , C25B1/00 , Y02P10/234
摘要： The method for separating ferrate salts from a solution comprising providing contact between the solution of essentially of aqueous hydroxide and the ferrate salts and a surface having a magnetic attraction, magnetically securing the ferrate salts to the surface; and eliminating contact between the solution and the surface. Contact is provided by immersing the surface in the solution, passing the liquid ferrate mixture over the surface, or combinations thereof. The magnetic attraction may be induced by permanent magnets, electromagnets, and combinations thereof. The apparatus for ferrate production comprises an electrochemical cell having an iron-containing anode, cathode, and an aqueous hydroxide solution in fluid communication with both the anode and the cathode, and a magnetic separator in fluid communication with the aqueous hydroxide solution for separating ferrate salts from the aqueous hydroxide solution.
摘要翻译： 从溶液中分离高铁酸盐的方法，包括提供基本上氢氧化物水溶液与高铁酸盐之间的接触和具有磁吸引力的表面，将铁酸盐盐磁性地固定到表面; 并消除溶液与表面之间的接触。 通过将表面浸入溶液中，使液体高铁酸盐混合物通过表面或其组合来提供接触。 磁吸引可以由永磁体，电磁体及其组合引起。 用于高铁酸盐生产的装置包括具有含铁阳极，阴极和与阳极和阴极流体连通的氢氧化物水溶液的电化学电池，以及与用于分离铁酸盐的氢氧化物水溶液流体连通的磁选机 从氢氧化钠水溶液中。
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2.发明授权公开(公告)号：US06500276B1
公开(公告)日：2002-12-31
申请号：US09464284
申请日：1999-12-15
申请人： Zoran Minevski , Cahit Eylem , Jason Maxey , Carl Nelson
发明人： Zoran Minevski , Cahit Eylem , Jason Maxey , Carl Nelson
IPC分类号： C23C2248
摘要： The present invention provides a conversion coating solution containing polymetalates and/or heteropolymetalates to oxidize the surface of various metal substrates. The polymetalates have the general formula MxOyn−, where M is selected from the group comprising Mo, V and W. The heteropolymetalates have the general formula BMxOyn−, where B is a heteroatom selected from P, Si, Ce, Mn or Co, and M is again selected from Mo, V, W or combinations thereof. The concentration of polymetalates and/or heteropolymetalates anions is preferably between about 1% and about 5% by weight. Examples of typical anions used include, but are not limited to, (PMo12O40)3−, (PMo10V2O40)5−, (MnPW11O39)5−, (PW12O40)3−, (SiMo12O40)4−, (SiW12O40)4−, (Mo7O24)6−, (CeMo7O24)8−and mixtures thereof.
摘要翻译： 本发明提供一种含有多金属酸盐和/或杂多金属酸盐以氧化各种金属基材表面的转化涂层溶液。 多金属酸盐具有通式MxOyn-，其中M选自Mo，V和W组。杂多金属盐具有通式BMxOyn-，其中B是选自P，Si，Ce，Mn或Co的杂原子，以及 M再次选自Mo，V，W或其组合。 聚金属酸盐和/或杂多金属酸盐阴离子的浓度优选为约1重量％至约5重量％之间。 使用的典型阴离子的实例包括但不限于（PMo 12 O 40）3，（PMO 10 V 2 O 40）5，（MnPW 11 O 39）5，（PW 12 O 40）3，（SiMo 12 O 40）4，（SiW 12 O 40）4，（ Mo 7 O 24）6，（CeMo 7 O 24）8 - 及其混合物。
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公开(公告)号：US07045051B2
公开(公告)日：2006-05-16
申请号：US10084029
申请日：2002-02-27
申请人： Zoran Minevski , Jason Maxey , Carl Nelson , Dylan Taylor
发明人： Zoran Minevski , Jason Maxey , Carl Nelson , Dylan Taylor
IPC分类号： C25B1/00
摘要： A method for the electrochemical production of ferrate salts in an aqueous electrolyte solution comprising one or more hydroxide components. Dramatically increased yields of ferrate salts are obtained from using a mixture of sodium hydroxide and potassium hydroxide. Preferably, both sodium hydroxide and potassium hydroxide are present in concentrations greater than 5 molar, most preferably at least 10 molar, i.e., 10 M NaOH and 10 M KOH. The anode is preferably a sacrificial anode made out of an iron-containing material to supply the iron necessary for the ferrate production reaction. The aqueous hydroxide solution, even a mixed potassium hydroxide (KOH) and sodium hydroxide (NaOH) solution, may be recycled and reused in the electrochemical cell, preferably after the extraction of the ferrate salt
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公开(公告)号：US20080257200A1
公开(公告)日：2008-10-23
申请号：US11940116
申请日：2007-11-14
IPC分类号： C09D5/00
摘要： Composite coating compositions, composite metallic coatings derived from these compositions, and methods of forming the composite coating compositions and composite metallic coatings, wherein the compositions and coatings comprise particles of at least one quasicrystalline metal alloy and at least one elemental metal. The methods include electrocodepositing suspended quasicrystalline metal alloy particles and dissolved metal ions onto a substrate. Preferably, the substrate is disposed in an aqueous bath containing at least one dissolved metal ion species and at least one suspended quasicrystalline metal alloy powder species. The compositions and coatings enhance the wear, friction, hardness, corrosion, and non-stick characteristics of the substrate.
摘要翻译： 复合涂层组合物，衍生自这些组合物的复合金属涂层以及形成复合涂层组合物和复合金属涂层的方法，其中所述组合物和涂层包含至少一种准晶体金属合金和至少一种元素金属的颗粒。 所述方法包括将悬浮的准晶体金属合金颗粒和溶解的金属离子电沉积到基底上。 优选地，将基底设置在含有至少一种溶解的金属离子物质和至少一种悬浮的准晶体金属合金粉末物质的水浴中。 组合物和涂层增强了基材的磨损，摩擦，硬度，腐蚀和不粘特性。
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公开(公告)号：US07309412B2
公开(公告)日：2007-12-18
申请号：US10824183
申请日：2004-04-12
摘要： Composite coating compositions, composite metallic coatings derived from these compositions, and methods of forming the composite coating compositions and composite metallic coatings, wherein the compositions and coatings comprise particles of at least one quasicrystalline metal alloy and at least one elemental metal. The methods include electrocodepositing suspended quasicrystalline metal alloy particles and dissolved metal ions onto a substrate. Preferably, the substrate is disposed in an aqueous bath containing at least one dissolved metal ion species and at least one suspended quasicrystalline metal alloy powder species. The compositions and coatings enhance the wear, friction, hardness, corrosion, and non-stick characteristics of the substrate.
摘要翻译： 复合涂层组合物，衍生自这些组合物的复合金属涂层以及形成复合涂层组合物和复合金属涂层的方法，其中所述组合物和涂层包含至少一种准晶体金属合金和至少一种元素金属的颗粒。 所述方法包括将悬浮的准晶体金属合金颗粒和溶解的金属离子电沉积到基底上。 优选地，将基底设置在含有至少一种溶解的金属离子物质和至少一种悬浮的准晶体金属合金粉末物质的水浴中。 组合物和涂层增强了基材的磨损，摩擦，硬度，腐蚀和不粘特性。
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公开(公告)号：US20070267289A1
公开(公告)日：2007-11-22
申请号：US11696354
申请日：2007-04-04
申请人： Harry Jabs , Daniel Westerheim , Brian Hennings , Daniel Soekamto , Surya Shandy , Zoran Minevski , Alan Cisar
发明人： Harry Jabs , Daniel Westerheim , Brian Hennings , Daniel Soekamto , Surya Shandy , Zoran Minevski , Alan Cisar
IPC分类号： B01J12/00
CPC分类号： B01J19/088 , B01J2219/0809 , B01J2219/0815 , B01J2219/0818 , B01J2219/082 , B01J2219/083 , B01J2219/0832 , B01J2219/0841 , B01J2219/0869 , B01J2219/0877 , B01J2219/0892 , B01J2219/0894 , C01B3/22 , C01B2203/0861 , H05H1/48
摘要： Hydrogen gas production includes supplying a hydrocarbon fluid to a gap between a pair of electrodes, applying a voltage across the electrodes to induce an electrical arc, wherein the electrical arc contacts the hydrocarbon to form a plasma and produces a gaseous product comprising hydrogen gas and a solid product comprising carbon, and dynamically adjusting the gap length to control at least one parameter of the plasma. Preferably, the gap length is decreased during plasma initiation or reformation and increased to increase the hydrogen gas production rate. The method preferably includes dynamically adjusting the spatial separation of the electrodes and rotating at least one electrode while generating hydrogen gas to reduce adherence of solids to the electrodes. Furthermore, the polarity of the electrodes may be periodically reversed, primarily to reduce adherence of solids. If the hydrocarbon fluid is a liquid, the method may include controlling the level of the hydrocarbon liquid relative to the pair of electrodes.
摘要翻译： 氢气生产包括向一对电极之间的间隙供应烃流体，在电极之间施加电压以引起电弧，其中电弧与烃接触以形成等离子体并产生包含氢气和 包含碳的固体产物，并且动态地调整间隙长度以控制等离子体的至少一个参数。 优选地，间隙长度在等离子体引发或改性期间减小并且增加以提高氢气产生速率。 该方法优选地包括动态地调节电极的空间分离并旋转至少一个电极同时产生氢气以减少固体对电极的粘附。 此外，电极的极性可以周期性地反转，主要是为了减少固体的粘附。 如果烃流体是液体，则该方法可以包括控制烃液体相对于该对电极的水平。
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7.发明申请Electrochemical method and apparatus for producing and separating ferrate(VI) compounds 失效用于生产和分离高铁酸盐（VI）化合物的电化学方法和装置公开(公告)号：US20050201912A1
公开(公告)日：2005-09-15
申请号：US11116486
申请日：2005-04-28
申请人： Zoran Minevski , Jason Maxey , Carl Nelson , Dylan Taylor
发明人： Zoran Minevski , Jason Maxey , Carl Nelson , Dylan Taylor
CPC分类号： C25B15/00 , C22B3/22 , C25B1/00 , Y02P10/234
摘要： The method for separating ferrate salts from a solution comprising providing contact between the solution of essentially of aqueous hydroxide and the ferrate salts and a surface having a magnetic attraction, magnetically securing the ferrate salts to the surface; and eliminating contact between the solution and the surface. Contact is provided by immersing the surface in the solution, passing the liquid ferrate mixture over the surface, or combinations thereof. The magnetic attraction may be induced by permanent magnets, electromagnets, and combinations thereof. The apparatus for ferrate production comprises an electrochemical cell having an iron-containing anode, cathode, and an aqueous hydroxide solution in fluid communication with both the anode and the cathode, and a magnetic separator in fluid communication with the aqueous hydroxide solution for separating ferrate salts from the aqueous hydroxide solution
摘要翻译： 从溶液中分离高铁酸盐的方法，包括提供基本上氢氧化物水溶液与高铁酸盐之间的接触和具有磁吸引力的表面，将铁酸盐盐磁性地固定到表面; 并消除溶液与表面之间的接触。 通过将表面浸入溶液中，使液体高铁酸盐混合物通过表面或其组合来提供接触。 磁吸引可以由永磁体，电磁体及其组合引起。 用于高铁酸盐生产的装置包括具有含铁阳极，阴极和与阳极和阴极流体连通的氢氧化物水溶液的电化学电池，以及与用于分离铁酸盐的氢氧化物水溶液流体连通的磁选机 从氢氧化钠水溶液中
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8.发明授权公开(公告)号：US06863743B2
公开(公告)日：2005-03-08
申请号：US10331963
申请日：2002-12-30
申请人： Zoran Minevski , Cahit Eylem , Jason Maxey , Carl Nelson
发明人： Zoran Minevski , Cahit Eylem , Jason Maxey , Carl Nelson
IPC分类号： C23C20060101 , C23C2/00 , C23C22/07 , C23C22/40 , C23C22/42 , C23C22/44 , C23C22/48 , C23C22/60 , C23C22/62 , C23C22/66
摘要： The present invention provides a conversion coating solution containing polymetalates and/or heteropolymetalates to oxidize the surface of various metal substrates. The polymetalates have the general formula MxOyn−, where M is selected from the group comprising Mo, V and W. The heteropolymetalates have the general formula BMxOyn−, where B is a heteroatom selected from P, Si, Ce, Mn or Co, and M is again selected from Mo, V, W or combinations thereof. The concentration of polymetalates and/or heteropolymetalates anions is preferably between about 1% and about 5% by weight. Examples of typical anions used include, but are not limited to, (PMo12O40)3−, (PMo10V2O40)5−, (MnPW11O39)5−, (PW12O40)3−, (SiMo12O40)4−, (SiW12O40)4−, (Mo7O24)6−, (CeMo12O42)8− and mixtures thereof.
摘要翻译： 本发明提供一种含有多金属酸盐和/或杂多金属酸盐以氧化各种金属基材表面的转化涂层溶液。 多金属酸盐具有通式M x O y n，其中M选自Mo，V和W组。杂多金属盐具有通式BM x O y n，其中B是选自P，Si，Ce的杂原子 ，Mn或Co，M再次选自Mo，V，W或其组合。 聚金属酸盐和/或杂多金属酸盐阴离子的浓度优选为约1重量％至约5重量％之间。 使用的典型阴离子的实例包括但不限于（PMo 12 O 40）3，（PMO 10 V 2 O 40）5，（MnPW 11 O 39）5，（PW 12 O 40）3 - ，（SiMo 12 O 40）4 - ，（SiW12O40）4，（Mo7O24）6 - ，（CeMo12O42）<8->及其混合物。
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9.发明授权Electrochemical method and apparatus for producing and separating ferrate(VI) compounds 失效用于生产和分离高铁酸盐（VI）化合物的电化学方法和装置公开(公告)号：US07314552B2
公开(公告)日：2008-01-01
申请号：US11116486
申请日：2005-04-28
申请人： Zoran Minevski , Jason Maxey , Carl Nelson , Dylan Taylor
发明人： Zoran Minevski , Jason Maxey , Carl Nelson , Dylan Taylor
CPC分类号： C25B15/00 , C22B3/22 , C25B1/00 , Y02P10/234
摘要： The method for separating ferrate salts from a solution comprising providing contact between the solution of essentially of aqueous hydroxide and the ferrate salts and a surface having a magnetic attraction, magnetically securing the ferrate salts to the surface; and eliminating contact between the solution and the surface. Contact is provided by immersing the surface in the solution, passing the liquid ferrate mixture over the surface, or combinations thereof. The magnetic attraction may be induced by permanent magnets, electromagnets, and combinations thereof. The apparatus for ferrate production comprises an electrochemical cell having an iron-containing anode, cathode, and an aqueous hydroxide solution in fluid communication with both the anode and the cathode, and a magnetic separator in fluid communication with the aqueous hydroxide solution for separating ferrate salts from the aqueous hydroxide solution.
摘要翻译： 从溶液中分离高铁酸盐的方法，包括提供基本上氢氧化物水溶液与高铁酸盐之间的接触和具有磁吸引力的表面，将铁酸盐盐磁性地固定到表面; 并消除溶液与表面之间的接触。 通过将表面浸入溶液中，使液体高铁酸盐混合物通过表面或其组合来提供接触。 磁吸引可以由永磁体，电磁体及其组合引起。 用于高铁酸盐生产的装置包括具有含铁阳极，阴极和与阳极和阴极流体连通的氢氧化物水溶液的电化学电池，以及与用于分离铁酸盐的氢氧化物水溶液流体连通的磁选机 从氢氧化钠水溶液中。
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公开(公告)号：US06471788B1
公开(公告)日：2002-10-29
申请号：US09461944
申请日：1999-12-15
申请人： Zoran Minevski , Jason Maxey , Carl Nelson , Cahit Eylem
发明人： Zoran Minevski , Jason Maxey , Carl Nelson , Cahit Eylem
IPC分类号： C23C2248
摘要： A method employing oxide film conversion coatings prepared using ferrate (VI) as the oxidizing agent is disclosed. Metal substrates or surfaces, such as aluminum, aluminum alloys or other metals, are contacted with an aqueous solution comprising ferrate (VI) anions to form a corrosion resistant conversion coating on the surface thereof. The ferrate anion concentration is preferably between about 0.0166% and about 1.66% by weight. The coating process is carried out by dipping, spraying, or painting at temperatures ranging from 25° C. to 100° C. for a period of time ranging from about 1 second to about 5 minutes.
摘要翻译： 公开了使用高铁酸盐（VI）作为氧化剂制备氧化膜转化膜的方法。 将金属基材或诸如铝，铝合金或其它金属的表面与包含高铁酸盐（VI）阴离子的水溶液接触，以在其表面上形成耐腐蚀转化膜。 高铁酸盐阴离子浓度优选为约0.0166重量％至约1.66重量％。 涂覆过程通过在25℃至100℃的温度范围内浸渍，喷涂或涂漆进行约1秒至约5分钟的时间。
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