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1.发明授权公开(公告)号：US06692714B2
公开(公告)日：2004-02-17
申请号：US10338136
申请日：2003-01-08
Applicant: Suresh Shankarappa Vagarali , Steven William Webb , William Edwin Jackson , William Frank Banholzer , Thomas Richard Anthony , George Rene Kaplan
Inventor： Suresh Shankarappa Vagarali , Steven William Webb , William Edwin Jackson , William Frank Banholzer , Thomas Richard Anthony , George Rene Kaplan
IPC: C01B3106
CPC classification number: B01J3/06 , B01J3/062 , B01J2203/062 , B01J2203/0655 , B01J2203/0695 , C30B29/04 , C30B33/00
Abstract: The present invention is directed to a method for changing the color of colored natural diamonds. The method includes placing a discolored natural diamond in a pressure-transmitting medium which is consolidated into a pill. Next, the pill is placed into a high pressure/high temperature (HP/HT) press at elevated pressure and elevated temperature for a time sufficient to improve the color of the diamond. The diamond may be exposed at elevated-pressure and elevated-temperature conditions within the graphite-stable region of the carbon-phase diagram—without significant graphitization of the diamond, or above the diamond-graphite equilibrium and within the diamond-stable region of the carbon-phase diagram. Finally, the diamond is recovered from said press. Colorless Type Ia and Type II diamonds may be made by this method.
Abstract translation: 本发明涉及一种改变有色天然钻石颜色的方法。 该方法包括将变色的天然金刚石置于压力传递介质中，将其固结成丸剂。 接下来，将药丸置于高压/高温（HP / HT）压机中，在高压和升高的温度下，足以改善金刚石的颜色。 金刚石可以在碳相图的石墨稳定区域内的高压和高温条件下暴露，没有金刚石的显着石墨化，或高于金刚石 - 石墨平衡，并且在金刚石稳定区域内 碳相图。 最后，从所述印刷机中回收钻石。 可以通过该方法制造无色Ia型和II型金刚石。
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公开(公告)号：US07175704B2
公开(公告)日：2007-02-13
申请号：US10455007
申请日：2003-06-05
Applicant: Mark Philip D'Evelyn , Thomas Richard Anthony , Stephen Daley Arthur , Lionel Monty Levinson , John William Lucek , Larry Burton Rowland , Suresh Shankarappa Vagarali
Inventor： Mark Philip D'Evelyn , Thomas Richard Anthony , Stephen Daley Arthur , Lionel Monty Levinson , John William Lucek , Larry Burton Rowland , Suresh Shankarappa Vagarali
IPC: C30B7/10
CPC classification number: B01J3/065 , B01J3/062 , B01J2203/0635 , B01J2203/0645 , B01J2203/066 , B01J2203/0665 , B01J2203/067 , B01J2203/0675 , B01J2203/069 , C30B33/00 , Y10T117/1004 , Y10T117/1008
Abstract: A method for removing defects at high pressure and high temperature (HP/HT) or for relieving strain in a non-diamond crystal commences by providing a crystal, which contains defects, and a pressure medium. The crystal and the pressure medium are disposed in a high pressure cell and placed in a high pressure apparatus, for processing under reaction conditions of sufficiently high pressure and high temperature for a time adequate for one or more of removing defects or relieving strain in the single crystal.
Abstract translation: 通过提供含有缺陷的晶体和压力介质，开始在高压高温（HP / HT）下除去非金刚石晶体中的缺陷或解除应变的方法。 将晶体和压力介质设置在高压电池中并放置在高压设备中，用于在足够高的压力和高温的反应条件下进行处理足够的时间以适应一个或多个去除缺陷或减轻单一应变的应变 水晶。
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公开(公告)号：US06908674B2
公开(公告)日：2005-06-21
申请号：US09799192
申请日：2001-03-05
Applicant: Suresh Shankarappa Vagarali , Thomas Richard Anthony , John Casey , Robert Charles DeVries , Stephen Lee Dole , John William Lucek , Alan Cameron Smith , Biju Varghese , Steven William Webb
Inventor： Suresh Shankarappa Vagarali , Thomas Richard Anthony , John Casey , Robert Charles DeVries , Stephen Lee Dole , John William Lucek , Alan Cameron Smith , Biju Varghese , Steven William Webb
CPC classification number: C01B33/26 , B01J3/062 , B01J2203/068 , C01B33/20 , Y10T428/2982 , Y10T428/2996
Abstract: A jadeite material has a thickness in excess of about 1.0 mm and CIELAB indices of L*>42, a* +6. The grain size of the jadeite material is less than about 30 microns and is an equiaxed grain structure. The jadeite material has an optical transmission peak between 500 and 565 nm with an I/IO optical transmission ratio of over 40%. The first step in making the jadeite material is to wrap a glass block, convertible by HP/HT into jadeite and having a nominal composition of NaAlSi2O6, with a graphite or refractive metal sheet. The wrapped glass block is placed in an HP/HT apparatus, rapidly heated, and subjected therein to a pressure in excess of about 3 GPa and a temperature in excess of about 1000° C. for a time adequate to convert the glass block into jadeite. The jadeite material then is cooled and the pressure subsequently released.
Abstract translation: 翡翠材料的厚度超过约1.0mm，CIELAB指数L *> 42，a * <-6和b *> + 6。 翡翠材料的晶粒尺寸小于约30微米，是等轴晶粒结构。 翡翠材料具有在500和565nm之间的光传输峰值，其中I / I / O光透射率超过40％。 制造翡翠材料的第一步是将玻璃块包裹，由HP / HT转化为翡翠，并具有标称组成的NaAlSi 2 O 6 6，与石墨 或折射金属片。 将包裹的玻璃块放置在HP / HT装置中，快速加热，并在其中进行超过约3GPa的压力和超过约1000℃的温度，足以将玻璃块转化成翡翠 。 然后将翡翠材料冷却并随后释放压力。
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公开(公告)号：US08216370B2
公开(公告)日：2012-07-10
申请号：US11300660
申请日：2005-12-12
Applicant: Mark Philip D'Evelyn , Thomas Richard Anthony , Stephen Daley Arthur , Lionel Monty Levinson , John William Lucek , Larry Burton Rowland , Suresh Shankarappa Vagarali
Inventor： Mark Philip D'Evelyn , Thomas Richard Anthony , Stephen Daley Arthur , Lionel Monty Levinson , John William Lucek , Larry Burton Rowland , Suresh Shankarappa Vagarali
IPC: C30B21/04
CPC classification number: B01J3/065 , B01J3/062 , B01J2203/0635 , B01J2203/0645 , B01J2203/066 , B01J2203/0665 , B01J2203/067 , B01J2203/0675 , B01J2203/069 , C30B33/00 , Y10T117/1004 , Y10T117/1008
Abstract: A method for removing defects at high pressure and high temperature (HP/HT) or for relieving strain in a non-diamond crystal commences by providing a crystal, which contains defects, and a pressure medium. The crystal and the pressure medium are disposed in a high pressure cell and placed in a high pressure apparatus, for processing under reaction conditions of sufficiently high pressure and high temperature for a time adequate for one or more of removing defects or relieving strain in the single crystal.
Abstract translation: 通过提供含有缺陷的晶体和压力介质，开始在高压高温（HP / HT）下除去非金刚石晶体中的缺陷或解除应变的方法。 将晶体和压力介质设置在高压电池中并放置在高压设备中，用于在足够高的压力和高温的反应条件下进行处理足够的时间以适应一个或多个去除缺陷或减轻单一应变的应变 水晶。
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Patent Agency Ranking
5.发明授权High temperature high pressure capsule for processing materials in supercritical fluids 有权用于加工超临界流体材料的高温高压胶囊公开(公告)号：US07625446B2
公开(公告)日：2009-12-01
申请号：US11010139
申请日：2004-12-10
Applicant: Mark Philip D'Evelyn , Kristi Jean Narang , Robert Arthur Giddings , Steven Alfred Tysoe , John William Lucek , Suresh Shankarappa Vagarali , Robert Vincent Leonelli, Jr. , Joel Rice Dysart
Inventor： Mark Philip D'Evelyn , Kristi Jean Narang , Robert Arthur Giddings , Steven Alfred Tysoe , John William Lucek , Suresh Shankarappa Vagarali , Robert Vincent Leonelli, Jr. , Joel Rice Dysart
CPC classification number: B01J3/008 , B01J3/062 , B01J19/02 , B01J2203/0665 , B01J2219/00777 , B01J2219/0236 , B01J2219/024 , C30B7/10 , C30B9/00 , C30B29/40 , C30B29/406 , Y02P20/544 , Y10T117/10 , Y10T117/1004 , Y10T117/1024 , Y10T117/108 , Y10T117/1092
Abstract: A capsule for containing at least one reactant and a supercritical fluid in a substantially air-free environment under high pressure, high temperature processing conditions. The capsule includes a closed end, at least one wall adjoining the closed end and extending from the closed end; and a sealed end adjoining the at least one wall opposite the closed end. The at least one wall, closed end, and sealed end define a chamber therein for containing the reactant and a solvent that becomes a supercritical fluid at high temperatures and high pressures. The capsule is formed from a deformable material and is fluid impermeable and chemically inert with respect to the reactant and the supercritical fluid under processing conditions, which are generally above 5 kbar and 550° C. and, preferably, at pressures between 5 kbar and 80 kbar and temperatures between 550 ° C. and about 1500° C. The invention also includes methods of filling the capsule with the solvent and sealing the capsule, as well as an apparatus for sealing the capsule.
Abstract translation: 一种用于在高压，高温处理条件下在基本无空气环境中含有至少一种反应物和超临界流体的胶囊。 所述胶囊包括封闭端，邻近所述封闭端并从所述封闭端延伸的至少一个壁; 以及与所述封闭端相对的所述至少一个壁相邻的密封端。 至少一个壁，封闭端和密封端在其中限定一个室，用于容纳反应物和在高温和高压下成为超临界流体的溶剂。 胶囊由可变形材料形成，并且在加工条件下相对于反应物和超临界流体是流体不可渗透和化学惰性的，其通常高于5kbar和550℃，并且优选在5kbar和80kPa之间的压力 kbar和550℃至约1500℃之间的温度。本发明还包括用溶剂填充胶囊并密封胶囊的方法以及用于密封胶囊的装置。
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公开(公告)号：US07125453B2
公开(公告)日：2006-10-24
申请号：US09683659
申请日：2002-01-31
Applicant: Mark Philip D'Evelyn , Kristi Jean Narang , Robert Arthur Giddings , Steven Alfred Tysoe , John William Lucek , Suresh Shankarappa Vagarali , Robert Vincent Leonelli, Jr. , Joel Rice Dysart
Inventor： Mark Philip D'Evelyn , Kristi Jean Narang , Robert Arthur Giddings , Steven Alfred Tysoe , John William Lucek , Suresh Shankarappa Vagarali , Robert Vincent Leonelli, Jr. , Joel Rice Dysart
IPC: C30B7/10
CPC classification number: B01J3/008 , B01J3/062 , B01J19/02 , B01J2203/0665 , B01J2219/00777 , B01J2219/0236 , B01J2219/024 , C30B7/10 , C30B9/00 , C30B29/40 , C30B29/406 , Y02P20/544 , Y10T117/10 , Y10T117/1004 , Y10T117/1024 , Y10T117/108 , Y10T117/1092
Abstract: A capsule for containing at least one reactant and a supercritical fluid in a substantially air-free environment under high pressure, high temperature processing conditions. The capsule includes a closed end, at least one wall adjoining the closed end and extending from the closed end; and a sealed end adjoining the at least one wall opposite the closed end. The at least one wall, closed end, and sealed end define a chamber therein for containing the reactant and a solvent that becomes a supercritical fluid at high temperatures and high pressures. The capsule is formed from a deformable material and is fluid impermeable and chemically inert with respect to the reactant and the supercritical fluid under processing conditions, which are generally above 5 kbar and 550° C. and, preferably, at pressures between 5 kbar and 80 kbar and temperatures between 550° C. and about 1500° C. The invention also includes methods of filling the capsule with the solvent and sealing the capsule, as well as an apparatus for sealing the capsule.
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7.发明授权公开(公告)号：US07323156B2
公开(公告)日：2008-01-29
申请号：US10737541
申请日：2003-12-15
Applicant: Suresh Shankarappa Vagarali , Steven William Webb , William Edwin Jackson , William Frank Banholzer , Thomas Richard Anthony , George Rene Kaplan
Inventor： Suresh Shankarappa Vagarali , Steven William Webb , William Edwin Jackson , William Frank Banholzer , Thomas Richard Anthony , George Rene Kaplan
CPC classification number: B01J3/06 , B01J3/062 , B01J2203/062 , B01J2203/0655 , B01J2203/0695 , C30B29/04 , C30B33/00
Abstract: The present invention is directed to a method for changing the color of colored natural diamonds. The method includes placing a discolored natural diamond in a pressure-transmitting medium which is consolidated into a pill. Next, the pill is placed into a high pressure/high temperature (HP/HT) press at elevated pressure and elevated temperature for a time sufficient to improve the color of the diamond. The diamond may be exposed at elevated-pressure and elevated-temperature conditions within the graphite-stable region of the carbon-phase diagram—without significant graphitization of the diamond, or above the diamond-graphite equilibrium and within the diamond-stable region of the carbon-phase diagram. Finally, the diamond is recovered from said press. Colorless Type Ia and Type II diamonds may be made by this method.
Abstract translation: 本发明涉及一种改变有色天然钻石颜色的方法。 该方法包括将变色的天然金刚石置于压力传递介质中，将其固结成丸剂。 接下来，将药丸置于高压/高温（HP / HT）压机中，在高压和升高的温度下，足以改善金刚石的颜色。 金刚石可以在碳相图的石墨稳定区域内的高压和高温条件下暴露，没有金刚石的显着石墨化，或高于金刚石 - 石墨平衡，并且在金刚石稳定区域内 碳相图。 最后，从所述印刷机中回收钻石。 可以通过该方法制造无色Ia型和II型金刚石。
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公开(公告)号：US07063741B2
公开(公告)日：2006-06-20
申请号：US10063164
申请日：2002-03-27
Applicant: Mark Philip D'Evelyn , Steven William Webb , Suresh Shankarappa Vagarali , Yavuz Kadioglu , Dong-Sil Park , Zheng Chen
Inventor： Mark Philip D'Evelyn , Steven William Webb , Suresh Shankarappa Vagarali , Yavuz Kadioglu , Dong-Sil Park , Zheng Chen
IPC: C30B9/12
CPC classification number: C30B29/403 , B82Y10/00 , B82Y30/00 , C30B7/00 , C30B9/00 , C30B29/406 , Y10T117/1052 , Y10T117/1096
Abstract: A method of forming at least one single crystal of a Group III metal nitride. The method includes the steps of: providing a flux material and a source material comprising at least one Group III metal selected from the group consisting of aluminum, indium, and gallium, to a reaction vessel; sealing the reaction vessel; heating the reaction vessel to a predetermined temperature and applying a predetermined pressure to the vessel. The pressure is sufficient to suppress decomposition of the Group III metal nitride at the temperature. Group III metal nitrides, as well as electronic devices having a Group III metal nitride substrate formed by the method are also disclosed.
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9.发明授权公开(公告)号：US06377340B1
公开(公告)日：2002-04-23
申请号：US09430477
申请日：1999-10-29
Applicant: Thomas Richard Anthony , John Kieran Casey , Alan Cameron Smith , Suresh Shankarappa Vagarali
Inventor： Thomas Richard Anthony , John Kieran Casey , Alan Cameron Smith , Suresh Shankarappa Vagarali
IPC: G01N2100
CPC classification number: G01N21/64 , G01N21/87 , G01N2021/6417
Abstract: A method for detecting whether a natural diamond has been processed at high pressure and high temperature (HPHT) conditions comprises steps of disposing the diamond in a cyrostat that is provided at temperatures equal to or less than liquid nitrogen; illuminating the diamond with a laser beam; recording an optical spectrum of the diamond with a photoluminescence spectrometer; and examining the optical spectrum of the diamond to detect an absence of selected photoluminescent spectral lines. The invention also sets forth a method for predicting whether a natural diamond has been treated under HPHT conditions
Abstract translation: 一种用于检测天然金刚石是否已经在高压和高温（HPHT）条件下被处理的方法包括将金刚石设置在等于或小于液氮的温度下的冷冻机中的步骤; 用激光束照射金刚石; 用光致发光光谱仪记录金刚石的光谱; 并检查金刚石的光谱以检测不存在所选择的光致发光光谱线。 本发明还提出了一种用于预测天然金刚石是否已经在HPHT条件下进行处理的方法
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