PROCESS FOR THE DISTILLATION OF FATTY ACID ESTERS
    1.
    发明申请
    PROCESS FOR THE DISTILLATION OF FATTY ACID ESTERS 有权
    消毒脂肪酸酯的方法

    公开(公告)号:US20130331588A1

    公开(公告)日:2013-12-12

    申请号:US14000443

    申请日:2012-03-03

    IPC分类号: C07C67/54 C07C69/587

    摘要: The present invention relates to a method for working up a mixture which contains esters of EPA and/or DHA with monohydric alcohols having 1 to 6 carbon atoms, esters of other fatty acids with monohydric alcohols having 1 to 6 carbon atoms, and free cholesterol, wherein the method comprises adding a transesterification catalyst to the mixture, converting at least some of the free cholesterol into esterified cholesterol and thereafter distilling the mixture, wherein the distillation is carried out in such a manner that a product is obtained which contains EPA and/or DHA, both in the form of esters thereof with monohydric alcohols having 1 to 6 carbon atoms, in a higher relative amount, based on all fatty acids in free or bound form present in the product, than said mixture. In addition, the present invention relates to a product which is obtainable by the method according to the invention, wherein the product contains 10 to 99.99% by weight of esters of EPA and/or of DHA with monohydric alcohols having 1 to 6 carbon atoms and 0.0001 to a maximum of 0.3% by weight of cholesterol in free or bound form.

    摘要翻译: 本发明涉及一种用于处理含有EPA和/或DHA的酯与具有1至6个碳原子的一元醇的混合物的混合物的方法,其它脂肪酸与具有1至6个碳原子的一元醇的酯和游离胆固醇, 其中所述方法包括向所述混合物中加入酯交换催化剂,将至少一些游离胆固醇转化为酯化胆固醇,然后蒸馏混合物,其中蒸馏是以获得含有EPA和/或 DHA,以其与具有1至6个碳原子的一元醇的酯的形式,以相对于所述混合物中存在的游离或结合形式的所有脂肪酸的相对量较高。 另外本发明涉及通过本发明的方法获得的产品,其中该产品含有10至99.99重量%的EPA和/或DHA的酯与具有1至6个碳原子的一元醇的酯和 0.0001至最大0.3重量%的游离或结合形式的胆固醇。

    Water-dispersable sterol containing dispersions
    2.
    发明授权
    Water-dispersable sterol containing dispersions 有权
    含水分散剂的分散体

    公开(公告)号:US08399042B2

    公开(公告)日:2013-03-19

    申请号:US12746626

    申请日:2008-11-28

    IPC分类号: A23D7/00

    摘要: The invention relates to aqueous dispersions containing (a) 5 to 50% by weight of sterols and/or stanols; and (b) 0.5 to 20% by weight of citric acid esters of mono- and/or diglycerides, based on the total weight of the dispersion, wherein the citric acid esters of mono- and/or diglycerides are partially neutralised; and to a process for the production of an aqueous sterol/stanol-containing dispersion, which process comprises (a) dissolving citric acid esters of mono- and/or diglycerides that are partly neutralised, in water; (b) dispersing sterols and/or stanols in the emulsifier solution to form a pre-dispersion; and (c) grinding the pre-dispersion in a ball-mill until the dispersion has a particle mass diameter, d90, of less than 5 μm. Optionally, this dispersion is spray-dried.

    摘要翻译: 本发明涉及含有(a)5至50重量%的甾醇和/或甾醇的水分散体; 和(b)基于分散体总重量的0.5至20重量%的甘油单酯和/或甘油二酯的柠檬酸酯,其中甘油单酯和/或甘油二酯的柠檬酸酯部分中和; 以及生产含水甾醇/含Stanol的分散体的方法,该方法包括(a)将部分中和的甘油单酯和/或甘油二酯的柠檬酸酯溶解在水中; (b)将甾醇和/或甾醇分散在乳化剂溶液中以形成预分散体; 和(c)在球磨机中研磨预分散体,直到分散体具有小于5μm的颗粒质量直径d 90。 任选地,将该分散体喷雾干燥。

    Oxidative Stabilizing of Sterols and Sterol Esters
    3.
    发明申请
    Oxidative Stabilizing of Sterols and Sterol Esters 审中-公开
    甾醇和甾醇酯的氧化稳定

    公开(公告)号:US20100260913A1

    公开(公告)日:2010-10-14

    申请号:US12747939

    申请日:2008-12-04

    IPC分类号: A23L3/3481

    摘要: The invention relates to a method for the production of oxidation-stable sterol formulations, wherein catechins and/or the derivatives thereof are added to the sterols or sterol esters, and to the formulations produced according to said method. The catechins are preferably used in an amount of 20 to 1000 ppm, based on the sterol or on the sterol ester. Green tea extract may be incorporated as the catechin formulation. The formulations containing sterols produced according to said method have very high oxidative stability and have no displeasing aftertaste.

    摘要翻译: 本发明涉及生产氧化稳定的甾醇制剂的方法,其中将儿茶素和/或其衍生物加入到甾醇酯或甾醇酯中,以及根据所述方法制备的制剂。 基于甾醇或甾醇酯,儿茶素优选以20至1000ppm的量使用。 可以将绿茶提取物作为儿茶素制剂掺入。 含有根据所述方法生产的甾醇的制剂具有非常高的氧化稳定性并且没有不愉快的回味。

    Processes for the production of triglycerides of conjugated linoleic acid
    5.
    发明授权
    Processes for the production of triglycerides of conjugated linoleic acid 失效
    用于生产共轭亚油酸的甘油三酯的方法

    公开(公告)号:US07067684B2

    公开(公告)日:2006-06-27

    申请号:US11013834

    申请日:2004-12-16

    IPC分类号: C11C3/00

    CPC分类号: C11C3/10

    摘要: Processes for preparing conjugated linoleic acid triglycerides are described which comprise: (a) providing a conjugated linoleic acid alkyl ester, wherein the alkyl group is linear or branched and has from 1 to 5 carbon atoms; and (b) subjecting conjugated linoleic acid alkyl ester to transesterification with triacetin to provide a conjugated linoleic acid triglyceride.

    摘要翻译: 描述了制备共轭亚油酸甘油三酸酯的方法,其包括:(a)提供共轭亚油酸烷基酯,其中烷基是直链或支链并具有1至5个碳原子; 和(b)使共轭亚油酸烷基酯与三醋精进行酯交换以提供共轭亚油酸甘油三酸酯。

    DEVICE AND METHOD FOR DISTILLING TEMPERATURE-SENSITIVE SUBSTANCES
    8.
    发明申请
    DEVICE AND METHOD FOR DISTILLING TEMPERATURE-SENSITIVE SUBSTANCES 审中-公开
    用于蒸馏温度敏感物质的装置和方法

    公开(公告)号:US20130292242A1

    公开(公告)日:2013-11-07

    申请号:US13879040

    申请日:2011-09-23

    IPC分类号: B01D3/14

    CPC分类号: B01D3/148 B01D1/065

    摘要: The present invention relates to an apparatus for the distillation of substance mixtures which comprise temperature-sensitive substances, where the apparatus comprises a thin-film evaporator and a fractionating column, and where the fractionating column is attached to the distillate outlet of the thin-film evaporator, and where the fractionating column has at least 3 theoretical plates, and where the pressure drop of the fractionating column during operation at an F factor of 1 Pa1/2 amounts to a maximum of 3 hPa (3 mbar). Furthermore, the present invention relates to a process for the distillation of substance mixtures which comprise temperature-sensitive substances, which process is carried out in the apparatus according to the invention.

    摘要翻译: 本发明涉及一种用于蒸馏含有温度敏感物质的物质混合物的装置,其中该装置包括薄膜蒸发器和分馏塔,并且其中分馏塔连接到薄膜的馏出物出口 蒸发器,并且分馏塔具有至少3个理论塔板,并且其中在F因子为1Pa 1/2的操作期间分馏塔的压降达到最大3hPa(3mbar)。 此外,本发明涉及蒸馏含有温度敏感物质的物质混合物的方法,该方法在根据本发明的设备中进行。

    Processes for the production of triglycerides of unsaturated fatty acids in the presence of enzymes
    10.
    发明授权
    Processes for the production of triglycerides of unsaturated fatty acids in the presence of enzymes 有权
    在酶存在下生产不饱和脂肪酸甘油三酸酯的方法

    公开(公告)号:US07981641B2

    公开(公告)日:2011-07-19

    申请号:US12061005

    申请日:2008-04-02

    IPC分类号: C12P7/64 C08L91/00

    CPC分类号: C12P7/6472

    摘要: Processes for the enzyme-catalyzed production of triglycerides using polyunsaturated fatty acids, in which (a) the reaction of polyunsaturated fatty acids and/or C1-4 alkyl esters thereof with glycerol in vacuo in the presence of an immobilized enzyme to form their triglycerides is accelerated by addition of an additive from the group of weakly basic salts, complexing agents and ion exchangers and/or addition of a weakly basic salt and/or addition of an entraining agent in the form of a solvent or a gas and/or addition of glycerol-binding adsorbers and/or heat treatment of the partial glyceride intermediate product, (b) the immobilized enzymes are removed from the triglyceride by separation or filtration and (c) the remaining fatty acids and/or C1-4 alkyl esters thereof are removed from the triglyceride by distillation, refining or extraction.

    摘要翻译: 使用多不饱和脂肪酸进行酶催化生产甘油三酸酯的方法,其中(a)在固定化酶存在下,多不饱和脂肪酸和/或其中C 1-4烷基酯与甘油在真空中反应形成其甘油三酸酯的方法是 通过加入来自弱碱性盐,络合剂和离子交换剂的添加剂和/或加入弱碱性盐和/或以溶剂或气体的形式加入夹带剂和/或添加 甘油结合吸附剂和/或热处理部分甘油酯中间产物,(b)通过分离或过滤从甘油三酯中除去固定化的酶,和(c)除去剩余的脂肪酸和/或其中的C 1-4烷基酯 从甘油三酯通过蒸馏,精制或提取。