公开(公告)号：US07544233B2

公开(公告)日：2009-06-09

申请号：US10554162

申请日：2004-04-28

Applicant: Frank Diedrich ,  Friedhelm Müller

Inventor： Frank Diedrich ,  Friedhelm Müller

IPC: B01D53/02

CPC classification number: H01J49/0422 ,  G01N30/7206 ,  G01N30/78 ,  G01N2030/025 ,  G01N30/66

Abstract: The aim of the invention is to optimize the analysis of substances separated by gas chromatography with a gas chromatograph, comprising a separating device and a mass spectrometer situated down there from. To this end, a detector that detects the separated substances in a nondestructive manner is placed in-line between the output of the separating device and a controllable inlet valve of the mass spectrometer. An evaluating device situated down from the detector evaluates the detector signals and, based on the evaluation, controls the inlet valve for introducing predeterminable substances into the mass spectrometer.

Abstract translation: 本发明的目的是通过气相色谱法优化气相色谱分离物质的分析，其中包括分离装置和位于其下的质谱仪。 为此，以非破坏性方式检测分离的物质的检测器被放置在分离装置的输出和质谱仪的可控入口阀之间。 从检测器向下定位的评估装置对检测器信号进行评估，并且基于评估，控制用于将可预定物质引入质谱仪的入口阀。

公开(公告)号：US06454840B1

公开(公告)日：2002-09-24

申请号：US09763157

申请日：2001-05-01

Applicant: Udo Gellert ,  Friedhelm Müller ,  Arno Steckenborn

Inventor： Udo Gellert ,  Friedhelm Müller ,  Arno Steckenborn

IPC: B01D1508

CPC classification number: G01N30/6095 ,  G01N30/6086 ,  G01N2030/025 ,  Y10S55/05

Abstract: A separation-column unit includes a support plate having a groove formed therein on one side and running, for example, in the form of a spiral, and having a cover plate which bears against this side. In order to achieve the high separation capacity combined with a high load-bearing capacity with regard to the amount of sample flowing through, the depth (d) of the groove is preferably at least three times greater than its width. The base of the groove preferably has a rounded cross section, it being possible for the cover plate to contain a corresponding channel.

Abstract translation: 分离柱单元包括支撑板，该支撑板在一侧形成有槽，并且以例如螺旋状的形式运行，并且具有抵靠该侧的盖板。 为了实现高的分离能力，结合相对于流过的样品的高的承载能力，槽的深度（d）优选为其宽度的至少三倍。 槽的底部优选地具有圆形横截面，盖板可以包含相应的通道。