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    Process for stabilizing hypophosphite salts
    2.
    发明授权
    Process for stabilizing hypophosphite salts 有权
    稳定次磷酸盐的方法

    公开(公告)号：US08883901B2

    公开(公告)日：2014-11-11

    申请号：US13392304

    申请日：2009-08-24

    申请人： Floryan De Campo ,  Annelyse Murillo ,  Junli Li ,  Tingting Zhang

    发明人： Floryan De Campo ,  Annelyse Murillo ,  Junli Li ,  Tingting Zhang

    IPC分类号： C08K3/32 ,  C09K21/04 ,  C01B25/165

    CPC分类号： C09K21/04 ,  C01B25/165 ,  C08K3/32

    摘要： The current invention relates to a process for stabilizing a hypophosphite salt, comprising the step of heating the hypophosphite salt at a temperature of between 150 and 370° C. during a sufficient period of time to prevent the formation of a dangerous quantity of phosphine in their application as FR in polymers and a flame retardant polymer composition comprising a polymer and 0.1 to 30 weight percent based on the total weight of the composition of the hypophosphite salt thermally stabilized by the above process.

    摘要翻译： 本发明涉及一种稳定次磷酸盐的方法，包括在足够的时间段内在150-370℃的温度下加热次磷酸盐以防止在其中形成危险量的磷化氢的步骤 作为聚合物中的FR的应用和包含聚合物的阻燃聚合物组合物和基于通过上述方法热稳定的次磷酸盐组合物的总重量的0.1-30重量％。

    Systems and methods for evaluating asphaltene deposition inhibitors
    4.
    发明授权
    Systems and methods for evaluating asphaltene deposition inhibitors 失效
    评估沥青质沉积抑制剂的系统和方法

    公开(公告)号：US08584513B2

    公开(公告)日：2013-11-19

    申请号：US12932386

    申请日：2011-02-24

    申请人： Lawrence A. Hough ,  Jean-Christophe Castaing ,  Gary Woodward ,  Ruela Talingting Pabalan ,  Floryan De Campo

    发明人： Lawrence A. Hough ,  Jean-Christophe Castaing ,  Gary Woodward ,  Ruela Talingting Pabalan ,  Floryan De Campo

    IPC分类号： G01N33/26

    CPC分类号： G01N33/26 ,  B01L3/5027 ,  G01N21/82

    摘要： Disclosed are methods of determining the effectiveness of an asphaltene deposition inhibitor in oilfield applications. Such methods typically comprising the steps of introducing an oil well fluid into a microfluidic/millifluidic system; introducing a mixture of an asphaltene deposition inhibitor and carrier into the microfluidic/millifluidic system; introducing a precipitating agent, typically comprising heptane, into the microfluidic/millifluidic system; and optionally introducing toluene into the microfluidic/millifluidic system; then observing the presence or absence of asphaltene aggregation within the microfluidic/millifluidic system.

    摘要翻译： 公开了确定沥青质沉积抑制剂在油田应用中的有效性的方法。 这些方法通常包括将油井流体引入微流体/微流体系统的步骤; 将沥青质沉积抑制剂和载体的混合物引入到微流体/微流体系统中; 将典型地包含庚烷的沉淀剂引入到微流体/微流体系统中; 并任选地将甲苯引入微流体/微流体系统中; 然后观察微流体/微流体系统内沥青质聚集的存在或不存在。

    PROCESS FOR THE PREPARATION OF HIGHLY PURIFIED, DIALKYL PHOSPHINIC ACIDS
    5.
    发明申请
    PROCESS FOR THE PREPARATION OF HIGHLY PURIFIED, DIALKYL PHOSPHINIC ACIDS 有权
    制备高纯度的二磷酸磷酸的方法

    公开(公告)号：US20060089508A1

    公开(公告)日：2006-04-27

    申请号：US11256704

    申请日：2005-10-24

    申请人： Shiming Wo ,  Floryan De Campo

    发明人： Shiming Wo ,  Floryan De Campo

    IPC分类号： C07F9/28 ,  C07F9/22

    CPC分类号： C07F9/301

    摘要： In a process for the production of dialkylphosphinic acids, especially branched, dialkylphosphinic acids in high purity via the reaction of an alpha olefin with a hypophosphorous acid or a salt thereof, the improvement comprising conducting the reaction in the presence of a stoichiometric excess of the olefin and isolating and purifying the desired dialkylphosphinic acid product by neutralizing the monoalkylphosphinic acid by-product with an aqueous base; removing the aqueous phase in which the neutralized monoalkylphosphinic acid is preferentially solubilized; acidifying the dialkyl product in the organic phase; and isolating the purified product.

    摘要翻译： 在通过α-烯烃与次亚磷酸或其盐的反应生产二烷基次膦酸，特别是具有高纯度的支链二烷基次膦酸的方法中，改进包括在化学计量过量的烯烃存在下进行反应 并通过用碱水溶液中和单烷基次膦酸副产物来分离和纯化所需的二烷基次膦酸产物; 除去中和的单烷基次膦酸优先溶解的水相; 在有机相中酸化二烷基产物; 并分离纯化的产物。

    Process for preparing an ortho-substituted 5-halophenol and a synthesis intermediate thereof
    7.
    发明授权
    Process for preparing an ortho-substituted 5-halophenol and a synthesis intermediate thereof 有权
    制备邻位取代的5-卤代苯酚的方法及其合成中间体

    公开(公告)号：US08975431B2

    公开(公告)日：2015-03-10

    申请号：US13698985

    申请日：2010-05-19

    申请人： Claude Mercier ,  Floryan De Campo ,  Sébastien Righini

    发明人： Claude Mercier ,  Floryan De Campo ,  Sébastien Righini

    IPC分类号： C07C309/75 ,  C07C41/01 ,  C07C303/28 ,  C07C41/26 ,  C07C303/30

    CPC分类号： C07C303/28 ,  C07C41/26 ,  C07C303/30 ,  C07C309/66 ,  C07C43/23

    摘要： A process for preparing a 5-halophenol, ortho-substituted by an electron-donating group, is described. Also described, is a process for preparing a sulphonic ester of an ortho-substituted phenol, which is the synthesis intermediate for the ortho-substituted 5-halophenol. The process for preparing a phenol ortho-substituted by an electron-donating group and protected in the form of a sulphonic ester can include reacting a phenol ortho-substituted by an electron-donating group with a sulphonylating agent in the presence of a Lewis acid. The process for preparing a 5-halophenol ortho-substituted by an electron-donating group can include a first step of preparing a phenol ortho-substituted by an electron-donating group and protected in the form of a sulphonic ester, as described above; a second step of halogenating the protected phenol intermediate obtained in the preceding step, in the position para to the electron-donating group; and a third step of deprotecting the sulphonic ester function to hydroxyl.

    摘要翻译： 描述了由给电子基团取代的5-卤代苯酚的制备方法。 还描述的是制备邻位取代的苯酚的磺酸酯的方法，其为邻位取代的5-卤代苯酚的合成中间体。 制备由供电子基团取代并以磺酸酯形式保护的苯酚的方法可以包括在路易斯酸存在下将由供电子基团邻位取代的苯酚与磺酰化剂反应。 制备由给电子基团取代的5-卤代苯酚的方法可以包括如上所述制备被供电子基团邻位取代并以磺酸酯形式保护的苯酚的第一步骤; 将前述步骤中获得的被保护的苯酚中间体卤化到给电子基团的对位的第二步骤; 以及将磺酸酯功能脱保护成羟基的第三步骤。

    New coupling agents for elastomer compositions
    8.
    发明申请
    New coupling agents for elastomer compositions 审中-公开
    用于弹性体组合物的新型偶联剂

    公开(公告)号：US20140135450A1

    公开(公告)日：2014-05-15

    申请号：US14114020

    申请日：2012-04-28

    申请人： Zhaoqing Liu ,  Floryan De Campo ,  Laurent Guy ,  David James Wilson ,  Philippe Jost

    发明人： Zhaoqing Liu ,  Floryan De Campo ,  Laurent Guy ,  David James Wilson ,  Philippe Jost

    IPC分类号： C08F8/40

    CPC分类号： C08F8/40 ,  C08F36/14 ,  C08K5/5313 ,  C08K5/5317 ,  C08K5/5333 ,  C08L21/00 ,  C08L7/00

    摘要： In an elastomer composition, which preferably comprises an isoprene elastomer, use of an inorganic filler with a compound having the following formula (I), and which is optionally, in all or part, in a polymerized form: wherein R is R6 or OR8; wherein R1, R2, R3, R4, R5, and R6, independently from each other, are chosen from: hydrogen, alkyl, aryl, alkaryl, aralkyl, cycloalkyl, heterocycloalkyl, and alkenyl groups; and wherein R7 and R8, independently from each other, are chosen from: hydrogen, alkyl, aryl, alkaryl, aralkyl, cycloalkyl, alkenyl groups, and metals selected from the group consisting of Na, Li, and Ca.

    摘要翻译： 在优选包含异戊二烯弹性体的弹性体组合物中，使用无机填料与具有下式（I）的化合物，并且任选地全部或部分地以聚合形式：其中R是R6或OR8; 其中R1，R2，R3，R4，R5和R6彼此独立地选自：氢，烷基，芳基，烷芳基，芳烷基，环烷基，杂环烷基和烯基; 其中R 7和R 8彼此独立地选自：氢，烷基，芳基，烷芳基，芳烷基，环烷基，烯基和选自Na，Li和Ca的金属。

    N-SUBSTITUTED ACRYLAMIDES, PREPARATION METHOD AND USE THEREOF
    10.
    发明申请
    N-SUBSTITUTED ACRYLAMIDES, PREPARATION METHOD AND USE THEREOF 有权
    N-取代的丙烯酰胺，其制备方法和用途

    公开(公告)号：US20120202958A1

    公开(公告)日：2012-08-09

    申请号：US13502853

    申请日：2009-10-30

    申请人： Zhaoqing Liu ,  Floryan De Campo

    发明人： Zhaoqing Liu ,  Floryan De Campo

    IPC分类号： C07F9/38 ,  C08F30/02

    CPC分类号： C08K5/5353 ,  C07F9/3826

    摘要： This invention relates to new monomers prepared from phosphorus-containing diene monomers and (meth)acrylonitrile via Ritter reactions, and the preparation method thereof. The polymer of these monomers can be utilized in various applications such as water treatment, rheology modifier, surface modification, etc. The monomers have the following structure (II), Wherein R1, R2, R3, R4, R5, R6and R7 represent, independently, hydrogen, alkyl, aryl, alkaryl, aralkyl, cycloalkyl, heterocycloalkyl, or alkenyl groups; R6 and R7 represents R9O, and R10 respectively wherein R9 and R10 represents hydrogen, alkyl, aryl, alkaryl, aralkyl, cycloalkyl, alkenyl groups, or metals selected from the group consisting of Na, Li, Ca; Rs represents H, or CH3.

    摘要翻译： 本发明涉及通过Ritter反应由含磷二烯单体和（甲基）丙烯腈制备的新单体及其制备方法。 这些单体的聚合物可用于各种应用中，例如水处理，流变改性剂，表面改性等。单体具有以下结构（II）：其中R1，R2，R3，R4，R5，R6和R7独立地表示 ，氢，烷基，芳基，烷芳基，芳烷基，环烷基，杂环烷基或烯基; R 6和R 7分别表示R9和R 10，其中R 9和R 10表示氢，烷基，芳基，烷芳基，芳烷基，环烷基，烯基或选自Na，Li，Ca的金属; Rs表示H或CH3。