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公开(公告)号：US5922916A
公开(公告)日：1999-07-13
申请号：US058827
申请日：1998-04-13
申请人： Heather Lynnette Rayle , Renee Caroline Roemmele , Randall Wayne Stephens , Joshua Anthony Chong , Fereydon Abdesaken , Charles Chao Wu
发明人： Heather Lynnette Rayle , Renee Caroline Roemmele , Randall Wayne Stephens , Joshua Anthony Chong , Fereydon Abdesaken , Charles Chao Wu
IPC分类号： C07D213/82 , A01N37/18 , B01J27/122 , C07B39/00 , C07B61/00 , C07C221/00 , C07C225/06 , C07C225/10 , C07C231/02 , C07C233/31 , C07C233/61 , C07C233/76 , C07C209/36
CPC分类号： C07C221/00
摘要： The present invention relates to a process for preparing 5-methylene cyclic carbamates either by cyclization of an alkynyl amine with carbon dioxide in the presence of a copper catalyst or by forming an isocyanate from a substituted acetoacetamide followed by hydrolysis. The 5-methylene cyclic carbamates by either method are converted to 5-(chloromethylene) cyclic carbamates, using trichloroisocyanuric acid, followed by hydrolysis to a chloroketoamine.The chloroketoamine from the process of this invention additionally can be reacted with an organic acid chloride to form an amide compound which is useful as a fungicide.
摘要翻译： 本发明涉及一种通过在铜催化剂存在下使炔基胺与二氧化碳环化或通过由取代的乙酰乙酰胺形成异氰酸酯然后水解制备5-亚甲基环状氨基甲酸酯的方法。 通过任一方法将5-亚甲基环状氨基甲酸酯转化为5-（氯亚甲基）环状氨基甲酸酯，使用三氯异氰脲酸，然后水解成氯酮胺。 本发明方法的氯代胺胺另外可以与有机酰氯反应形成可用作杀真菌剂的酰胺化合物。
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公开(公告)号：US5688742A
公开(公告)日：1997-11-18
申请号：US516841
申请日：1995-08-18
CPC分类号： B01J2/06
摘要： A method for preparing a dust-free beaded product from a low melting material is disclosed. The method is particularly applicable to manufacturing processes in which the last step in preparation of a product is a water wash step.
摘要翻译： 公开了一种从低熔点材料制备无尘珠粒产品的方法。 该方法特别适用于制备产品的最后步骤是水洗步骤的制造方法。
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公开(公告)号：US06307094B1
公开(公告)日：2001-10-23
申请号：US09564656
申请日：2000-05-02
申请人： Joshua Anthony Chong , Fereydon Abdesaken , Lori Ann Spangler , Renee Caroline Roemmele , Randall Wayne Stephens , Peter David Nightingale , David John Hartley
发明人： Joshua Anthony Chong , Fereydon Abdesaken , Lori Ann Spangler , Renee Caroline Roemmele , Randall Wayne Stephens , Peter David Nightingale , David John Hartley
IPC分类号： C07C6963
CPC分类号： C07C67/31 , C07C69/675
摘要： The present invention provides a solventless process for the catalytic hydrogenation of esters of 4,4,4-trihaloacetoacetic acid using a platinum catalyst in the presence of an acid or base co-catalyst to provide the analagous 3-hydroxybutyrate ester. Such 3-hydroxybutyrate esters are useful as solvents, cleaners or fine chemical intermediates.
摘要翻译： 本发明提供了一种在酸或碱助催化剂存在下使用铂催化剂催化氢化4,4,4-三卤乙酰乙酸酯的无溶剂方法，以提供分离的3-羟基丁酸酯。 这种3-羟基丁酸酯可用作溶剂，清洁剂或精细化学中间体。
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公开(公告)号：US6124500A
公开(公告)日：2000-09-26
申请号：US218571
申请日：1998-12-22
申请人： Joshua Anthony Chong , Fereydon Abdesaken , Lori Ann Spangler , Sudhir Ramtirth Joshi , Charles Chao Wu
发明人： Joshua Anthony Chong , Fereydon Abdesaken , Lori Ann Spangler , Sudhir Ramtirth Joshi , Charles Chao Wu
IPC分类号： C07C51/15 , C07C51/367 , C07C51/58 , C07C65/03 , C07C65/21 , C07C67/08 , C07C69/07 , C07C69/157 , C07C69/24
CPC分类号： C07C51/367 , C07C51/15 , C07C51/58 , C07C67/08
摘要： A nucleophilic substitution reaction on optionally substituted dihalobenzenes is carried out in the presence of an optional catalyst followed by formation of and subsequent carboxylation of a Grignard reaction intermediate. In particular the present invention provides a process leading to optionally substituted hydroxybenzoic, alkanoyloxybenzoic, formyloxybenzoic and alkoxybenzoic acids from 1-substituted 2,6-dihalobenzenes. The invention also provides a process for the direct formation of an acyl chloride from a Grignard reagent by quenching with phosgene.
摘要翻译： 任选取代的二卤代苯的亲核取代反应在任选的催化剂存在下进行，然后形成和随后的格利雅反应中间体羧化。 特别地，本发明提供一种从1-取代的2,6-二卤代苯衍生的任选取代的羟基苯甲酸，烷酰氧基苯甲酸，甲酰氧基苯甲酸和烷氧基苯甲酸的方法。 本发明还提供了通过用光气淬灭从格氏试剂直接形成酰氯的方法。
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公开(公告)号：US06278015B1
公开(公告)日：2001-08-21
申请号：US09617381
申请日：2000-07-17
IPC分类号： C07C6963
CPC分类号： C07C327/22 , C07C67/14 , C07C69/63
摘要： The present invention provides a process for preparing esters or thioesters of trifluoroacetic acid from trifluoroacetyl chloride and an alcohol or a thiol with the ester or thioester being present as the solvent. Esters and thioesters of trifluoroacetic acid are fine chemical intermediates which can be used in the manufacture of pharmaceuticals, agricultural chemicals, liquid crystals, dyes and industrial chemicals. Trifluoroacetate esters and thioesters can also be used as solvents in the manufacture of other fine chemicals, pharmaceuticals, agricultural chemicals, liquid crystals, industrial chemicals and dyes.
摘要翻译： 本发明提供从三氟乙酰氯和醇或硫醇制备三氟乙酸的酯或硫酯的方法，其中酯或硫酯作为溶剂存在。 三氟乙酸的酯和硫酯是精细化学中间体，可用于制药，农药，液晶，染料和工业化学品的制造。 三氟乙酸酯和硫酯也可用作制造其他精细化学品，药物，农药，液晶，工业化学品和染料的溶剂。
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公开(公告)号：US5965766A
公开(公告)日：1999-10-12
申请号：US017176
申请日：1998-02-02
IPC分类号： B01J27/122 , B01J27/128 , B01J27/26 , B01J31/24 , C07B61/00 , C07C41/16 , C07C43/225 , C07C51/08 , C07C51/347 , C07C51/367 , C07C65/03 , C07C67/08 , C07C253/14 , C07C253/30 , C07C255/53 , C07C255/54 , C07C253/00 , C07C65/01 , C07C69/00 , C07C255/00
CPC分类号： C07C51/08 , C07C253/14 , C07C51/347 , C07C51/367 , C07C67/08
摘要： Nucleophilic substitution reactions on halobenzenes or triflyl substituted benzenes are carried out in the presence of catalysts. In particular the present invention provides a process leading to optionally substituted hydroxybenzoic, alkanoyloxybenzoic, formyloxybenzoic and alkoxybenzoic acids and optionally substituted hydroxybenzonitriles and alkoxybenzonitriles from substituted 2,6-dihalobenzenes, 2-halo-6-triflylbenzene and 2,6-ditriflylbenzenes.
摘要翻译： 在卤代苯或三氟甲苯取代的苯上的亲核取代反应在催化剂存在下进行。 特别地，本发明提供了一种导致任选取代的羟基苯甲酸，烷酰氧基苯甲酸，甲酰氧基苯甲酸和烷氧基苯甲酸以及任选取代的羟基苯并腈和烷氧基苯腈从取代的2,6-二卤代苯，2-卤代-6-三氟苯和2,6-二硝基苯的方法。
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公开(公告)号：US5917079A
公开(公告)日：1999-06-29
申请号：US884193
申请日：1997-07-01
IPC分类号： B01J27/122 , B01J27/128 , B01J27/26 , B01J31/24 , C07B61/00 , C07C20060101 , C07C41/16 , C07C43/225 , C07C51/08 , C07C51/347 , C07C51/367 , C07C51/377 , C07C65/03 , C07C65/21 , C07C67/08 , C07C253/14 , C07C253/30 , C07C255/53 , C07C255/54 , C07C253/00 , C07C63/00 , C07C255/00
CPC分类号： C07C253/14 , C07C51/08 , C07C51/347 , C07C51/367
摘要： Nucleophilic substitution reactions on halobenzenes are carried out in the presence of catalysts. In particular the present invention provides a process leading to optionally substituted hydroxybenzoic and alkoxybenzoic acids and optionally substituted hydroxybenzonitriles and alkoxybenzonitriles from substituted 2,6-dihalobenzenes.
摘要翻译： 在卤代苯上的亲核取代反应在催化剂的存在下进行。 特别地，本发明提供了一种导致任选取代的羟基苯甲酸和烷氧基苯甲酸和任选取代的羟基苯腈和取代的2,6-二卤苯的烷氧基苯腈的方法。
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