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61.发明授权
公开(公告)号：US5451434A
公开(公告)日：1995-09-19
申请号：US158374
申请日：1993-11-29
申请人： Guenther Doellein
发明人： Guenther Doellein
CPC分类号： C07C49/92 , C07C45/77 , C23C16/404 , C23C16/408 , Y10S505/734
摘要： Alkaline earth metal heptane dionates which have uniform evaporation properties in a vacuum and are therefore highly suitable for use in CVD synthesis for depositing layers containing alkaline earth metal useful in fields such as the production of high temperature superconductors.
摘要翻译： 在真空中具有均匀蒸发性质的碱土金属庚烷二元酸盐，因此非常适用于CVD合成，用于沉积含有碱土金属的层，其可用于生产高温超导体等领域。
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公开(公告)号：US5248787A
公开(公告)日：1993-09-28
申请号：US533539
申请日：1990-06-05
IPC分类号： C07D323/00 , C07C45/77 , C07C49/167 , C07C209/68 , C07C211/03 , C07C211/09 , C07C231/12 , C07C233/03 , C07C315/04 , C07C317/04 , C07D213/22 , C07D471/10 , C07F3/00 , C23C16/30 , C23C16/40 , C30B25/02
CPC分类号： C23C16/404 , C07F3/003 , C23C16/30 , C23C16/408 , C30B25/02 , C30B29/22
摘要： Volatile organic barium, strontium and calcium compounds, which consist of the complex of a barium-, strontium- or calcium-.beta. diketonate and one or more coordinating ligands, characterized in that at least one coordinating ligand of the barium or strontium compound is formed by a neutral oxygen or a neutral nitrogen donor ligand, or one of the coordinating ligands of the calcium compound is formed by a neutral oxygen donor ligand.
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公开(公告)号：US4511515A
公开(公告)日：1985-04-16
申请号：US508602
申请日：1983-06-28
申请人： David A. Thompson
发明人： David A. Thompson
摘要： A method for the synthesis of tetrakis-(6,6,7,7,8,8,8,-heptafluoro-2,2-dimethyl-3,5-octanedione) cerium (IV), [Ce(fod).sub.4 ] wherein the product is directly formed by reacting the deprotonated beta-diketonate ligand with a cerium (IV) salt, is disclosed.
摘要翻译： 合成四（6,6,7,7,8,8,8- pt基-2,2-二甲基-3,5-辛二酮）铈（Ⅳ），〔Ce（fod）4〕〕的方法， 其中所述产物通过使脱质子化的β-二酮配体与铈（IV）盐反应直接形成。
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公开(公告)号：US4424165A
公开(公告)日：1984-01-03
申请号：US418216
申请日：1982-09-15
申请人： David A. Thompson
发明人： David A. Thompson
摘要： A volatile and thermally stable complex of cerium, Cd(fod).sub.4, and alkali metal-cerium .beta.-diketonate intermediates useful in its preparation and as sources of mixed metals, such as Na�Ce(fod).sub.4 !, are described.
摘要翻译： 描述了可用于其制备和作为混合金属如Na [Ce（fod）4]的来源的铈，Cd（fod）4和碱金属 - 铈β-二酮中间体的挥发性和热稳定的络合物。
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65.发明授权Palladium (II) bis(hexafluoroacetylacetonate), adducts derived therefrom and uses thereof 失效钯（II）双（六氟乙酰丙酮化物），由其衍生的加合物及其用途
公开(公告)号：US4410569A
公开(公告)日：1983-10-18
申请号：US351505
申请日：1982-02-23
申请人： Allen R. Siedle
发明人： Allen R. Siedle
IPC分类号： B01J23/44 , C02F5/12 , C02F5/14 , C07C45/77 , C07C49/92 , C07F15/00 , C23C18/18 , C23C18/30 , B05D3/04
CPC分类号： C23C18/30 , B01J23/44 , C02F5/12 , C02F5/14 , C07C45/77 , C07C49/92 , C07F15/0066 , C23C18/1865 , C23C18/1879
摘要： Preparation of palladium (II) bis(hexafluoracetylacetonate) and adducts derived therefrom are disclosed, said adducts having the formulaPd(F.sub.6 ACAC).sub.2.L.sub.nwherein L is a Lewis base selected from certain classes, and n is an integer from 1 to 4. These compounds are useful in preparing catalytic and primer surfaces of elemental palladium.
摘要翻译： 公开了双（六氟乙酰丙酮）钯（II）和由其衍生的加合物的制备，所述加合物具有式Pd（F6ACAC）2。
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66.发明授权Use of acyl trimethyl cyclohexene derivatives in augmenting or enhancing the organoleptic properties of smoking tobacco or smoking tobacco article 失效酰基三甲基环己烯衍生物在增强或增强吸烟烟草或烟草制品的感官特性方面的应用
公开(公告)号：US4289145A
公开(公告)日：1981-09-15
申请号：US156647
申请日：1980-06-05
申请人： Robert W. Trenkle , Braja D. Mookherjee , John B. Hall , Robin Kasper , Manfred H. Vock , Ronald Schreck , Edward J. Granda , Joaquin F. Vinals
发明人： Robert W. Trenkle , Braja D. Mookherjee , John B. Hall , Robin Kasper , Manfred H. Vock , Ronald Schreck , Edward J. Granda , Joaquin F. Vinals
IPC分类号： A23G3/00 , A23G3/36 , C07C29/42 , C07C29/68 , C07C45/51 , C07C45/62 , C07C45/64 , C07C45/66 , C07C45/72 , C07C45/77 , C07C49/92 , A24B3/12 , A24B15/30
CPC分类号： A23G3/36 , C07C29/42 , C07C29/68 , C07C45/51 , C07C45/62 , C07C45/64 , C07C45/66 , C07C45/72 , C07C45/77 , C07C49/92 , C07C2101/14
摘要： Described is a process for augmenting or enhancing the aroma or taste of a smoking tobacco comprising the step of adding to smoking tobacco an organoleptic property modifying amount of the compound having the structure: ##STR1##
摘要翻译： 描述了一种用于增强或增强烟草的香气或味道的方法，其包括向吸烟烟草中添加具有以下结构的化合物的感官特性修饰量的步骤：
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公开(公告)号：US4206139A
公开(公告)日：1980-06-03
申请号：US946110
申请日：1978-09-27
IPC分类号： C07C45/67 , C07C45/77 , C07C47/575 , C07C49/92 , C07C51/36 , C07C51/367 , C07C309/73 , C07F1/00 , C07F11/00 , G03C8/18 , C07C68/06 , C07C45/00 , G03C5/54
CPC分类号： G03C8/18 , C07C309/73 , C07C45/673 , C07C45/77 , C07C47/575 , C07C49/92 , C07C51/36 , C07C51/367 , C07F1/005 , C07F11/005 , Y02P20/55
摘要： Novel benzaldehydes of the formula: ##STR1## Where n.sup.1 is the integer 1-8 and each OR.sup.1 group is hydroxy or a protective group which can be converted or removed to provide the dihydroxyphenyl moiety.The benzaldehydes are particularly useful as intermediates in the preparation of yellow azomethine dye developers.
摘要翻译： 新的苯甲醛，其分子式如下：其中n1是整数1-8，每个OR1基团是羟基或可被转化或除去以提供二羟基苯基部分的保护基。 苯甲醛特别可用作制备黄色偶氮甲碱染料显影剂的中间体。
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公开(公告)号：US4020073A
公开(公告)日：1977-04-26
申请号：US471926
申请日：1974-05-21
CPC分类号： C07C49/92 , C07C45/455 , C07C45/68 , C07C45/77 , C07C51/56 , C07C67/14 , C07C67/343 , C07F5/069 , C07H19/16 , C07C2101/08
摘要： Thallous salts of .beta.-dicarbonyl compounds, prepared by reaction of the .beta.-dicarbonyl compounds with a thallous alkoxide, are treated with alkyl halides to give C-alkyl products in high yield, with acyl halides at room temperature to give C-acyl products, and with acyl halides at low temperatures to give O-acyl products. Thallous phenolates are esterified with acyl or aroyl halides. Anhydrides are also prepared, as are biaryls and bi-sec-alkyls. N-heterocyclics, including purines and pyrimidines, are N-alkylated. Lactams are O-acylated or N-alkylated.
摘要翻译： 通过β-二羰基化合物与铊醇盐反应制备的β-二羰基化合物的铊盐用烷基卤化物处理，以高产率与酰基卤在室温下反应得到C-酰基产物， 并在低温下与酰卤反应，得到O-酰基产物。 柠檬酸酚酯与酰基或芳酰基卤酯化。 还制备了酸酐，联芳基和双仲烷基也是如此。 N-杂环化合物，包括嘌呤和嘧啶，是N-烷基化的。 内酰胺是O-酰化或N-烷基化的。
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公开(公告)号：US4015980A
公开(公告)日：1977-04-05
申请号：US601765
申请日：1975-08-04
CPC分类号： C22B3/0021 , C07C45/455 , C07C49/80 , C07C49/92 , Y02P10/234
摘要： Zinc is extracted from aqueous ammoniacal solutions using fluorinated .beta.-diketones of the structure ##STR1## where n is a whole integer of 1 to 4, m is 0, 1 or 2 and R is an alkyl group of 1-25 carbons, the R group or groups providing requisite solubility in liquid hydrocarbon solvents.
摘要翻译： 使用结构“IMAGE”的氟化β-二酮从含水氨水溶液中提取锌，其中n为1至4的整数，m为0,1或2，R为1-25个碳原子的烷基，R 在液态烃溶剂中提供必需溶解度的基团或基团。
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公开(公告)号：US3950135A
公开(公告)日：1976-04-13
申请号：US491594
申请日：1974-07-24
IPC分类号： C07C45/45 , C07C45/77 , C07C49/297 , C07C49/313 , C07C49/92 , C07F5/00 , C01F17/00 , G01N27/78
CPC分类号： C07F5/003 , C07C45/455 , C07C49/297 , C07C49/313 , C07C49/92 , Y10T436/24
摘要： The ability of nuclear magnetic resonance spectroscopy to distinguish between compounds and between parts of compounds is substantially increased by the use of certain rare earth chelate shift reagents. The preferred shift reagents are the europium III chelates of substituted or unsubstituted dicampholyl ligands, and europium III chelates of substituted or unsubstituted nopinato compounds. The reagents are particularly useful in determining the enantiomeric purity of compositions containing mixtures of enantiomers.
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