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197 条记录 (耗时 0.018 秒)

    Process for preparation of organosilicon halides
    41.
    发明授权
    Process for preparation of organosilicon halides 失效
    有机硅卤化物的制备方法

    公开(公告)号：US5175331A

    公开(公告)日：1992-12-29

    申请号：US809430

    申请日：1991-12-18

    申请人： Won S. Park ,  William R. Beard

    发明人： Won S. Park ,  William R. Beard

    IPC分类号： C07F7/12

    CPC分类号： C07F7/122 ,  C07F7/123 ,  C07F7/125

    摘要： A process for preparing a silane mixture of the formulaSi R.sub.n X.sub.4-nwhere R is C.sub.1 to C.sub.12 linear or branched alkyl, phenyl or phenyl substituted with one or more C.sub.1 to C.sub.6 linear or branched alkyl; X is chloro, bromo or iodo; and n is an integer from 1 to 4; comprising reacting silicon tetrafluoride with metallic aluminum and RX, where R and X are as previously described, at a temperature of about 150.degree. C. to about 400.degree. C.

    摘要翻译： 制备式SiRnX4-n的硅烷混合物的方法，其中R是C1-C12直链或支链烷基，苯基或被一个或多个C1-C6直链或支链烷基取代的苯基; X是氯，溴或碘; n为1〜4的整数。 包括使四氟化硅与金属铝和RX（其中R和X如前所述）在约150℃至约400℃的温度下反应。

    Conversion of low-boiling constituents from alkyl-chlorosilane synthesis
    45.
    发明授权
    Conversion of low-boiling constituents from alkyl-chlorosilane synthesis 失效
    低沸点成分从烷基氯硅烷合成转化

    公开(公告)号：US4297500A

    公开(公告)日：1981-10-27

    申请号：US209932

    申请日：1980-11-24

    申请人： Ulrich Finke ,  Hans-Heinrich Moretto

    发明人： Ulrich Finke ,  Hans-Heinrich Moretto

    IPC分类号： C07F7/12 ,  C07F7/08

    CPC分类号： C07F7/123 ,  C07F7/122

    摘要： A process for converting the low-boiling constituents formed in the preparation of methylchlorosilane to the Muller-Rochow process and which consist essentially of tetramethylsilane, dimethylmonochlorosilane and 2-methylbut-2-ene into a product mixture consisting essentially of trimethylchlorosilane, dimethylchlorosilane and C.sub.2 -.sub.20 alkyldimethylchlorosilanes or C.sub.6-10 -aryldimethylchlorosilanes, comprising contacting the low-boiling product mixture with AlCl.sub.3, AlOCl and/or AlBr.sub.3, together with hydrogen chloride, in the liquid phase at about 40.degree. to +25.degree. C. The mixture prior to conversion may be contacted with HCl and either ZnCl.sub.2 or active charcoal and/or an olefin may be added thereto.

    摘要翻译： 将在甲基氯硅烷制备中形成的低沸点组分转化为Müller-Rochow工艺的方法，其基本上由四甲基硅烷，二甲基一氯甲硅烷和2-甲基丁-2-烯组成基本上由三甲基氯硅烷，二甲基氯硅烷和C2- 20烷基二甲基氯硅烷或C6-10-芳基二甲基氯硅烷，其包括在约40℃至+ 25℃下将液体相中的低沸点产物混合物与AlCl 3，AlOCl和/或AlBr 3一起与氯化氢接触。转化前的混合物 可以与HCl接触，并且可以向其中加入ZnCl 2或活性炭和/或烯烃。

    Transition metal catalyst compositions
    47.
    发明授权
    Transition metal catalyst compositions 失效
    过渡金属催化剂组合物

    公开(公告)号：US3987009A

    公开(公告)日：1976-10-19

    申请号：US532211

    申请日：1974-12-12

    申请人： Frank G. Young

    发明人： Frank G. Young

    IPC分类号： B01J31/16 ,  B01J31/24 ,  B01J37/24 ,  C07F7/08 ,  C07F7/12 ,  C07F9/02 ,  C07F9/53 ,  C08G77/30 ,  C08G77/398 ,  C08G77/04

    CPC分类号： C08G77/398 ,  B01J31/1675 ,  B01J31/2404 ,  B01J37/24 ,  C07F7/0834 ,  C07F7/122 ,  C07F9/02 ,  C07F9/53 ,  C08G77/30 ,  B01J2231/20 ,  B01J2231/32 ,  B01J2231/321 ,  B01J2231/323 ,  B01J2231/645 ,  B01J2531/824 ,  B01J2531/828

    摘要： A catalyst composition consisting essentially of a non-linear polymer consisting essentially of a recurring unit having the following structural formula:(R.sup.2).sub.2 P--R.sup.1 --Si--O.sub.3/2wherein R.sup.1 is an unsubstituted or substituted straight or branched chain divalent saturated alkylene radical having 1 to 10 carbon atoms or an unsubstituted or substituted divalent aryl radical having 1 to 3 benzene rings wherein the substituents for the alkylene radical can be halogen or a phenyl radical and the substituents for the aryl radical can be halogen or straight or branched chain saturated alkyl radicals having 1 to 5 carbon atoms; andR.sup.2 is an unsubstituted or substituted straight or branched chain or cyclic monovalent saturated alkyl radical having 1 to 10 carbon atoms or an unsubstituted or substituted monovalent aryl radical having 1 to 3 benzene rings wherein the substituents for the alkyl radical can be halogen or a phenyl radical and the substituents for the aryl radical can be halogen or straight or branched chain saturated alkyl radicals having 1 to 5 carbon atoms; andWherein each phosphorous atom in the polymer is coordinated with a platinum or palladium metal atom having a zero or positive charge, each positively charged metal atom having a sufficient number of negatively charged organic or inorganic radicals, devoid of functional groups, attached thereto to satisfy the valence of said transition metal atom, and wherein the radicals are selected from the group consisting of halogens; nitrates; sulfates; straight chain alkoxy or acyloxy radicals having 1 to 10 carbon atoms; and aryloxy radicals having 1 to 3 benzene rings.

    Method of producing dialkyldifluorosilane compounds
    48.
    发明授权
    Method of producing dialkyldifluorosilane compounds 失效
    制备二烷基二氟硅烷化合物的方法

    公开(公告)号：US3927059A

    公开(公告)日：1975-12-16

    申请号：US54885875

    申请日：1975-02-10

    申请人： CONTINENTAL OIL CO

    发明人： LIBBEY WILLIAM J ,  LUNDEEN ALLAN J

    IPC分类号： C07F7/12 ,  C07F7/08

    CPC分类号： C07F7/122

    摘要： Dialkyldifluorosilane compounds can readily be produced by a two step process wherein the first step involves the formation of an alkyltrifluorosilane compound from the reaction of an organoaluminum compound with silicon tetrafluoride and then reacting the alkyltrifluorosilane compound with an organo-aluminum compound to produce a reaction mixture containing the desired dialkyldifluorosilane compounds.

    摘要翻译： 二烷基二氟硅烷化合物可以容易地通过两步法制备，其中第一步涉及由有机铝化合物与四氟化硅反应形成烷基三氟硅烷化合物，然后使烷基三氟硅烷化合物与有机铝化合物反应以产生反应 含有所需的二烷基二氟硅烷化合物的混合物。

    Process for preparing organochlorosilanes
    49.
    发明授权
    Process for preparing organochlorosilanes 失效
    制备有机碳酰胺的方法

    公开(公告)号：US3844915A

    公开(公告)日：1974-10-29

    申请号：US27690972

    申请日：1972-08-01

    申请人： SHINETSU CHEMICAL CO

    发明人： TAKAMIZAWA M ,  HAYASHI T ,  TAKITA M

    IPC分类号： C07F7/12 ,  B01J1/10

    CPC分类号： C07F7/122

    摘要： Aromatic group containing organochlorosilanes are prepared by mixing chlorine, in the absence of irradiation, with a mixture of trichlorosilanes or methyldichlorosilanes and aromatic compounds, the then introducing the resulting mixture within an extremely short period of time into a zone irradiation with light, at least 30 percent of whose rays have wave lengths not exceeding 3,800 Angstrom. A wide variety of aromatic group containing organochlorosilanes are selectively obtained by the inventive process with high yields. Further, the formation of byproducts, which are difficult to separate and/or which have not utility, is effectively prevented.

    摘要翻译： 含有有机氯硅烷的芳族基团是通过在不存在辐射的情况下将氯与三氯硅烷或甲基二氯硅烷和芳族化合物的混合物混合，然后将所得混合物在极短的时间内引入到用光照射的区域中，至少30 其光线的百分比波长不超过3800埃。 通过本发明方法以高收率选择性地获得含有多种含芳基的有机氯硅烷。 此外，有效地防止难以分离和/或没有效用的副产物的形成。