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    Radiation-curable compositions and cured articles
    41.
    发明授权
    Radiation-curable compositions and cured articles 有权
    可辐射固化组合物和固化制品

    公开(公告)号：US06660374B2

    公开(公告)日：2003-12-09

    申请号：US10053021

    申请日：2002-01-18

    Applicant: David A. Smetana ,  Joseph V. Koleske

    Inventor： David A. Smetana ,  Joseph V. Koleske

    IPC: C08F248

    CPC classification number: C08K5/0025 ,  C08F283/10 ,  C08F290/061 ,  C08F290/064 ,  H05K3/287 ,  Y10T428/25 ,  Y10T428/252 ,  Y10T428/254 ,  Y10T428/259 ,  Y10T428/26 ,  Y10T428/261 ,  Y10T428/263 ,  Y10T428/265 ,  Y10T428/2982 ,  Y10T428/2993 ,  Y10T428/2998 ,  Y10T428/31511 ,  Y10T428/31935

    Abstract: A radiation-curable composition in a liquid or solid form comprises at least one solid, non-crystalline radiation-transmissible material, dispersed in at least one cationic-curable or free-radical curable composition or mixture thereof. The solid, non-crystalline radiation-transmissible materials comprise glasses and other suitable materials that transmit (i.e., are transparent to) at least about 40% of radiation having a wavelength from about 180 to about 600 nanometers. The cationic-curable compositions comprise at least one cycloaliphatic epoxide, at least one polyol, and at least one cation-generating photoinitiator. The free-radical curable compositions comprise at least one ethylenically unsaturated compound and at least one free-radical-generating photoinitiator unless electron beam curing is used, in which case the amount of photoinitiator can be reduced or even eliminated. The solid forms of the radiation-curable compositions of the invention are useful as powder coatings for coating decorative and functional objects and that would be cured by a thermal heating flow process followed by radiation exposure. The cured compositions of the invention are useful as coatings and inks for metal, paper, plastics, glass, ceramics, and wood, as adhesives, as sealants, and as composite materials and other articles. The cured compositions of this invention also are useful in biomedical and dental applications, including prosthetic devices such as dentures; coatings, fillings, and caps for teeth; and the like.

    Abstract translation: 液体或固体形式的可辐射固化组合物包含分散在至少一种阳离子可固化或自由基可固化组合物或其混合物中的至少一种固体，非结晶辐射透射材料。 固体，非结晶辐射透射材料包括玻璃和其它合适的材料，其透射（即，透明）至少约40％的波长为约180至约600纳米的辐射。阳离子可固化组合物包含 至少一种脂环族环氧化物，至少一种多元醇和至少一种产生阳离子的光引发剂。 自由基可固化组合物包含至少一种烯键式不饱和化合物和至少一种产生自由基的光引发剂，除非使用电子束固化，在这种情况下光引发剂的量可以减少甚至消除。固体形式的辐射 本发明的可固化组合物可用作涂覆装饰性和功能性物体的粉末涂料，并且其将通过热加热流程固化，随后进行辐射曝光。 本发明的固化组合物可用作金属，纸，塑料，玻璃，陶瓷和木材的涂料和油墨，作为粘合剂，作为密封剂，以及作为复合材料和其它制品。 本发明的固化组合物还可用于生物医学和牙科应用，包括假体装置如假牙; 牙齿的涂层，填充物和盖子; 等等。

    Radiation-curable compositions and cured articles
    42.
    发明授权
    Radiation-curable compositions and cured articles 有权
    可辐射固化组合物和固化制品

    公开(公告)号：US06350792B1

    公开(公告)日：2002-02-26

    申请号：US09616201

    申请日：2000-07-13

    Applicant: David A. Smetana ,  Joseph V. Koleske

    Inventor： David A. Smetana ,  Joseph V. Koleske

    IPC: C08F246

    CPC classification number: C08K5/0025 ,  C08F283/10 ,  C08F290/061 ,  C08F290/064 ,  H05K3/287 ,  Y10T428/25 ,  Y10T428/252 ,  Y10T428/254 ,  Y10T428/259 ,  Y10T428/26 ,  Y10T428/261 ,  Y10T428/263 ,  Y10T428/265 ,  Y10T428/2982 ,  Y10T428/2993 ,  Y10T428/2998 ,  Y10T428/31511 ,  Y10T428/31935

    Abstract: A radiation-curable composition in a liquid or solid form comprises at least one solid, non-crystalline radiation-transmissible material, dispersed in at least one cationic-curable or free-radical curable composition or mixture thereof. The solid, non-crystalline radiation-transmissible materials comprise glasses and other suitable materials that transmit (i.e., are transparent to) at least about 40% of radiation having a wavelength from about 180 to about 600 nanometers. The solid forms of the radiation-curable compositions of the invention are useful as powder coatings for coating decorative and functional objects and that would be cured by a thermal heating flow process followed by radiation exposure. The cured compositions of the invention are useful as coatings and inks for metal, paper, plastics, glass, ceramics, and wood, as adhesives, as sealants, and as composite materials and other articles and in biomedical and dental applications.

    Abstract translation: 液体或固体形式的可辐射固化组合物包含分散在至少一种阳离子可固化或自由基可固化组合物或其混合物中的至少一种固体，非结晶辐射透射材料。 固体，非结晶辐射透射材料包括玻璃和其它合适的材料，其透射（即透明的）至少约40％的具有约180至约600纳米的波长的辐射。 本发明的可辐射固化组合物的固体形式可用作用于涂覆装饰性和功能性物体的粉末涂料，并且其将通过热加热流程固化，随后进行辐射曝光。 本发明的固化组合物可用作金属，纸，塑料，玻璃，陶瓷和木材的涂料和油墨，作为粘合剂，作为密封剂，以及作为复合材料和其它制品以及生物医学和牙科应用。

    (N-substituted carbamoyloxy)alkanoyloxyalkyl acrylate polymers and compositions made therefrom
    45.
    发明授权
    (N-substituted carbamoyloxy)alkanoyloxyalkyl acrylate polymers and compositions made therefrom 失效
    （N-取代氨基甲酰氧基）烷酰氧基烷基丙烯酸酯聚合物及由其制备的组合物

    公开(公告)号：US5115025A

    公开(公告)日：1992-05-19

    申请号：US373548

    申请日：1989-06-30

    Applicant: Joseph V. Koleske ,  Donald F. Smith, Jr. ,  Robert J. Weber, Jr.

    Inventor： Joseph V. Koleske ,  Donald F. Smith, Jr. ,  Robert J. Weber, Jr.

    IPC: C08F20/36

    CPC classification number: C08F20/36

    Abstract: This invention is directed to polymers (including oligomers) that contain (N-substituted carbamoyloxy)alkanoyloxyalkyl acrylates, to a process for their preparation by reacting the carbamoyloxy alkanoyloxyalkyl acrylates with themselves, with lactone acrylates, and/or with other ethylenically unsaturated monomers, and to coating, ink, adhesive, and sealant compositions (including the cured coatings, inks, adhesives, and sealants) that are obtained by curing the above compositions by various means. The cured compositions, which are, for example, high-quality industrial finishes, sealants or encapsulants, are preferably made by incorporation of various conventional crosslinking agents and other normally-used formulating ingredients with the polymeric compositons of the invention.

    Abstract translation: 本发明涉及含有（N-取代氨基甲酰氧基）烷酰氧基烷基丙烯酸酯的聚合物（包括低聚物），其通过使丙烯酸氨基甲酰氧基烷酰氧基烷基酯与丙烯酸内酯与丙烯酸内酯和/或与其它烯键式不饱和单体反应而制备的方法，以及 涉及通过各种方法固化上述组合物而获得的涂料，油墨，粘合剂和密封剂组合物（包括固化涂料，油墨，粘合剂和密封剂）。 固化的组合物，例如高品质工业涂料，密封剂或密封剂，优选通过将各种常规交联剂和其它常用配方成分与本发明的聚合物组合物并入而制备。

    Blends of epoxides and monoepoxides
    49.
    发明授权
    Blends of epoxides and monoepoxides 失效
    环氧化物和单环氧化物的共混物

    公开(公告)号：US4814361A

    公开(公告)日：1989-03-21

    申请号：US902780

    申请日：1986-09-02

    Applicant: Joseph V. Koleske ,  Neil J. McCarthy, Jr.

    Inventor： Joseph V. Koleske ,  Neil J. McCarthy, Jr.

    IPC: C08F299/02 ,  C08G59/14 ,  C08G59/68 ,  C08G59/24 ,  C08G59/62 ,  C08J3/28

    CPC classification number: C08F299/026 ,  C08G59/145 ,  C08G59/68

    Abstract: Described herein are compositions suitable for photocopolymerization comprising (a) an epoxide containing two or more epoxy groups, and (b) a hydroxyl substituted cycloaliphatic monoepoxide. The composition may additionally contain a poly (active hydrogen) organic compound and/or a photoinitiator. A coating produced from such a composition has a good combination of properties.

    Abstract translation: 本文描述的是适用于光聚合的组合物，其包含（a）含有两个或多个环氧基的环氧化物和（b）羟基取代的脂环族单环氧化物。 该组合物可另外含有聚（活性氢）有机化合物和/或光引发剂。 由这种组合物制成的涂层具有良好的性能组合。

    Low viscosity adducts of a polycaprolactone polyol and a polyepoxide
    50.
    发明授权
    Low viscosity adducts of a polycaprolactone polyol and a polyepoxide 失效
    聚己内酯多元醇和聚环氧化物的低粘度加合物

    公开(公告)号：US4725653A

    公开(公告)日：1988-02-16

    申请号：US797471

    申请日：1985-11-13

    Applicant: Joseph V. Koleske

    Inventor： Joseph V. Koleske

    IPC: C08G59/62 ,  C09D163/00 ,  C08L63/00

    CPC classification number: C09D163/00 ,  C08G59/62

    Abstract: This invention is directed to adducts of a polycaprolactone polyol and a polyepoxide comprising the reaction product of at least one polycaprolactone polyol and a polyepoxide containing two or more epoxy groups per molecule in a molar ratio of polycaprolactone polyol to polyepoxide of from about 2:1 to about 3:1, said adducts having an oxirane content of less than about 0.10 percent and a viscosity of less than about 3700 centistokes at 54.5.degree. C. The adducts are useful in the formulation of high solids coating compositions, polyurethane elastomers, inks, sealants, adhesives and the like.

    Abstract translation: 本发明涉及聚己内酯多元醇和聚环氧化物的加合物，其包含至少一种聚己内酯多元醇和每分子含有两个或多个环氧基团的聚环氧化物的反应产物，聚己内酯多元醇与聚环氧化物的摩尔比为约2:1至 约3:1，所述加合物的环氧乙烷含量小于约0.10％，粘度在54.5℃下小于约3700厘沲。加合物可用于制备高固含量涂料组合物，聚氨酯弹性体，油墨，密封剂 ，粘合剂等。

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