摘要:
Wall temperatures within a movable, internally cooled scraper element that is used to dislodge metal oxide accumulation from the internal wall of a reactor are monitored by a thermocouple electrically connected to mercury baths which are in turn electrically connected to a temperature recorder. The thermocouple output can be used to control a regulator of coolant fed to the scraper element.
摘要:
Described is a control system for a refining hydrogenation and deodorizing plant for edible oils and the like wherein various system variables are converted into signals which are fed to a computer which controls the system to optimize performance and reduce oil losses.
摘要:
A HOLLOW ELONGATED SHELL HAVING AN INLET AND AN OUTLET AT OPPOSITE ENDS HAS A SERIES OF AGITATING ASSEMBLIES MOUNTED AT AXIALLY-SPACED LOCATIONS IN THE SHELL. EACH AGITATING ASSEMBLY INCLUDES A HOLLOW DRAFT TUBE HAVING INLET PORT MEANS AT ONE END COMMUNICATING WITH THE CORRESPONDING END OF AN ANNULAR FLOW PASSAGE BETWEEN THE DRAFT TUBE AND SHELL AND OUTLET PORT MEANS AT THE OPPOSITE END COMMUNICATING WITH THE OTHER END OF THE PASSAGE. AN IMPELLER IS MOUNTED FOR ROTATION IN THE DRAFT TUBE ADJACENT THE OUTLET PORT MEANS TO FLOW THE PROCESS INGREDIENTS AXIALLY THROUGHT THE DRAFT TUBE AND OUTWARDLY THROUGH THE OUTLET PORTS WHERE THE INGREDIENTS ARE MIXED WITH INGREDIENTS FLOWING INTO THE OTHER END OF THE PASSAGE. BAFFLE MEANS IS ASSOICATED WITH THE OUTLET PORTS TO REDIRECT THE FLOW OF THE REACTED INGREDIENTS AFTER THEY EXIT THE OUTLET PORTS AND TO BREAK UP ANY SWIRL CAUSED BY THE IMPELLER. THE IMPELLER AND BAFFLE MEANS COOPERATE TO PROVIDE HYDRAULIC AND MECHANICAL SHEAR FORCES ON THE INGREDIENTS TO IMPROVE REACTION IN THE APPARATUS.
摘要:
AN APPARATUS FOR CONVERTING CYANIDE WASTES INTO SODIUM CYANIDE IN WHICH A HEAT EXCHANGER IS INTERCONNECTED BETWEEN A PLURALITY OF REACTION TANKS AND A FIRST TOWER ADAPTED TO HOLD A CHARGE OR SODIUM HYDROXIDE. SAID TOWER IS INTERCONNECTED TO ONE COMPARTMENT OF A CHAMBERED TANK, AND A SECOND COMPARTMENT IN SAID TANK IS CONNECTED TO A SECOND TOWER ADAPTED TO HOLD A CHARGE OF SODIUM HYDROXIDE. A PUMPING ASSEMBLY IS PROVIDED FOR WITHDRAWING THE SODIUM CYANIDE FROM THE FIRST COMPARTMENT AND FOR RECYCLING THE REACTION MIXTURE THROUGH THE TOWERS AND THE COMPARTMENTED TANK.
摘要:
IN AN OPERATION WHEREIN SELENIUM VALUES ARE RECOVERED FROM PELLETIZED SELEMIUM-CONTAINING MATERIALS INVOLVING HEATING PELLETIZED SELENIUM-CONTAINING MATERIALS IN THE PRESENCE OF AIR SO AS TO VOLATILIZE THE SELENIUM FROM SAID PELLETIZED SELENIUM-CONTAINING MATERIALS IN THE FORM OF SELENIUM DIOXIDE, IMPROVED RESULTS ARE OBTAINED BY EMPLOYING AN APPARATUS WHEREIN A MASS OF PELLETIZED SELENNIUM-CONTAINING MATERIAL IS MAINTAINED STATIC WITHIN A ROASTING ZONE AND PREHEATED AIR EMPLOYED TO HEAT THE MASS OF PELLETIZED SELENIUM-CONTAINING MATERIALS IS PASSED
DOWNWARDLY THROUGH SAID MASS OF PELLETIZED SELENIUMCONTAINING MATERIALS MAINTAINED AT A TEMPERATURE OF ABOUT 1350*F. FOR A PERIOD OF TIME IN THE RANGE ABOUT 1-6 HOURS SUFFICIENT TO VOLATILIZE SUBSTANTIALLY ALL OF THE SELENIUM FROM SAID PELLETIZED SELENIUM-CONTAINING MATERIALS AND THEREUPON DISCHARGING THE RESULTING SUBSTANTIALLY DESELENIZED PELLETIZED MATERIAL FROM SAID ROASTING ZONE.
AND N IS ESSENTIALLY 0 OR GREATER (E.G.,0-20), (B) A POLYTHIOL, THE EQUIVALET RATIO OF POLYENE TO POLYTHIOL BEING AOUT 1:0.5-1.5, AND (C) A MEMBER SELECTED FROM A GROUP CONSISTING OF A MONOMERIC ACID HAVING THE FORMULA
CH2=C(-R)-COOH
WHERE R IS H, CH3, OR C2H5 OR A HOMPOLYMER OF COPOLYMER OF SUCH MONOMERIC ACID HAVING AN AVERAGE MOLECULAR WEIGHT OF ABOUT 140-1000, THE GROUP MEMBER CONSTITUTING ABOUT 2-10% BY WEIGHT OF THE COMPOSITION. THE ABOVE COMPOSITON CAN CONTAIN AN EFFECTIVE AMOUNT OF A PHOTOCURING RATE ACCELERATORR.
摘要:
DIACETONE ACRYLAMIDE AND ANALOGOUS SUBSTITUTED ACRYLAMIDES REACT WITH ALDEHYDES CONTAINING CONJUGATE UNSATURATION WITH RESPECT TO THE CARBONYL GROUP, IN THE PRESENCE OF AN ALKAINE REAGENT, TO YIELD MONOMERIC COMPOUNDS WHICH ARE PHOTOSENSITIVE AND WHICH FORM PHOTOSENSITIVE POLYMERS. THE LATTER CAN ALSO BE PREPARED BY REACTING SAID ALDEHYDES WITH A DIACETONE ACRYLAMIDE POLYMER WHILE GRADUALLY ADDING SAID ALKALINE REAGENT. THE POLYMERS CROSSLINK ON EXPOSURE TO VISIBLE OR (PREFERABLY) ULTRAVIOLET RADIATION AND ARE USEFUL IN THE PREPARATION OF LITHOGRAPHIC PRINTING PLATES, PHOTORESISTS, ETC.
摘要:
The preparation of aqueous latices from solvent dispersions of elastomers and other high polymer compositions has presented problems including excessive viscosity during processing and foaming and coagulation, which have produced losses and increased costs. Herein combinations of steps are disclosed which reduce or eliminate various of these problems; enable the preparation of latices from high solids, high viscosity cements as well as from high solids cements of low molecular weight polymer; enable preparation of latices of grafted or filler extended or filler reinforced elastomers; enable preparation of latices of low molecular weight polymer which are then modified to materially increase the molecular weight of the polymer and/or the latex particle size; and enable the preparation of improved latices both dilute and of high solids contents, which are useful for example for adhesive and film forming purposes. The process in common with that of related copending applications is characterized, inter alia, by the establishment of a flow of latex through the separating zone and the impingement on said flow of the coalesced latex droplets from the solvent vapor stream in which they are delivered to the separator, and in certain embodiments by the use of particular additive materials. New combinations of steps and of apparatus for performing the same are also disclosed and claimed. The process disclosed is applicable to the production of latices from specified rubbery and non-rubbery polymer compositions, and certain of such latices are new and useful products also claimed herein.
摘要:
Production of CIF3O by reacting under ultraviolet light a compound selected from the group consisting of ClF2F and ClO3F with a compound selected from the group consisting of ClF5, ClF3, ClF, OF2 and F2.
摘要:
The invention relates to the modification of ethylenically unsaturated polymers using polyfunctional quaternary amidoximidinium salts as the modifying agents. These salts are precursors to the corresponding polyfunctional nitrile N-oxides and the latter, upon being generated from the salt precursors, are the active modifying agents in the modification process. Representative of these salts is terephthalo-bis(hydroximoyl pyridinium chloride).