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    METHODS OF PREPARING POLYMER-ORGANOCLAY COMPOSITES AND ARTICLES DERIVED THEREFROM
    15.
    发明申请
    METHODS OF PREPARING POLYMER-ORGANOCLAY COMPOSITES AND ARTICLES DERIVED THEREFROM 失效
    制备聚合物 - 组织复合材料的方法及其衍生物

    公开(公告)号：US20080004391A1

    公开(公告)日：2008-01-03

    申请号：US11766456

    申请日：2007-06-21

    申请人： Kwok Chan ,  Sarah Genovese ,  Erik Hagberg ,  David Hall ,  John Maxam ,  Tara Mullen ,  Roy Odle ,  Albert Stella ,  James White

    发明人： Kwok Chan ,  Sarah Genovese ,  Erik Hagberg ,  David Hall ,  John Maxam ,  Tara Mullen ,  Roy Odle ,  Albert Stella ,  James White

    IPC分类号： C08K9/04

    CPC分类号： C08F2/44

    摘要： A method for preparing a polymer-organoclay composite composition comprises combining a solvent and an unexfoliated organoclay to provide a first mixture, wherein the unexfoliated organoclay comprises alternating inorganic silicate layers and organic layers, and has an initial spacing between the silicate layers; exposing the first mixture to an energized condition of a sufficient intensity and duration to increase the initial spacing of the inorganic silicate layers, to provide a second mixture; contacting the second mixture with a polymer composition so that the polymer composition fills at least one region located between at least one pair of silicate layers, wherein the polymer composition is at least partially soluble in the solvent; and removing at least a portion of the solvent from the second mixture, wherein the inorganic silicate layers remain separated by the polymer after removal of the solvent.

    摘要翻译： 一种制备聚合物 - 有机粘土复合材料组合物的方法，包括将溶剂和未剥离的有机粘土组合以提供第一混合物，其中未剥离的有机粘土包含交替的无机硅酸盐层和有机层，并且在硅酸盐层之间具有初始间隔; 将第一混合物暴露于足够强度和持续时间的通电状态以增加无机硅酸盐层的初始间隔，以提供第二混合物; 使所述第二混合物与聚合物组合物接触，使得所述聚合物组合物填充位于至少一对硅酸盐层之间的至少一个区域，其中所述聚合物组合物至少部分地可溶于所述溶剂中; 以及从所述第二混合物中除去至少一部分所述溶剂，其中在去除所述溶剂之后，所述无机硅酸盐层保持被所述聚合物分离。

    COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES
    17.
    发明申请
    COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
    聚合物复合材料的组合物和方法

    公开(公告)号：US20070299188A1

    公开(公告)日：2007-12-27

    申请号：US11766423

    申请日：2007-06-21

    申请人： Kwok Chan ,  Erik Hagberg ,  Tara Mullen ,  Roy Odle ,  James White ,  Norimitsu Yamaguchi

    发明人： Kwok Chan ,  Erik Hagberg ,  Tara Mullen ,  Roy Odle ,  James White ,  Norimitsu Yamaguchi

    IPC分类号： C08K9/04 ,  C08K5/50

    CPC分类号： C08J3/201 ,  B82Y30/00 ,  C01B33/44 ,  C08J5/005 ,  C08K3/346 ,  C08K5/50 ,  C08K9/04

    摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a method of making a polymer-organoclay composite composition, said method comprising melt mixing a quaternary organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary organic cation with a polymeric resin comprising at least one polymer selected from the group consisting of polyamides, polyesters, polyarylene sulfides, polyarylene ethers, polyether sulfones, polyether ketones, polyether ether ketones, polyphenylenes, and polycarbonates, said polymeric resin being substantially free of polyetherimides; said melt mixing being carried out at a temperature in a range between about 300° C. and about 450° C. to provide a polymer-organoclay composite composition, said polymer-organoclay composite composition being characterized by a percent exfoliation of at least 10 percent.

    摘要翻译： 本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合材料组合物和制备聚合物纳米复合材料的方法的有机盐组合物。 在一个实施方案中，本发明提供了制备聚合物 - 有机粘土复合材料组合物的方法，所述方法包括熔融混合包含交替的无机硅酸盐层和有机层的季有机粘土组合物，所述有机层包含季铵有机阳离子与聚合树脂， 选自聚酰胺，聚酯，聚亚芳基硫醚，聚亚芳基醚，聚醚砜，聚醚酮，聚醚醚酮，聚苯基和聚碳酸酯的至少一种聚合物，所述聚合物树脂基本上不含聚醚酰亚胺; 所述熔体混合在约300℃至约450℃之间的温度下进行，以提供聚合物 - 有机粘土复合材料组合物，所述聚合物 - 有机粘土复合组合物的特征在于至少10％的剥离百分比 。

    Solventless process for the preparation of amine functional polyetherimide resins with improved melt flow
    18.
    发明授权
    Solventless process for the preparation of amine functional polyetherimide resins with improved melt flow 有权
    用于制备具有改进的熔体流动的胺官能聚醚酰亚胺树脂的无溶剂方法

    公开(公告)号：US08722187B2

    公开(公告)日：2014-05-13

    申请号：US13286093

    申请日：2011-10-31

    申请人： Robert R. Gallucci ,  Roy Odle ,  Daniel F. Lowery ,  Richard Peters

    发明人： Robert R. Gallucci ,  Roy Odle ,  Daniel F. Lowery ,  Richard Peters

    IPC分类号： B32B27/34

    CPC分类号： C08G73/1071 ,  C08G73/10 ,  C08G73/1017 ,  C08G73/1028 ,  C08G73/1046 ,  C08G73/1053 ,  C08G73/106 ,  C08G73/1064 ,  C08G75/23 ,  C08G77/382 ,  C08L79/08 ,  D01D5/08 ,  D01F6/74 ,  D01F6/78 ,  D04H1/4326 ,  Y10T428/249921 ,  Y10T428/2933 ,  Y10T428/2969

    摘要： The disclosure relates to a process that includes blending a polyimide resin and a primary alky amine organic compound to produce an aryl amine functionalized polyimide, having aryl amine functionality in excess of any anhydride functionality. The polyimide resin can have a weight average molecular weight (Mw) from 5,000 to 100,000 daltons. The organic compound can include at least one primary aliphatic amine without a direct linkage of a nitrogen to an aryl group and without a functionality selected from a halogen functionality, a hydroxyl functionality, a sulfonic acid functionality, a sulfonic acid salt functionality, and combinations thereof. The disclosure also relates to alkyl imide functionalized polyimides also with aryl amine functionalized polyimides, having aryl amine functionality in excess of any anhydride functionality and articles produced therefrom.

    摘要翻译： 本公开涉及一种方法，其包括将聚酰亚胺树脂和伯烷基胺有机化合物混合以制备芳基胺官能化聚酰亚胺，其芳基胺官能度超过任何酸酐官能度。 聚酰亚胺树脂的重均分子量（Mw）可以为5,000至100,000道尔顿。 有机化合物可以包括至少一种伯脂族胺，而不将氮直接连接到芳基上，而不具有选自卤素官能团，羟基官能团，磺酸官能团，磺酸盐官能团及其组合的官能团 。 本公开还涉及具有芳基胺官能化聚酰亚胺的烷基酰亚胺官能化聚酰亚胺，其具有超过任何酸酐官能团的芳基胺官能团和由其制备的制品。

    Polyetherimide and Polyetherimide Sulfone Blends Having Automotive Lighting Applications
    19.
    发明申请
    Polyetherimide and Polyetherimide Sulfone Blends Having Automotive Lighting Applications 有权
    具有汽车照明应用的聚醚酰亚胺和聚醚酰亚胺砜共混物

    公开(公告)号：US20090258991A1

    公开(公告)日：2009-10-15

    申请号：US12347542

    申请日：2008-12-31

    申请人： Norimitsu Yamaguchi ,  Roy Odle ,  Sanjay Mishra

    发明人： Norimitsu Yamaguchi ,  Roy Odle ,  Sanjay Mishra

    IPC分类号： C08L77/00

    CPC分类号： C08L79/08 ,  C08L2205/02 ,  Y10T428/3163 ,  Y10T428/31681 ,  Y10T428/31721 ,  C08L2666/20

    摘要： Compositions and articles of manufacture made therefrom for use in high temperature application, such as automotive reflectors, have a minimum haze onset temperature of about 205° C. and are made from a transparent, miscible blend of from about 30 to about 70 weight percent of a polyetherimide sulfone comprising greater than or equal to 50 mole percent of the polymer linkages have an aryl sulfone group and from about 70 to about 30 weight percent of a polyetherimide or polyimide.

    摘要翻译： 由用于高温应用的组合物和制品，例如汽车反射器，具有约205℃的最小雾度起始温度，并且由透明的，可混溶的约30至约70重量％的共混物制成 包含大于或等于50摩尔％的聚合物键的聚醚酰亚胺砜具有芳基砜基团和约70至约30重量％的聚醚酰亚胺或聚酰亚胺。

    COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES
    20.
    发明申请
    COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 失效
    聚合物复合材料的组合物和方法

    公开(公告)号：US20070299189A1

    公开(公告)日：2007-12-27

    申请号：US11766850

    申请日：2007-06-22

    申请人： Feng Cao ,  Kwok Chan ,  Erik Hagberg ,  Farid Khouri ,  Tara Mullen ,  Roy Odle ,  James White ,  Norimitsu Yamaguchi

    发明人： Feng Cao ,  Kwok Chan ,  Erik Hagberg ,  Farid Khouri ,  Tara Mullen ,  Roy Odle ,  James White ,  Norimitsu Yamaguchi

    IPC分类号： C08K9/04

    CPC分类号： C08F2/44

    摘要： In one embodiment, the present invention provides a method of making a polymer-organoclay composite composition comprising (a) contacting under condensation polymerization conditions a first monomer, a second monomer, a solvent, and an organoclay composition, said organoclay composition comprising alternating inorganic silicate layers and organic layers, to provide a first polymerization reaction mixture, wherein one of said first monomer and second monomers is a diamine and the other is an dianhydride; (b) carrying out a stoichiometry verification step on the first polymerization reaction mixture; (c) optionally adding additional reactant (monomer 1, monomer 2, or chainstopper) to the first polymerization reaction mixture to provide a second polymerization reaction mixture; and (d) removing solvent from the first polymerization reaction mixture or the second polymerization reaction mixture to provide a first polymer-organoclay composite composition comprising a polymer component and an organoclay component wherein the organoclay component is at least 10% exfoliated.

    摘要翻译： 在一个实施方案中，本发明提供制备聚合物 - 有机粘土复合组合物的方法，其包含（a）在缩聚条件下使第一单体，第二单体，溶剂和有机粘土组合物接触，所述有机粘土组合物包含交替的无机硅酸盐 层和有机层，以提供第一聚合反应混合物，其中所述第一单体和第二单体之一是二胺，另一个是二酐; （b）在第一聚合反应混合物上进行化学计量验证步骤; （c）任选地向第一聚合反应混合物中加入另外的反应物（单体1，单体2或链截止剂）以提供第二聚合反应混合物; 和（d）从第一聚合反应混合物或第二聚合反应混合物中除去溶剂以提供包含聚合物组分和有机粘土组分的第一聚合物 - 有机粘土复合组合物，其中有机粘土组分至少10％剥离。