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11.发明申请Phosphors and related manufacturing method, display device, and fluorescent lamp 有权荧光体及相关制造方法，显示装置和荧光灯公开(公告)号：US20050017218A1
公开(公告)日：2005-01-27
申请号：US10867121
申请日：2004-06-14
CPC分类号： H01J1/63 , C09K11/7734
摘要： Phosphors having high luminescence characteristics are provided while achieving manufacturing cost reductions by minimizing the usage amount of Eu, the luminescence center. Also provided are a display device (PDP, etc) and a fluorescent lamp having excellent display and/or luminescence characteristics as a result of using the phosphors, while achieving manufacturing cost reductions by minimizing the Eu usage amount.
摘要翻译： 提供具有高发光特性的荧光体，同时通过使Eu的发光中心的使用量最小化来实现制造成本的降低。 还提供了作为使用荧光体的结果，具有优异的显示和/或发光特性的显示装置（PDP等）和荧光灯，同时通过使Eu使用量最小化来实现制造成本的降低。
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公开(公告)号：US20120013248A1
公开(公告)日：2012-01-19
申请号：US13148129
申请日：2011-02-24
IPC分类号： H01J17/49
摘要： A PDP has a front plate and a rear plate. The front plate includes a protective layer, and the rear plate includes phosphor layers. The protective layer includes a base layer. Agglomerated particles are dispersed on the base layer. The base layer includes a first metallic oxide and a second metallic oxide. The base layer has a peak through an X-ray diffraction analysis between a first peak of the first metallic oxide and a second peak of the second metallic oxide. The first metallic oxide and the second metallic oxide are two selected from a group consisting of MgO, CaO, SrO, and BaO. The phosphor layers include particles of a platinum group element.
摘要翻译： PDP具有前板和后板。 前板包括保护层，后板包括荧光体层。 保护层包括基层。 聚集的颗粒分散在基层上。 基层包括第一金属氧化物和第二金属氧化物。 基底层通过第一金属氧化物的第一峰和第二金属氧化物的第二峰之间的X射线衍射分析具有峰值。 第一金属氧化物和第二金属氧化物是选自MgO，CaO，SrO和BaO的两种。 荧光体层包括铂族元素的颗粒。
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13.发明申请METHOD OF MANUFACTURING BLUE SILICATE PHOSPHOR, AND BLUE SILICATE PHOSPHOR AND LIGHT-EMITTING DEVICE 有权制造蓝色硅酸盐磷光体和蓝色硅酸盐荧光体和发光器件的方法公开(公告)号：US20090218926A1
公开(公告)日：2009-09-03
申请号：US12299868
申请日：2007-05-16
CPC分类号： C09K11/7734 , C09K11/595 , C09K11/7774 , C09K11/778 , C09K11/7784 , C09K11/7797
摘要： The present invention provides a method of manufacturing a blue silicate phosphor having high luminance and a chromaticity y comparable to or lower than that of BAM:Eu. The present invention is a method of manufacturing a blue silicate phosphor represented by the general formula aAO.bEuO.(Mg1−w,Znw)O.cSiO2.dCaCl2, where A is at least one selected from Sr, Ba and Ca, and 2.970≦a≦3.500, 0.006≦b≦0.030, 1.900≦c≦2.100, 0≦d≦0.05, and 0≦w≦1 are satisfied. In this manufacturing method, heat treatment is carried out in a gas atmosphere having an oxygen partial pressure of 1×10−15.5 atm to 1×10−10 atm at a temperature of 1200° C. to 1400° C.
摘要翻译： 本发明提供一种制造与BAM：Eu相当或更低的亮度和色度y的蓝色硅酸盐荧光体的方法。 本发明是制造由通式aAO.bEuO（Mg1-w，Znw）O.cSiO2.dCaCl2表示的蓝色硅酸盐荧光体的方法，其中A为选自Sr，Ba和Ca中的至少一种，2.970 <= a <= 3.500,0.006 <= b <= 0.030,1.900 <= c <= 2.100,0 <= d <= 0.05，0 <= w <= 1。 在该制造方法中，在1200〜1400℃的温度下，在氧分压为1×10-15.5atm〜1×10-10atm的气氛中进行热处理。
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公开(公告)号：US20090072704A1
公开(公告)日：2009-03-19
申请号：US11911402
申请日：2006-04-14
IPC分类号： H01J1/63
CPC分类号： C09K11/7734 , C09K11/595 , C09K11/778 , C09K11/7787 , C09K11/7797 , H01J2211/42
摘要： The present invention provides a phosphor that has high luminance, a property of low luminance degradation during PDP driving, and chromaticity y comparable to that of BAM:Eu. The present invention is the phosphor that is represented by the general formula xAO.y1EuO.y2EuO3/2.DO.zSiO2 wherein A is at least one selected from Ca, Sr and Ba, D is at least one selected from Mg and Zn, and 2.970≦x≦3.500, 0.001≦y1+y2≦0.030, and 1.900≦z≦2.100 are satisfied, and that has 50 mol % or less of the divalent Eu ratio (ratio of the divalent Eu element to the total of the Eu elements) in the vicinity of the surface of the phosphor particle.
摘要翻译： 本发明提供了具有高亮度，PDP驱动时亮度劣化低的特性和与BAM：Eu相当的色度y的荧光体。 本发明是由通式xAO.y1EuO.y2EuO3 / 2.DO.zSiO2表示的荧光体，其中A是选自Ca，Sr和Ba中的至少一种，D是选自Mg和Zn中的至少一种，以及 2.970 <= x <= 3.500，0.001 <= y1 + y2 <= 0.030，并且满足1.900 <= z <= 2.100，并且具有50mol％以下的二价Eu比（二价Eu元素与 荧光体颗粒表面附近的Eu元素的总和）。
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公开(公告)号：US07238303B2
公开(公告)日：2007-07-03
申请号：US10928516
申请日：2004-08-27
申请人： Kojiro Okuyama , Takehiro Zukawa , Masahiro Sakai , Seigo Shiraishi , Kazuhiko Sugimoto , Masaki Aoki , Junichi Hibino
发明人： Kojiro Okuyama , Takehiro Zukawa , Masahiro Sakai , Seigo Shiraishi , Kazuhiko Sugimoto , Masaki Aoki , Junichi Hibino
CPC分类号： C09K11/595 , C09K11/7734 , C09K11/778 , H01J1/63 , H01J2211/42
摘要： Phosphor and a plasma display device are provided whose deterioration in brightness of phosphors and a degree of change in chromaticity are alleviated and whose discharge characteristics are improved and that has excellent initial characteristics. Phosphor of the present invention is an alkaline-earth metal aluminate phosphor containing an element M (where M denotes at least one type of element selected from the group consisting of Nb, Ta, W and B). In this phosphor, a concentration of M in the vicinity of a surface of the phosphor particles is higher than the average concentration of M in the phosphor particles as a whole. A plasma display device according to the present invention includes a plasma display panel in which a plurality of discharge cells in one color or in a plurality of colors are arranged and phosphor layers are arranged so as to correspond to the discharge cells in colors and in which light is emitted by exciting the phosphor layers with ultraviolet rays. The phosphor layers include blue phosphor, where the afore-mentioned phosphor is used as the blue phosphor.
摘要翻译： 提供了荧光体和等离子体显示装置，其荧光体的亮度劣化和色度变化程度得到缓解，其放电特性得到改善并具有优异的初始特性。 本发明的荧光体是含有元素M的碱土金属铝酸盐荧光体（其中M表示选自Nb，Ta，W和B中的至少一种元素）。 在该荧光体中，荧光体粒子表面附近的M浓度高于荧光体粒子的M的平均浓度。 根据本发明的等离子体显示装置包括等离子体显示面板，其中排列有一种颜色或多种颜色的多个放电单元，并且荧光体层被布置为与颜色的放电单元相对应，并且其中 通过用紫外线激发荧光体层来发射光。 荧光体层包括蓝色荧光体，其中上述荧光体用作蓝色荧光体。
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公开(公告)号：US20050277570A1
公开(公告)日：2005-12-15
申请号：US10528589
申请日：2003-10-07
CPC分类号： C09K11/7734 , H01J61/44 , H01J2211/42 , Y10T428/2991 , Y10T428/2993
摘要： The present invention aims at realizing a PDP and a mercury-free fluorescent lamp feasible to maintain excellent luminescent characteristics over long periods by suppressing time-lapse changes in luminescent characteristics of a phosphor that is excited by vacuum ultraviolet light to thereby emit light. To accomplish this object, the oxide phosphor of the invention comprises individual particles, each of which has a region at and near the surface thereof modified, and the elemental composition of the surface region is in a more oxidized state than that of the internal region of the particles. Alternatively, the surface region has more halogen or chalcogen in the elemental composition. In the phosphor treatment method of the invention, the surface region of individual phosphor particles is selectively modified by (i) forming a highly reactive gas atmosphere by exciting gas which contains reactive gas, and (ii) exposing the phosphor to the gas atmosphere.
摘要翻译： 本发明旨在实现通过抑制由真空紫外光激发的荧光体的发光特性的延时变化从而发光的方法，实现长时间保持优异发光特性的PDP和无汞荧光灯。 为了实现这个目的，本发明的氧化物荧光体包括单个颗粒，每个颗粒在其表面处和附近的区域都被修饰，并且表面区域的元素组成比内部区域的 颗粒。 或者，表面区域在元素组合物中具有更多的卤素或硫族元素。 在本发明的荧光体处理方法中，通过（i）通过激发含有反应性气体的气体形成高反应性气体气氛，并且（ii）将荧光体暴露于气体气氛，来选择性地修饰单个荧光体颗粒的表面区域。
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公开(公告)号：US20050062417A1
公开(公告)日：2005-03-24
申请号：US10928516
申请日：2004-08-27
申请人： Kojiro Okuyama , Takehiro Zukawa , Masahiro Sakai , Seigo Shiraishi , Kazuhiko Sugimoto , Masaki Aoki , Junichi Hibino
发明人： Kojiro Okuyama , Takehiro Zukawa , Masahiro Sakai , Seigo Shiraishi , Kazuhiko Sugimoto , Masaki Aoki , Junichi Hibino
IPC分类号： C09K11/08 , C09K11/55 , C09K11/59 , C09K11/64 , C09K11/67 , C09K11/68 , C09K11/77 , C09K11/80 , H01J1/62 , H01J1/63 , H01J11/00 , H01J11/22 , H01J11/24 , H01J11/34 , H01J11/42 , H01J63/04 , H01J17/49
CPC分类号： C09K11/595 , C09K11/7734 , C09K11/778 , H01J1/63 , H01J2211/42
摘要： Phosphor and a plasma display device are provided whose deterioration in brightness of phosphors and a degree of change in chromaticity are alleviated and whose discharge characteristics are improved and that has excellent initial characteristics. Phosphor of the present invention is an alkaline-earth metal aluminate phosphor containing an element M (where M denotes at least one type of element selected from the group consisting of Nb, Ta, W and B). In this phosphor, a concentration of M in the vicinity of a surface of the phosphor particles is higher than the average concentration of M in the phosphor particles as a whole. A plasma display device according to the present invention includes a plasma display panel in which a plurality of discharge cells in one color or in a plurality of colors are arranged and phosphor layers are arranged so as to correspond to the discharge cells in colors and in which light is emitted by exciting the phosphor layers with ultraviolet rays. The phosphor layers include blue phosphor, where the afore-mentioned phosphor is used as the blue phosphor.
摘要翻译： 提供了荧光体和等离子体显示装置，其荧光体的亮度劣化和色度变化程度得到缓解，其放电特性得到改善并具有优异的初始特性。 本发明的荧光体是含有元素M的碱土金属铝酸盐荧光体（其中M表示选自Nb，Ta，W和B中的至少一种元素）。 在该荧光体中，荧光体粒子表面附近的M浓度高于荧光体粒子的M的平均浓度。 根据本发明的等离子体显示装置包括等离子体显示面板，其中排列有一种颜色或多种颜色的多个放电单元，并且荧光体层被布置为与颜色的放电单元相对应，并且其中 通过用紫外线激发荧光体层来发射光。 荧光体层包括蓝色荧光体，其中上述荧光体用作蓝色荧光体。
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18.发明授权Method of manufacturing blue silicate phosphor, and blue silicate phosphor and light-emitting device 有权制造蓝色硅酸盐荧光体的方法，以及蓝色硅酸盐荧光体和发光装置公开(公告)号：US08142684B2
公开(公告)日：2012-03-27
申请号：US12299868
申请日：2007-05-16
IPC分类号： C09K11/08
CPC分类号： C09K11/7734 , C09K11/595 , C09K11/7774 , C09K11/778 , C09K11/7784 , C09K11/7797
摘要： The present invention provides a method of manufacturing a blue silicate phosphor having high luminance and a chromaticity y comparable to or lower than that of BAM:Eu. The present invention is a method of manufacturing a blue silicate phosphor represented by the general formula aAO.bEuO.(Mg1−w,Znw)O.cSiO2.dCaCl2, where A is at least one selected from Sr, Ba and Ca, and 2.970≦a≦3.500, 0.006≦b≦0.030, 1.900≦c≦2.100, 0≦d≦0.05, and 0≦w≦1 are satisfied. In this manufacturing method, heat treatment is carried out in a gas atmosphere having an oxygen partial pressure of 1×10−15.5 atm to 1×10−10 atm at a temperature of 1200° C. to 1400° C.
摘要翻译： 本发明提供一种制造与BAM：Eu相当或更低的亮度和色度y的蓝色硅酸盐荧光体的方法。 本发明是制造由通式aAO.bEuO（Mg1-w，Znw）O.cSiO2.dCaCl2表示的蓝色硅酸盐荧光体的方法，其中A为选自Sr，Ba和Ca中的至少一种，2.970 ＆nlE; a＆nlE; 3.500,0.006＆nlE; b＆nlE; 0.030，1.900＆nlE; c＆nlE; 2.100,0＆nlE; d＆nlE; 0.05和0＆nlE; w＆nlE; 1。 在该制造方法中，在1200℃〜1400℃的温度下，在氧分压为1×10-15.5atm〜1×10-10atm的气氛中进行热处理。
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公开(公告)号：US20100156266A1
公开(公告)日：2010-06-24
申请号：US11997084
申请日：2006-07-26
IPC分类号： H01J17/49
CPC分类号： H01J11/42 , C09K11/7734 , H01J1/63 , H01J11/12
摘要： A gas discharge light emitting panel is provided that prevents deterioration in display properties of the panel, which accompanies changes in light-emitting properties of phosphors. It includes a front panel and a rear panel that are disposed to oppose each other, with a discharge space being interposed therebetween, and a phosphor layer that is disposed above a principal surface located on the discharge space side of the rear panel and that emits light by being irradiated with ultraviolet rays generated in the discharge space. The phosphor layer contains first and second phosphors in which the changes in at least one property selected from luminance and chromaticity, which accompany driving of the panel, occur in the opposite directions to each other.
摘要翻译： 提供一种气体放电发光面板，其防止伴随荧光体的发光特性变化的面板的显示特性的劣化。 它包括彼此相对设置的前面板和后面板，其间插入有放电空间，以及荧光体层，其设置在位于后面板的放电空间侧的主表面上方并发出光 通过在放电空间中产生的紫外线照射。 磷光体层包含第一和第二荧光体，其中伴随着面板的驱动而选择的亮度和色度中的至少一个性质的变化发生在彼此相反的方向上。
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公开(公告)号：US20090021145A1
公开(公告)日：2009-01-22
申请号：US12278345
申请日：2007-02-07
CPC分类号： H01J11/12 , C09K11/7734 , H01J1/63 , H01J11/42 , H01J61/44
摘要： The present invention is a blue phosphor that is represented by a general formula xSrO.yEuO.MgO.zSiO2, where 2.970≦x≦3.500, 0.006≦y≦0.030, and 1.900≦z≦2.100. This blue phosphor has a crystal structure that is essentially a merwinite structure, and the crystal structure has a unit cell volume of 714.8 Å3 or less. Or, in this blue phosphor, a peak appearing around 2θ=22.86 degrees in an X-ray diffraction pattern obtained by measurement of the blue phosphor using an X-ray with a wavelength of 0.773 Å has a one-fifth value width of 0.17 degrees or less. Furthermore, the present invention is a light-emitting device having a phosphor layer including the phosphor. A suitable example of the light-emitting device is a plasma display panel.
摘要翻译： 本发明是由通式xSrO.yEuO.MgO.zSiO2表示的蓝色荧光体，其中2.970 <= x <= 3.500,0.006 <= y <= 0.030和1.900 <= z <= 2.100。 这种蓝色荧光体具有基本上为细锰矿结构的晶体结构，晶体结构的单位电池体积为714.83以下。 或者，在该蓝色荧光体中，通过使用波长为0.773的X射线测量蓝色荧光体而获得的X射线衍射图中的2θ= 22.86度附近出现的峰值的1/5值宽度为0.17度 或更少。 此外，本发明是具有包含荧光体的荧光体层的发光装置。 发光装置的合适示例是等离子体显示面板。
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