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    Pesticidal phenylcarbamoylbenzimidates
    92.
    发明授权
    Pesticidal phenylcarbamoylbenzimidates 失效
    杀虫剂苯基氨基甲酰基苯甲酰亚胺酯

    公开(公告)号：US4357347A

    公开(公告)日：1982-11-02

    申请号：US326895

    申请日：1981-12-04

    申请人： Stephen J. Nelson

    发明人： Stephen J. Nelson

    IPC分类号： A01N47/34 ,  C07C275/44 ,  A01N37/28 ,  A01N37/34 ,  C07C119/00 ,  C07C121/78

    CPC分类号： A01N47/34 ,  C07C275/44

    摘要： Phenylcarbamoylbenzimidates of the formula ##STR1## wherein X.sub.1 is selected from the group consisting of methyl, trifluoromethyl, chlorine, fluorine and bromine; X.sub.2 is selected from the group consisting of hydrogen, methyl, trifluoromethyl, chlorine, fluorine and bromine; R is alkyl of from 1 to 5 carbon atoms; X.sub.3 and X.sub.4 can be the same or different and are selected from the group consisting of hydrogen, chlorine and bromine; X.sub.5 is selected from the group consisting of hydrogen, chlorine, bromine and trifluoromethyl; and X.sub.6 is selected from the group consisting of cyano and nitro; with the proviso that when X.sub.1 and X.sub.2 are chlorine or when X.sub.1 is fluorine and X.sub.2 is hydrogen then R, X.sub.3, X.sub.4, X.sub.5 and X.sub.6 are respectively not 1-methylethyl, chlorine, hydrogen, chlorine and nitro; with the further proviso that when X.sub.1 is fluorine and X.sub.2 is hydrogen then R, X.sub.3, X.sub.4, X.sub.5 and X.sub.6 are respectively not 1-methylethyl, chlorine, hydrogen, hydrogen and nitro; and with the further proviso that when X.sub. 1 is florine or methyl and X.sub.2 is hydrogen then R, X.sub.3, X.sub.4, X.sub.5 and X.sub.6 are respectively not ethyl, hydrogen, hydrogen, hydrogen and nitro; and with the proviso that when X.sub.1 and X.sub.2 are florine, then R, X.sub.3, X.sub.4, X.sub.5 and X.sub.6 are respectively not ethyl, chlorine, hydrogen, chlorine and nitro.

    摘要翻译： 其中X 1选自甲基，三氟甲基，氯，氟和溴的下式的苯基氨基甲酰基苯甲亚胺： X 2选自氢，甲基，三氟甲基，氯，氟和溴; R是1至5个碳原子的烷基; X3和X4可以相同或不同，并且选自氢，氯和溴; X5选自氢，氯，溴和三氟甲基; X 6选自氰基和硝基; 条件是当X1和X2为氯时，或当X1为氟且X2为氢时，则R，X3，X4，X5和X6分别不为1-甲基乙基，氯，氢，氯和硝基; 进一步的条件是当X1是氟并且X2是氢时，则R，X3，X4，X5和X6分别不是1-甲基乙基，氯，氢，氢和硝基; 并且进一步的条件是当X 1为氟或甲基且X 2为氢时，则R，X 3，X 4，X 5和X 6分别不是乙基，氢，氢，氢和硝基; 并且条件是当X1和X2是氟，则R，X3，X4，X5和X6分别不是乙基，氯，氢，氯和硝基。

    Preparation of perchloro-2,5-diaza-1,5-hexadiene
    93.
    发明授权
    Preparation of perchloro-2,5-diaza-1,5-hexadiene 失效
    全氯-2,5-二氮杂-1,5-己二烯的制备

    公开(公告)号：US4225510A

    公开(公告)日：1980-09-30

    申请号：US974413

    申请日：1978-12-29

    申请人： Hermann D. Krall ,  Herbert Schwarz

    发明人： Hermann D. Krall ,  Herbert Schwarz

    IPC分类号： C07C211/24 ,  C07C20060101 ,  C07C67/00 ,  C07C209/00 ,  C07C241/00 ,  C07C251/02 ,  C07C119/00

    CPC分类号： C07C2101/04

    摘要： In the preparation of perchloro-2,5-diaza-1,5-hexadiene by chlorination of N,N-dimethylaminoacetonitrile, the improvement which comprises in a first stage (a) chlorinating N,N-dimethylaminoacetonitrile or its hydrochloride at about 70.degree. to 80.degree. C. in a solvent, removing the solvent by distillation under chlorinating conditions until a bottom temperature of about 120.degree. to 160.degree. is reached, and after-treating the residual reaction at this temperature with chlorine, and in a second stage (b) chlorinating the resulting reaction mixture at a temperature from about 150.degree. to 220.degree. C. Advantageously the solvent in stage (a) is phosphorus oxychloride, the weight ratio of nitrile to solvent is about 1:3, the after-chlorination in stage (a) is carried out at a temperature from about 120.degree. to 140.degree. C., and stage (b) is carried out at a temperature from about 180.degree. to 210.degree. C. in a multi-stage bubble column cascade reactor operated with gas and liquid in counter-current.

    摘要翻译： 在通过氯化N，N-二甲基氨基乙腈制备全氯-2,5-二氮杂-1,5-己二烯时，其改进包括在第一阶段（a）在约70℃下将N，N-二甲基氨基乙腈或其盐酸盐氯化 至80℃，在氯化条件下通过蒸馏除去溶剂，直到达到约120〜160℃的底部温度，并在该温度下用氯处理残留反应，在第二阶段 b）在约150℃至220℃的温度下对所得反应混合物进行氯化。有利的是（a）阶段中的溶剂是三氯氧化磷，腈与溶剂的重量比约为1:3，后处理阶段 （a）在约120℃至140℃的温度下进行，并且阶段（b）在约180℃至210℃的温度下进行，在多级鼓泡塔级联反应器中操作， 气体和液体逆流。

    Substituted cyanamidic compounds
    95.
    发明授权
    Substituted cyanamidic compounds 失效
    取代的氰氨基化合物

    公开(公告)号：US4048228A

    公开(公告)日：1977-09-13

    申请号：US758617

    申请日：1977-01-12

    申请人： James P. Shoffner

    发明人： James P. Shoffner

    IPC分类号： C07C119/00

    CPC分类号： C07D251/16 ,  Y02P20/582

    摘要： Substituted cyanamidic compounds as exemplified by N-(diphenylmethylidene)cyanamide may be prepared by reacting nitrogen-containing compounds having the formula: ##STR1## in which R.sub.1 and R.sub.2 are selected from the group consisting of hydrogen, aryl, alkyl possessing from 1 to about 30 carbon atoms, cycloalkyl possessing from about 5 to about 12 carbon atoms in the ring, alkyl-substituted cycloalkyl, aryl-substituted cycloalkyl, alkaryl and aralkyl radicals and R.sub.3 is selected from the group consisting of hydrogen, alkyl possessing from 1 to about 30 carbon atoms, aryl, cycloalkyl possessing from 5 to about 12 carbon atoms in the ring, alkyl-substituted cycloalkyl, aryl-substituted cycloalkyl and bicycloalkyl radicals with cyanamide and a compound selected from the group consisting of an acid-acting compound, an alkyl halide and an alkyl sulfate.

    摘要翻译： 通过N-（二苯基亚甲基）氨基氰示例的取代的氰酰胺化合物可以通过使具有下式的含氮化合物：其中R 1和R 2选自氢，芳基，具有1至约 30个碳原子，环中具有约5至约12个碳原子的环烷基取代的环烷基，芳基取代的环烷基，烷芳基和芳烷基，R 3选自氢，具有1至约30个 碳原子，芳基，环中具有5至约12个碳原子的环烷基取代的环烷基，芳基取代的环烷基和双环烷基与氰酰胺和选自酸作用化合物，烷基卤化物 和烷基硫酸盐。

    Preparation of carbodiimides from ureas by dehydration
    98.
    发明授权
    Preparation of carbodiimides from ureas by dehydration 失效
    通过脱水从尿素制备碳二亚胺

    公开(公告)号：US3972933A

    公开(公告)日：1976-08-03

    申请号：US473616

    申请日：1974-05-28

    申请人： Ernest L. Lawton

    发明人： Ernest L. Lawton

    IPC分类号： C07C273/18 ,  C07C275/28 ,  D06M13/395 ,  C07C119/00

    CPC分类号： C07C267/00 ,  C07C273/1827 ,  D06M13/395

    摘要： Biscarbodiimides which are known to be effective as a surface application for polyethylene terephthalate fibers in lowering carboxyl end group concentration of the fibers and increasing hydrolytic stability, are prepared by the dehydration of ureas with triphenylphosphine and carbon tetrachloride.

    摘要翻译： 通过用三苯基膦和四氯化碳脱水来制备已知作为聚对苯二甲酸乙二醇酯纤维降低纤维的羧基端基浓度和增加水解稳定性的表面应用的双碳二亚胺。

    Nitrone compounds
    100.
    发明授权
    Nitrone compounds 失效
    硝基化合物

    公开(公告)号：US3917700A

    公开(公告)日：1975-11-04

    申请号：US43807874

    申请日：1974-01-30

    申请人： GOODYEAR TIRE & RUBBER

    发明人： AUERBACH MELVIN

    IPC分类号： C07C291/02 ,  C07C119/00

    CPC分类号： C07C291/02

    摘要： Compositions of matter corresponding to the general formula

    WHEREIN R is selected from a group consisting of alkyl radicals, cycloalkyl radicals, phenyl radicals and substituted phenyl radicals.

    摘要翻译： 对应于通式为WHEREIN R的物质组成选自烷基，环烷基，苯基和取代的苯基。