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    Copolymers Containing Nanoparticles
    3.
    发明申请
    Copolymers Containing Nanoparticles 失效
    含有纳米粒子的共聚物

    公开(公告)号：US20080146743A1

    公开(公告)日：2008-06-19

    申请号：US11722567

    申请日：2005-12-22

    申请人： Oliver Minge ,  Richard Weidner ,  Frank Sandmeyer ,  Hans-Peter Weitzel

    发明人： Oliver Minge ,  Richard Weidner ,  Frank Sandmeyer ,  Hans-Peter Weitzel

    IPC分类号： C08F261/00

    CPC分类号： C09C1/3081 ,  C01P2004/64 ,  C08F2/22 ,  C08F4/40 ,  C08F218/08 ,  C08F220/14 ,  C08F220/18 ,  C08F230/08 ,  C08F283/12 ,  C08F292/00 ,  C08L51/085 ,  C09D133/06 ,  Y10T428/2995 ,  Y10T428/2998 ,  C08L2666/02

    摘要： Copolymers of ethylenically unsaturated monomers and ethylenically functionalized nanoparticles in the form of aqueous polymer dispersions or water-redispersible polymer powders, are obtained by aqueous free-radically polymerizing and optionally drying a copolymerizate of,A) one or more ethylenically unsaturated monomers in the presence of B) particles having an average diameter of ≦1000 nm, functionalized with ethylenically unsaturated, free-radically polymerizable groups, wherein B1) particles are metal oxides or semimetal oxides, and/or B2) particles are silicone resins and where B1) and B2) are functionalized with one or more α-organosilanes of the formula (R1O)3−n(R2)nSi—(CR32)—X (I), where X is a radical having 2 to 20 hydrocarbon atoms containing an ethylenically unsaturated group.

    摘要翻译： 通过水溶液自由基聚合和任选地干燥A）一种或多种烯键式不饱和单体的共聚物，在存在下共聚物的情况下获得烯键式不饱和单体和烯键式官能化纳米颗粒的聚合物分散体或水可再分散聚合物粉末形式的共聚物 B）具有平均直径<= 1000nm的颗粒，用烯属不饱和的可自由基聚合的基团官能化，其中B1）颗粒是金属氧化物或半金属氧化物，和/或B2）颗粒是有机硅树脂，其中B1）和B2 ）用一种或多种下式的α-有机硅烷（R 1 O 3）3-n（R 2）n n进行官能化 X（I），其中X是含有烯属不饱和基团的具有2-20个烃基的基团。

    Process for preparing lattices stabilized by polyvinyl alcohol
    5.
    发明申请
    Process for preparing lattices stabilized by polyvinyl alcohol 有权
    制备由聚乙烯醇稳定的晶格的方法

    公开(公告)号：US20070112117A1

    公开(公告)日：2007-05-17

    申请号：US11600537

    申请日：2006-11-16

    申请人： Hans-Peter Weitzel

    发明人： Hans-Peter Weitzel

    IPC分类号： C08F2/16

    CPC分类号： C08F2/20

    摘要： A process for preparing polymer dispersions stabilized by polyvinyl alcohol includes a step of emulsion polymerization. The polymerization occurs such that at least 60% of the total conversion occurs at a temperature from 100° C. to 140° C.

    摘要翻译： 用于制备由聚乙烯醇稳定的聚合物分散体的方法包括乳液聚合的步骤。 发生聚合使得总转化率的至少60％在100℃至140℃的温度下进行。

    Redispersion powder composition with a binding acceleration effect
    6.
    发明申请
    Redispersion powder composition with a binding acceleration effect 有权
    再分散粉末组合物具有结合加速效果

    公开(公告)号：US20070037925A1

    公开(公告)日：2007-02-15

    申请号：US10553310

    申请日：2004-03-04

    申请人： Hans-Peter Weitzel ,  Hermann Lutz ,  Peter Fritze

    发明人： Hans-Peter Weitzel ,  Hermann Lutz ,  Peter Fritze

    IPC分类号： C08L31/00

    CPC分类号： C04B40/0042 ,  C04B28/02 ,  C04B2103/0057 ,  C04B2111/00146 ,  C04B22/10 ,  C04B24/24 ,  C04B24/2623 ,  C04B2103/10 ,  C04B22/085 ,  C04B22/16 ,  C04B24/04

    摘要： Water-redispersible polymer powder compositions based on a) homo- or copolymers of one or more monomers from the group consisting of vinyl esters of unbranched or branched C1-15 alkylcarboxylic acids methacrylic esters and acrylic esters of C1-15 alcohols, vinylaromatics, olefins, dienes, and vinyl halides, with one or more protective colloids, and optionally, one or more antiblocking agents, in conjunction with one or more alkali metal or alkaline earth metal C1-4 carboxylates as setting accelerants added follwoing polymerization accelerate the setting of construction chemistry products with hydraulically setting binders.

    摘要翻译： 基于以下的水可再分散性聚合物粉末组合物：a）一种或多种单体的均聚物或共聚物，所述单体来自由无支链或支链C 1-15烷基羧酸的甲基丙烯酸酯和C的丙烯酸酯组成的组 乙烯基芳烃，烯烃，二烯和卤乙烯与一种或多种保护胶体和任选的一种或多种防粘连剂结合一种或多种碱金属或碱土金属 C 1-4羧酸盐作为固化促进剂，加入聚合后加速了水硬性粘合剂的施工化学产品的凝固。

    Process for preparing protective-colloid-stabilized polymers by continuous emulsion polymerization
    7.
    发明授权
    Process for preparing protective-colloid-stabilized polymers by continuous emulsion polymerization 有权

    公开(公告)号：US06664322B2

    公开(公告)日：2003-12-16

    申请号：US09891561

    申请日：2001-06-26

    申请人： Hans-Peter Weitzel

    发明人： Hans-Peter Weitzel

    IPC分类号： C08F216

    CPC分类号： C08L51/003 ,  C08F218/04 ,  C08F218/08 ,  C08F263/04 ,  C08L23/0869 ,  C08L29/04 ,  C08L2666/02 ,  C09D151/003 ,  C09J151/003 ,  C08L2666/04 ,  C08F210/02

    摘要： A process for preparing polyvinyl-alcohol-stabilized polymers based on vinyl ester, ethylene, and optionally other comonomers, in the form of aqueous polymer dispersions or water-redispersible polymer powders, by means of free radical initiated continuous emulsion polymerization and optionally drying the resultant polymer dispersion, comprising carrying out the emulsion polymerization in minimally two pressurized reactors arranged in series at a temperature of from 40° C. to 100° C. and at a pressure of from 5 to 100 bar, to a residual monomer content less than 3% by weight, and continuing the polymerization in minimally one unpressurized reactor at a temperature of from 20° C. to 60° C. and at a pressure of less than 1.0 bar, wherein the polymerization is initiated using a redox system made from an oxidizing component and a reducing component, at least a portion of the reducing component introduced within the first pressurized reactor.

    Vinylaromatic/1,3-diene copolymer stabilized with protective colloids as adhesives for porous substrates
    8.
    发明授权
    Vinylaromatic/1,3-diene copolymer stabilized with protective colloids as adhesives for porous substrates 失效
    用保护胶体稳定的乙烯基芳烃/ 1,3-二烯共聚物作为多孔基材的粘合剂

    公开(公告)号：US06656983B1

    公开(公告)日：2003-12-02

    申请号：US09856538

    申请日：2001-08-01

    申请人： Theo Mayer ,  Thomas Kohler ,  Reinhard Harzschel ,  Hans-Peter Weitzel ,  Bernd Schilling

    发明人： Theo Mayer ,  Thomas Kohler ,  Reinhard Harzschel ,  Hans-Peter Weitzel ,  Bernd Schilling

    IPC分类号： C08L100

    CPC分类号： C09J125/10 ,  C08F236/10 ,  C08L2666/02 ,  C09J109/06

    摘要： The invention provides mixed aromatic vinyl-1,3-diene polymers stabilized by a protective colloid and present in the form of aqueous polymer dispersions or polymer powders redispersible in water as adhesives for porous substrates. The polymer dispersions and the polymer powders are obtained by emulsion polymerization of a mixture containing: a) 20 to 80 percent by weight of one or more vinylaromatics; b) 19.9 to 79.9 percent by weight of one or more 1,3-dienes; c) 0.1 to 15 percent by weight of one or more comonomers from the group consisting of N-methylolacrylamide, N-methylolmethacrylamide and the N-(alkoxymethyl)-acrylamides and N-(alkoxymethyl)-methacrylamides with a C1 to C6-alkyl radical. The sum of the above percentages adds up to 100% by weight. Emulsion polymerization is carried out in the presence of one or more protective colloids and without emulsifiers, optionally followed by drying of the resulting aqueous polymer dispersion.

    摘要翻译： 本发明提供了由保护胶体稳定并以聚合物水分散体形式存在的混合芳族乙烯基-1,3-二烯聚合物或可再分散在水中的聚合物粉末作为多孔基材的粘合剂。 聚合物分散体和聚合物粉末通过混合物的乳液聚合获得，所述混合物包含：a）20至80重量％的一种或多种乙烯基芳烃; b）19.9至79.9重量％的一种或多种1,3-二烯; c）0.1至15重量％的来自由N-羟甲基丙烯酰胺，N-羟甲基甲基丙烯酰胺和N-（烷氧基甲基） - 丙烯酰胺和具有C 1至C 6 - 烷基的N-（烷氧基甲基） - 甲基丙烯酰胺组成的组中的一种或多种共聚单体 。 上述百分比的总和高达100重量％。 乳液聚合在一种或多种保护胶体和不含乳化剂的存在下进行，任选然后干燥所得的聚合物水分散体。

    Process for the preparation of polymers having a reduced content of volatile components
    9.
    发明授权
    Process for the preparation of polymers having a reduced content of volatile components 失效
    制备挥发性组分含量降低的聚合物的方法

    公开(公告)号：US06639049B2

    公开(公告)日：2003-10-28

    申请号：US10046320

    申请日：2001-11-09

    申请人： Hans-Peter Weitzel

    发明人： Hans-Peter Weitzel

    IPC分类号： C08G6400

    CPC分类号： C08F6/006 ,  C04B24/2641 ,  C04B40/0042 ,  C04B2103/0057 ,  C04B2111/00482 ,  C04B2111/00663 ,  C08F6/003 ,  C08J3/122 ,  C04B20/023 ,  C04B24/2623 ,  C04B24/2688

    摘要： The invention relates to a process for the preparation of polymers stabilized with protective colloids in the form of water-redispersible powders or aqueous dispersions thereof having a reduced content of volatile components, by a) polymerizing by emulsion or suspension polymerization, one or more monomers from the group consisting of vinyl esters, (meth)acrylates, vinyl aromatics, olefins, 1,3-dienes and vinyl halides and optionally further monomers copolymerizable therewith, b) aftertreating the polymer dispersion thus obtained by means of postpolymerization, distillation, and/or introduction of steam or inert gas to obtain a residual content of volatile, nonaqueous components of 120° C., and optimally d) redispersing of the resulting powder in water.

    摘要翻译： 本发明涉及一种用保护性胶体稳定的聚合物的方法，该保护性胶体为具有降低的挥发性成分含量的水分散性粉末或其水分散体的形式，其通过乳液或悬浮聚合聚合，一种或多种来自 由乙烯基酯，（甲基）丙烯酸酯，乙烯基芳族化合物，烯烃，1,3-二烯和乙烯基卤化物组成的组和任选的可与其共聚的其它单体组成的组，b）通过后聚合，蒸馏和/或引入后处理得到的聚合物分散体 的蒸汽或惰性气体，以获得<2000PPM的挥发性非水成分的残留含量，ANDc）将后处理的聚合物分散体喷雾干燥至<400ppm的挥发性非水性组分的残留量，在喷雾干燥前调节分散体 在喷雾之前的固体含量<45重量％，在入口温度> 120℃下用气体进行喷雾干燥 C.，并优化）将所得粉末再分散在水中。

    Method for producing polymers stabilized with protective colloids
    10.
    发明授权
    Method for producing polymers stabilized with protective colloids 有权
    制备保护胶体稳定聚合物的方法

    公开(公告)号：US06300403B1

    公开(公告)日：2001-10-09

    申请号：US09424193

    申请日：1999-11-19

    申请人： Theo Mayer ,  Hans-Peter Weitzel ,  Reinhard Haerzschel ,  Thomas Bastelberger

    发明人： Theo Mayer ,  Hans-Peter Weitzel ,  Reinhard Haerzschel ,  Thomas Bastelberger

    IPC分类号： C08F220

    CPC分类号： C08F2/24 ,  C08F6/24 ,  C08F236/10 ,  C08F2/20

    摘要： A method for producing protective-colloid-stabilized polymers in the form of their aqueous polymer dispersions or in the form of powders which can be re-dispersed in water, wherein one or several monomers from the group made up of vinyl aromatics, 1.3 dienes, acrylic acid esters and methacrylic acid esters of alcohols with 1 to 15 C-atoms are polymerized in the presence of a combination of protective colloids consisting of one or several protective colloids from the group of hydrophobically modified, partly saponified polyvinyl esters which produce a surface tension of ≦40 mN/m as a 2% aqueous solution, and one or several protective colloids which produce a surface tension of >40 mN/m as a 2% aqueous solution.

    摘要翻译： 一种制备其聚合物水分散体形式的保护胶体稳定的聚合物的方法，或以可再分散在水中的粉末形式的方法，其中一种或多种由乙烯基芳族化合物，1,3-二烯， 丙烯酸酯和具有1至15个C原子的醇的甲基丙烯酸酯在由一种或几种由疏水改性的部分皂化聚乙烯基酯组成的保护胶体组合的存在下聚合，产生表面张力 作为2％水溶液<= 40mN / m，作为2％水溶液产生表面张力> 40mN / m的一种或几种保护胶体。