Method for continuously generating silicon monoxide gas

    公开(公告)号:US12024437B2

    公开(公告)日:2024-07-02

    申请号:US17563129

    申请日:2021-12-28

    发明人: Yusuke Kashitani

    IPC分类号: C01B33/113

    CPC分类号: C01B33/113 C01B2210/0009

    摘要: In a method for continuously generating silicon monoxide (SiO) gas, wherein a silicon monoxide gas-generating raw material in a raw material supply unit is continuously charged into a reaction chamber RM, an inert gas is flowed through the raw material supply unit so as to be directed toward the charging direction of the silicon monoxide gas-generating raw material. The method for continuously generating silicon monoxide gas prevents a decrease in yield of the silicon monoxide (SiO) gas-generating raw material.

    METHOD FOR CONTINUOUSLY GENERATING SILICON MONOXIDE GAS

    公开(公告)号:US20230202848A1

    公开(公告)日:2023-06-29

    申请号:US17563129

    申请日:2021-12-28

    发明人: Yusuke KASHITANI

    IPC分类号: C01B33/113

    CPC分类号: C01B33/113 C01B2210/0009

    摘要: In a method for continuously generating silicon monoxide (SiO) gas, wherein a silicon monoxide gas-generating raw material in a raw material supply unit is continuously charged into a reaction chamber RM, an inert gas is flowed through the raw material supply unit so as to be directed toward the charging direction of the silicon monoxide gas-generating raw material. The method for continuously generating silicon monoxide gas prevents a decrease in yield of the silicon monoxide (SiO) gas-generating raw material.

    METHOD FOR PREPARING TWO-DIMENSIONAL ORDERED MESOPOROUS NANOSHEETS BY INORGANIC SALT INTERFACE-INDUCED ASSEMBLY

    公开(公告)号:US20220194811A1

    公开(公告)日:2022-06-23

    申请号:US17603587

    申请日:2020-03-09

    申请人: FUDAN UNIVERSITY

    摘要: A method for preparing two-dimensional (2D) ordered mesoporous nanosheets by inorganic salt interface-induced assembly includes the following steps: carrying out, by using a soluble inorganic salt as a substrate and an amphiphilic block copolymer as a template, uniform mass diffusion of a target precursor solution at an inorganic salt crystal interface through vacuum filtration or low-speed centrifugation; forming a single-layer ordered mesoporous structure by using the solvent evaporation-induced co-assembly (EICA) technology; and promoting, through gradient temperature-controlled Ostwald ripening, the evaporation and induced formation of an organic solvent, and removing the template in N2 to obtain a 2D single-layer ordered mesoporous nanosheet material. The assembled nanosheet material has a large pore size, regular spherical pores and orderly arrangement. By changing the type of the precursor, a variety of mesoporous metal oxides, metal elements, inorganic non-metal nanosheets are synthesized.

    High energy, long cycle life electrode for lithium-ion batteries

    公开(公告)号:US10714745B2

    公开(公告)日:2020-07-14

    申请号:US15663268

    申请日:2017-07-28

    摘要: Anodes for electrochemical cells and batteries are described herein. In particular, and anode comprises silicon oxide particles on a transition metal current collector (e.g., copper, nickel, copper alloy, and the like), wherein the particles comprise nanocrystalline domains of silicon dispersed within a silicon oxide matrix. The particles do not include a metal oxide coating, and are produced by heating a silicon monoxide powder at a temperature in the range of about 400 to about 1100° C. under an inert atmosphere for about 2 to about 20 hours. In some embodiments, the particles are free from a metal oxide coating and have an average diameter of about 20 to 10000 nm; the nanocrystalline domains of silicon comprise about 10 to about 90 mole percent of the particles; and the nanocrystalline domains have dimensions of about 0.2 to about 50 nm in average diameter.