3,3'-Dichloro-4,4-diaminodiphenyl sulfonic acids
    1.
    发明授权
    3,3'-Dichloro-4,4-diaminodiphenyl sulfonic acids 失效
    3,3'-二氯-4,4-二氨基二苯基磺酸

    公开(公告)号:US4892968A

    公开(公告)日:1990-01-09

    申请号:US226008

    申请日:1988-07-29

    CPC classification number: C09B35/105

    Abstract: The invention provides compounds having the formula I or II ##STR1## and their salts and hydrates, having high value as intermediates for dyestuff additives for pigment compositions and as intermediates for metal-containing pigments.

    Abstract translation: 本发明提供具有式I或II(II)的化合物及其盐和水合物,其作为颜料组合物的染料添加剂和含金属颜料的中间体具有高价值的中间体。

    Diaryl pigments with improved heat stability obtained by coupling
bis-diazotized diamines with acetoacetanilides
    2.
    发明授权
    Diaryl pigments with improved heat stability obtained by coupling bis-diazotized diamines with acetoacetanilides 失效
    通过将双重重氮化二胺与乙酰乙酰苯胺偶联获得的具有改善的热稳定性的二芳基颜料

    公开(公告)号:US4665163A

    公开(公告)日:1987-05-12

    申请号:US507711

    申请日:1983-06-23

    CPC classification number: C09B35/105

    Abstract: Diaryl pigments having an excellent stability to heat are obtained by carrying out the coupling of bis-diazotized 3,3'-dichloro-4,4'-diaminobiphenyl with acetoacetanilides in the presence of an added quantity of acetoacetanilides which are monosubstituted or disubstituted in the 3-position or 4-position of the nucleus. As a result of their good heat stability, these pigments are particularly suitable for pigmenting plastics having processing temperatures above 200.degree. C.

    Abstract translation: 通过在添加量的乙酰乙酰苯胺的存在下进行双重重氮化的3,3'-二氯-4,4'-二氨基联苯与乙酰乙酰苯胺的偶合获得具有优异的耐热稳定性的二芳基颜料,所述乙​​酰乙酰替苯胺在 核的3位或4位。 由于其良好的热稳定性,这些颜料特别适用于加工温度高于200℃的着色塑料。

    Benzidine yellow type pigment
    3.
    发明授权
    Benzidine yellow type pigment 失效
    BENZIDINE黄色颜料

    公开(公告)号:US3719658A

    公开(公告)日:1973-03-06

    申请号:US3719658D

    申请日:1969-03-12

    Applicant: HERCULES INC

    Inventor: CONLEY J

    CPC classification number: C09B35/105

    Abstract: IS PRODUCED BY TETRAZOTIZING 3,3'',5,5''-TETRACHLOROBENZIDINE AND THEN COUPLING THE TETRAZOTIZED PRODUCT WITH ACETO-ACET-OPHENETIDIDE. In a preferred method N,N''-diacetyl-3,3'',5,5''tetrachlorobenzidine is hydrolyzed to the corresponding amine in situ in the acid solution which is to be used for the tetrazotizing step.

    A benzidine yellow type pigment of unusually good lightfastness and superior strength is described. The pigment, which is a compound of the formula

    Process for the production of dis-azo pigment whose amine content is
small, and pigment produced by said process
    7.
    发明授权
    Process for the production of dis-azo pigment whose amine content is small, and pigment produced by said process 失效
    用于生产胺含量小的偶氮颜料的制备方法和由所述方法生产的颜料

    公开(公告)号:US5489672A

    公开(公告)日:1996-02-06

    申请号:US329234

    申请日:1994-10-26

    CPC classification number: C09B35/035 C09B35/105 C09B67/0096

    Abstract: A process for the production of a dis-azo pigment which is excellent in sanitary condition and almost free of a residual coupler component and decomposition products derived from the residual coupler component, and has a reduced aromatic amine content, and a dis-azo pigment produced by the said process, the process comprising the steps of (a) coupling-reacting a solution of a tetrazonium salt of benzidine with a slurry of acetoacetanilide of which the amount is stoichiometrically excess relative to an amount of said tetrazonium salt, to prepare a dis-azo pigment slurry, and (b) adding a halogen to the dis-azo pigment slurry to treat the acetoacetanilide in said slurry.

    Abstract translation: 一种生产偶氮颜料的方法,其具有优异的卫生条件,几乎不含残留的成色剂成分和残留的成色剂成分的分解产物,芳族胺含量降低,产生的偶氮颜料 通过所述方法,所述方法包括以下步骤:(a)将联苯胺的四唑鎓盐溶液与相对于所述四唑鎓盐的量的化学计量过量的乙酰乙酰苯胺的浆料偶联反应,以制备dis - 颜料色浆,和(b)将卤素加入到偶氮颜料浆料中以处理所述浆料中的乙酰乙酰苯胺。

    Modified form of a disazo pigment
    9.
    发明授权
    Modified form of a disazo pigment 失效
    改性形式的双偶氮颜料

    公开(公告)号:US3974136A

    公开(公告)日:1976-08-10

    申请号:US434039

    申请日:1974-01-17

    CPC classification number: C09B35/105 C09B67/0015

    Abstract: The disazo pigment of the formula ##SPC1##Characterized by a specific surface of 12 - 20, preferably 13 - 18 m.sup.2 /g, a maximum of the distribution of the grain sizes of between 500 and 1000 nm and a proportion of these grain sizes in the total distribution of between 35 and 65 %. This disazo pigment is obtained by isolating the pigment, after coupling, by stirring it out with alkali and, after having filtered it and washed it to neutrality, heating it to temperatures above 100.degree. C in a mixture of water and a solvent which is immiscible with water or miscible with water to a limited degree only.

    Abstract translation: 由12 - 20特定表面表征的配方的双偶氮颜料,优选13 - 18 M2 / G,最大分配500和1000 NM之间的颗粒尺寸,以及总分布中这些颗粒尺寸的比例 35%至65%之间。 这种双偶氮颜料是通过在偶联后通过将其与碱反应来分离颜料而获得的,并且在将其过滤并将其洗涤至中性后,将其加热至高于100℃的水和溶剂的混合物中,所述混合物是不混溶的 用水或与水混合在一定程度上。

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