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公开(公告)号：US20120296097A1
公开(公告)日：2012-11-22
申请号：US13516775
申请日：2009-12-17
Applicant: Dezhi Xiang , Dejun Yan , Chongli Xu , Ying Shao , Ping Fu , Hongwei Wang , Shunli Su , Jiarong Wei , Changjing Wang , Qinghe Shang , Jian Li , Yan Dou , Hui Du , Jinchao Miao , Hui Liu , Yongwei Li , Lianfeng Li , Yongmei Xu , Mei Zhang , Xianxu Zhang
Inventor： Dezhi Xiang , Dejun Yan , Chongli Xu , Ying Shao , Ping Fu , Hongwei Wang , Shunli Su , Jiarong Wei , Changjing Wang , Qinghe Shang , Jian Li , Yan Dou , Hui Du , Jinchao Miao , Hui Liu , Yongwei Li , Lianfeng Li , Yongmei Xu , Mei Zhang , Xianxu Zhang
IPC: C09B5/28
CPC classification number: C07D209/80 , C09B1/005 , C09B1/42 , C09B1/516 , C09B5/2436 , C09B5/26 , C09B5/28 , C09B67/0077 , D06P1/24 , D06P3/6025
Abstract: A preparation method of original dye of Vat Brown R comprises the following steps: a. after acylation of 1,5-diaminoanthraquinone, 1-amino-5-benzamidoanthraquinone was prepared by acidic hydrolysis; b. 1-benzamido-4-bromoanthraquinone was obtained from 1-aminoanthraquinone by acylation and bromination; c. a condensate of Vat Brown R was obtained by condensation reaction of 1-amino-5-benzamidoanthraquinone and 1-benzamido-4-bromoanthraquinone; d. the original dye of Vat Brown R was obtained from the condensate of Vat Brown R by ring closing reaction and oxidation reaction. The method omits one oxidation step, economizes significant amount of oxidizing agent, and reduces significant amount of waste water, so it is very beneficial to environment protection; and the method also exhibited the advantages of highly increasing product yield and reducing the costs of raw materials to an extent of more than 30%.
Abstract translation: 瓦特棕R原染料的制备方法包括以下步骤：a。 酰化1,5-二氨基蒽醌后，通过酸性水解制备1-氨基-5-苯甲酰氨基蒽醌; b。 通过酰化和溴化从1-氨基蒽醌得到1-苯甲酰氨基-4-溴蒽醌; C。 通过1-氨基-5-苯甲酰氨基蒽醌和1-苯甲酰氨基-4-溴蒽醌的缩合反应获得瓦特棕色R的缩合物; d。 通过闭环反应和氧化反应从瓦特布朗R的缩合物获得了原始的Vat Brown R染料。 该方法省略了一个氧化步骤，节省了大量的氧化剂，减少了大量的废水，对环境保护非常有利; 该方法还显示出产品产量大幅提高，原料成本降低30％以上的优点。
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公开(公告)号：US3741720A
公开(公告)日：1973-06-26
申请号：US3741720D
申请日：1970-10-12
Applicant: BAYER AG
Inventor： NEEFF R , HEDERICH V , GEHRKE G
Abstract: THE CONTINOUS DYEING OF SYBTHETIC FIBRE MATERIALS FROM ORGANIC SOLVENTS. THE FIBRE MATERIALS ARE IMPREGNATED WITH DYE LIQUORS WHICH CONTAIN ANTHRAQUINONE DYESTUFFS OF THE FORMULA
1-(R1-NH-),4-(R-CO-NH-)ANTHRAQUINONE
IN WHICH R REPRESENTS A C1-C17-ALKYL RADICAL, AN ARALKYL OR OPTINALLY SUBSTITUTED ARYL RADICAL AND R1 STANDS FOR AN ALKYL RADICAL WHICH MAY BE SUBSTITUTED BY ALKOXY OR ALKYLAMINO GROUPS, FOR A CYCLOALKYL, ARALKYL OR FOR AN OPTIONALLY SUBSTITUTED ARYL RADICAL, AND SUBEQUENTLY SUBJUCTED TO A HEAT TREATMENT.-
公开(公告)号：US3651099A
公开(公告)日：1972-03-21
申请号：US3651099D
申请日：1968-04-02
Applicant: GAF CORP
Inventor： PERLINGER HANS L , MILAZZO JOSEPH S
IPC: C09B1/42
CPC classification number: C09B1/42
Abstract: A PROCESS FOR PRODUCING MONOACYLATED DERIVATIVES OF DIAMINOANTHRAQUINONES COMPRISING REACTING THE DIAMINOANTHRAQUINONE WITH BENZOYL CHLORIDE OR A MIXTURE OF BENZOIC ACID AND AN INORGANIC ACID CHLORIDE IN THE PRESENCE OF AN N,N-DIALKYL CARBOXYLIC ACID AMIDE.
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公开(公告)号：US3639430A
公开(公告)日：1972-02-01
申请号：US3639430D
申请日：1968-01-16
Applicant: CIBA LTD
Inventor： ALTERMATT HANS
IPC: C07C50/34 , C09B1/00 , C09B1/16 , C09B1/36 , C09B1/42 , C09B1/43 , C09B1/46 , C09B1/467 , C09B1/48 , C09B1/54 , C09B1/56 , C09B1/58 , C09B3/00 , C09B3/64 , C09B3/68 , C09B5/00 , C09B5/10 , C09B5/14 , C09B5/28 , C09B5/36 , C09B5/62 , C09B6/00 , C09B9/00 , C09B43/36 , C09B49/00 , C09B56/12 , C09B57/12 , C09B62/00 , C09B62/004 , C09B62/006 , C09B62/024 , C09B62/04 , C09B62/06 , C09B62/44 , D06P1/38
CPC classification number: D06P1/38 , C07C243/00 , C09B1/36 , C09B1/42 , C09B1/43 , C09B1/46 , C09B1/467 , C09B1/48 , C09B1/547 , C09B1/58 , C09B1/585 , C09B3/00 , C09B3/64 , C09B3/68 , C09B5/00 , C09B5/10 , C09B5/14 , C09B5/28 , C09B5/36 , C09B5/62 , C09B6/00 , C09B9/00 , C09B43/36 , C09B49/00 , C09B56/12 , C09B57/12 , C09B62/00 , C09B62/004 , C09B62/0068 , C09B62/024 , C09B62/06 , C09B62/4409 , C09B62/4422 , Y10S8/918
Abstract: NEW WATER-SOLUBLE VAT DYESTUFFS CONTAINING ARYLOXY-OR ARYLMERCAPTO GROUPS AND TWO ANTHRAQUINONE RADICALS OR A VATTABLE CHROMOPHOR CONTAINING AT LEAST 4 FUSED RINGS.
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Patent Agency Ranking6.发明授权
公开(公告)号：US3356693A
公开(公告)日：1967-12-05
申请号：US33829864
申请日：1964-01-17
Applicant: CIBA LTD
Inventor： ERNST REICH , WERNER DETTWILER
IPC: C07D209/88 , C07D277/66 , C08K5/32 , C09B1/42 , C09B51/00
CPC classification number: C07D277/66 , C07C2603/48 , C07D209/88 , C08K5/32 , C09B1/42 , C09B51/00
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7.发明授权
公开(公告)号：US3310563A
公开(公告)日：1967-03-21
申请号：US27328563
申请日：1963-04-16
Applicant: HOECHST AG
Inventor： HEINRICH SIEBER , OTTO FUCHS
Abstract: Vat dyes are made by condensing a 41:51-dichloroo 41:51-dibromo-11:81-naphthoylene-benz- or naphthimidazole or substitution product thereof with a 1-amino-anthraquinone in the presence of an acid-binding agent and heating the chlorine- or bromine-containing intermediate thus obtained in the presence of an acid amide which may be substituted at the nitrogen atom, such as acetamide, pyrrolidone, benzamide or phosphoric acid-tris-dimethylamide, and an acid-binding agent in the presence or absence of an organic liquid such as a -chloronaphthalene at temperatures from 150 DEG to 270 DEG C. Olive-green to green vat dyes are obtained.
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公开(公告)号：US3275651A
公开(公告)日：1966-09-27
申请号：US33056363
申请日：1963-12-16
Applicant: GULF RESEARCH DEVELOPMENT CO
Inventor： ELLIS ALAN F , SCHULZ JOHANN G D
IPC: C07C233/00 , C07D209/48 , C09B1/42
CPC classification number: C07D209/48 , C09B1/42 , C10M5/00 , C10M7/00 , C10M2215/068 , C10M2215/08 , C10M2215/082 , C10M2215/086 , C10M2215/12 , C10M2215/122 , C10M2215/28 , C10M2229/02 , C10M2229/05 , C10N2250/10
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公开(公告)号：US3221020A
公开(公告)日：1965-11-30
申请号：US21420862
申请日：1962-08-02
Applicant: BAYER AG
Inventor： RUTGER NEEFF
IPC: C07D513/04 , C09B1/20 , C09B1/22 , C09B1/42 , C09B5/10
CPC classification number: C07D513/04 , C07C2603/24 , C09B1/20 , C09B1/22 , C09B1/42 , C09B5/10
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