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    Method for preparing and using a soluble metal pentafluoride-hydrogen fluoride catalyst
    1.
    发明授权
    Method for preparing and using a soluble metal pentafluoride-hydrogen fluoride catalyst 失效
    制备和使用可溶性金属五氟化氢 - 氟化氢催化剂的方法

    公开(公告)号：US4105704A

    公开(公告)日：1978-08-08

    申请号：US758054

    申请日：1976-12-29

    申请人： Geoffrey R. Say ,  William C. Baird, Jr.

    发明人： Geoffrey R. Say ,  William C. Baird, Jr.

    IPC分类号： B01J27/12 ,  C07C2/54 ,  C07C5/22 ,  C07C3/52 ,  C07C5/24

    CPC分类号： C07C5/2253 ,  B01J27/12 ,  C07C2/54 ,  C07C2527/1206 ,  C07C2527/133 ,  Y10S585/906

    摘要： A soluble HF/TaF.sub.5 catalyst is prepared in the absence of an organic solvent according to the steps of:(1) contacting tantalum metal with substantially anhydrous liquid HF to form soluble TaF.sub.5, the amount of HF being sufficient to maintain the TaF.sub.5 thus formed as a homogeneous substantially liquid phase catalyst at a temperature ranging from about 0.degree. to 150.degree. C.,(2) contacting the catalyst thus formed with a hydrocarbon feedstock in a hydrocarbon conversion process to form an acid catalyst phase and a hydrocarbon product phase,(3) stripping HF from said catalyst phase with a gas containing molecular hydrogen thereby reducing the mole ratio of HF to TaF.sub.5, and(4) passing the stripped acid catalyst phase from step (3) to the hydrocarbon conversion process, thereby maintaining the mole ratio of HF to TaF.sub.5 within said process at a level between that obtained in step (1) and step (3).

    摘要翻译： 根据以下步骤在不存在有机溶剂的情况下制备可溶性HF / TaF 5催化剂：

    Isomerization of tetrahydropolycyclopentadienes to a missile fuel additive
    2.
    发明授权
    Isomerization of tetrahydropolycyclopentadienes to a missile fuel additive 失效
    四氢聚环戊二烯异构化为导弹燃料添加剂

    公开(公告)号：US4086286A

    公开(公告)日：1978-04-25

    申请号：US720306

    申请日：1976-09-03

    申请人： Edward J. Janoski ,  Abraham Schneider ,  Richard E. Ware

    发明人： Edward J. Janoski ,  Abraham Schneider ,  Richard E. Ware

    IPC分类号： C07C5/22 ,  C07C1/00

    CPC分类号： C07C5/2253 ,  C07C2103/68 ,  C07C2103/91 ,  C07C2527/126 ,  Y10S585/905

    摘要： Mixed tetrahydropolycyclopentadienes are isomerized in the presence of anhydrous aluminum trichloride to form an additive suitable for use with a high energy missile fuel. The amount of aluminum trichloride present is such that the weight ratio of trichloride to the tetrahydropolydiene is in the range between from about 0.005 to about 0.75. Also the isomerization involves an inert solvent and is at a temperature between from about -20.degree. C to about 25.degree. C. Also anhydrous hydrogen chloride is present to facilitate the isomerization.

    摘要翻译： 混合的四氢聚环戊二烯在无水三氯化铝存在下异构化，形成适用于高能导弹燃料的添加剂。 存在的三氯化铝的量使得三氯化物与四氢聚二烯的重量比在约0.005至约0.75的范围内。 异构化还涉及惰性溶剂，并且在约-20℃至约25℃之间的温度下。还存在无水氯化氢以促进异构化。

    Hydrocarbon conversion in the presence of a catalyst of a lewis acid intercalated in graphite
    3.
    发明授权
    Hydrocarbon conversion in the presence of a catalyst of a lewis acid intercalated in graphite 失效
    在石墨中嵌入的路易斯酸的催化剂存在下的烃转化

    公开(公告)号：US3925495A

    公开(公告)日：1975-12-09

    申请号：US46731674

    申请日：1974-05-06

    申请人： MOBIL OIL CORP

    发明人： RODEWALD PAUL G

    IPC分类号： C07C5/22 ,  C07C5/27 ,  C07C5/29 ,  C07C5/28

    CPC分类号： C07C5/2724 ,  C07C5/2253 ,  C07C5/2721 ,  C07C5/29 ,  C07C2523/42 ,  C07C2527/126 ,  C07C2527/133 ,  C07C2601/08 ,  Y02P20/582 ,  C07C13/10

    摘要： Hydrocarbon conversion is effected in the presence of a catalyst consisting essentially of graphite having intercalated in the lattice thereof between about 5 and about 75 weight percent of a Lewis acid. The catalyst may additionally have intercalated therein a minor proportion of a Bronsted acid and/or a Group VI-B or Group VIII metal. The catalyst of graphite having the specified components intercalated in its structure is shown to be much more effective in hydrocarbon conversion, e.g., isomerization, than catalysts having said components deposited on the surface of the graphite.

    摘要翻译： 烃转化在催化剂存在下进行，所述催化剂基本上由在其格子中插入约5至约75重量％的路易斯酸之间的石墨组成。 催化剂还可以在其中插入少量的布朗斯台德酸和/或VI-B族或VIII族金属。 具有插入其结构中的特定组分的石墨的催化剂显示出比具有沉积在石墨表面上的所述组分的催化剂在烃转化（例如异构化）中更有效。