Method for preparing triethylenediamine (TEDA)
    1.
    发明授权
    Method for preparing triethylenediamine (TEDA) 失效
    制备三亚乙基二胺(TEDA)的方法

    公开(公告)号:US07754139B2

    公开(公告)日:2010-07-13

    申请号:US10559493

    申请日:2004-06-04

    IPC分类号: B28B3/20

    摘要: An increase in the cutting hardness of a shaped body comprising a crystalline aluminosilicate is achieved by treating the shaped body with a gas comprising water vapor at from 100 to 600° C. and an absolute pressure of from 0.1 to 10 bar for a period of at least 20 hours, and this shaped body having an increased cutting hardness can be used in processes for chemical synthesis, in particular in a process for preparing triethylenediamine (TEDA) by reaction of ethylenediamine (EDA) and/or piperazine (PIP).

    摘要翻译: 包含结晶硅铝酸盐的成形体的切削硬度的增加通过用包含100-600℃的水蒸气和0.1至10巴的绝对压力的气体处理成形体来实现一段时间 至少20小时,具有增加的切削硬度的成形体可用于化学合成的方法中,特别是在通过乙二胺(EDA)和/或哌嗪(PIP)的反应制备三亚乙基二胺(TEDA)的方法中。

    Method for Producing Polyurethane-Soft Foam Materials
    3.
    发明申请
    Method for Producing Polyurethane-Soft Foam Materials 失效
    聚氨酯软泡沫材料的生产方法

    公开(公告)号:US20070282028A1

    公开(公告)日:2007-12-06

    申请号:US11575165

    申请日:2005-09-20

    IPC分类号: C08G18/48

    摘要: The invention relates to a process for producing flexible polyurethane foams, in particular molded flexible polyurethane foams, by reacting a) polyisocyanates with b) compounds having at least two hydrogen atoms which are reactive toward isocyanate groups, wherein at least one polyether alcohol bi) which has been prepared by means of a DMC catalyst and has a hydroxyl number in the range from 15 to 35 mg KOH/g, and ethylene oxide content in the range from 5 to 18% by weight, based on the total weight of the polyether alcohol and an end block of ethylene oxide and propylene oxide having an ethylene oxide content of from 25 to 75% by weight, based on the amount of alkylene oxide in the end block, is used as compound b) having at least two hydrogen atoms which are reactive toward isocyanate groups.

    摘要翻译: 本发明涉及通过使a)多异氰酸酯与b)具有至少两个对异氰酸酯基反应的氢原子的化合物来生产柔性聚氨酯泡沫,特别是模制柔性聚氨酯泡沫的方法,其中至少一种聚醚醇bi) 已经通过DMC催化剂制备,羟值为15至35mg KOH / g,环氧乙烷含量为5至18重量%,基于聚醚醇的总重量 并且使用环氧乙烷和环氧丙烷的端嵌段,其具有25至75重量%的环氧乙烷含量,基于端嵌段中的环氧烷烃的量,作为具有至少两个氢原子的化合物b),其为 对异氰酸酯基反应。

    Method for increasing the cutting hardness of a molded body
    4.
    发明申请
    Method for increasing the cutting hardness of a molded body 失效
    提高成型体的切削硬度的方法

    公开(公告)号:US20060116517A1

    公开(公告)日:2006-06-01

    申请号:US10559493

    申请日:2004-06-04

    IPC分类号: C07D487/04 C04B33/34

    摘要: An increase in the cutting hardness of a shaped body comprising a crystalline aluminosilicate is achieved by treating the shaped body with a gas comprising water vapor at from 100 to 600° C. and an absolute pressure of from 0.1 to 10 bar for a period of at least 20 hours, and this shaped body having an increased cutting hardness can be used in processes for chemical synthesis, in particular in a process for preparing triethylenediamine (TEDA) by reaction of ethylenediamine (EDA) and/or piperazine (PIP).

    摘要翻译: 包含结晶硅铝酸盐的成形体的切削硬度的增加通过用包含100-600℃的水蒸气和0.1至10巴的绝对压力的气体处理成型体达到一段时间 至少20小时,具有增加的切削硬度的成形体可用于化学合成的方法中,特别是在通过乙二胺(EDA)和/或哌嗪(PIP)的反应制备三亚乙基二胺(TEDA)的方法中。

    Use of quinaldine and naphthaline derivatives as crystallisation modifiers

    公开(公告)号:US20060150866A1

    公开(公告)日:2006-07-13

    申请号:US10560039

    申请日:2004-06-08

    IPC分类号: A61K8/49 C08K5/00

    CPC分类号: C09B67/0034 C09B25/00

    摘要: The use of compounds of the general formula I where A is ═N— or ═CH—; X when A is ═N— is methyl or a radical of the formula IIa or when A is ═CH— is an R radical; Y is an R radical or a radical of the formula IIb with either X being a radical of the formula IIa or Y being a radical of the formula IIb; R is hydrogen, halogen, C1-C4-alkyl, —SO3H, —SO3−Me+, —SO3−N+R1R2R3R4, —SO2NR1R2, —CH2NR1R2, —CH2R5, —COOH, —COO−N+R1R2R3R4, —COOR6 or —COR6; R1, R2, R3 and R4 are each independently hydrogen; C1-C22-alkyl or C2-C22-alkenyl whose carbon chain may in either case be interrupted by one or more —O—, —S—, —NR7—, —CO— or —SO2− moieties and/or which may be substituted by one or more of hydroxyl, halogen, aryl, C1-C4-alkoxy and acetyl; C3-C8-cycloalkyl whose carbon skeleton may be interrupted by one or more —O—, —S—, —NR7— or —CO— moieties and/or which may be substituted by one or more of hydroxyl, halogen, aryl, C1-C4-alkoxy and acetyl; hydroabietyl, abietyl or aryl; R1 and R2 or R1, R2 and R3 may combine to form a 5- to 7-membered cyclic radical which contains the nitrogen atom and may contain further hetero atoms; R5 is a radical of the formula IIb′ R6 is one of the R1 alkyl radicals; R7 is hydrogen or C1-C4-alkyl; Me is an alkali metal ion; Z and Z′ are each independently arylene which may be substituted by one or more of halogen, —SO3H, —SO3−Me+, —SO3−N+R1R2R3R4, and C1-C12-alkyl, and the rings B1 and B2 may each be independently additionally substituted by one or more identical or different R radicals other than hydrogen, as crystallization modifiers for organic pigments.

    Use of an Apparatus for Adding at Least One Additive to a Reactor Interior
    10.
    发明申请
    Use of an Apparatus for Adding at Least One Additive to a Reactor Interior 有权
    使用最少添加到反应器内部的装置

    公开(公告)号:US20090008220A1

    公开(公告)日:2009-01-08

    申请号:US11994138

    申请日:2006-07-03

    IPC分类号: B65G33/00

    摘要: The invention relates to the use of an apparatus for adding at least one solid or viscous liquid additive, or an additive dispersed in solvent, to a reactor interior of a reactor for preparing crosslinked, finely divided polymers by copolymerizing (a) water-soluble, monoethylenically unsaturated monomers and (b) from 0.001 to 5 mol %, based on the monomers (a), of monomers comprising at least two polymerizable groups, (c) from 0 to 20 mol %, based on the monomers (a), of water-insoluble monoethylenically unsaturated monomers, where the apparatus comprises at least one screw for conveying the at least one additive and the at least one screw ends in an addition orifice substantially flush with the inner wall of the reactor interior.

    摘要翻译: 本发明涉及一种用于将至少一种固体或粘稠液体添加剂或分散在溶剂中的添加剂添加到用于制备交联的细碎聚合物的反应器内部的装置的用途,其通过以下方式共聚合(a)水溶性, 单烯属不饱和单体和(b)基于单体(a)0.001至5摩尔%的包含至少两个可聚合基团的单体,(c)基于单体(a)的0至20摩尔% 水不溶性单烯属不饱和单体,其中该装置包括用于将至少一种添加剂输送的至少一个螺杆和至少一个与反应器内部的内壁齐平的添加孔的螺杆端。