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    DISPERSION OF HYDROPHOBICIZED SILICON DIOXIDE PARTICLES AND GRANULES THEREOF
    1.
    发明申请
    DISPERSION OF HYDROPHOBICIZED SILICON DIOXIDE PARTICLES AND GRANULES THEREOF 审中-公开
    疏水性二氧化硅二氧化硅颗粒及其颗粒的分散

    公开(公告)号：US20110123806A1

    公开(公告)日：2011-05-26

    申请号：US12996635

    申请日：2009-06-03

    申请人： Wolfgang Lortz ,  Gabriele Perlet ,  Uwe Diener ,  Sascha Reitz

    发明人： Wolfgang Lortz ,  Gabriele Perlet ,  Uwe Diener ,  Sascha Reitz

    IPC分类号： B32B1/00 ,  C09D7/12 ,  B82Y30/00

    CPC分类号： C09C1/3018 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/22 ,  C08K3/36 ,  C08K9/06 ,  C09C1/3063 ,  C09C1/3081 ,  C09C1/309 ,  C09D7/62 ,  C09D7/67 ,  Y10T428/2995

    摘要： Process for preparing a dispersion of surface-modified silicon dioxide particles having an average particle diameter of not more than 100 nm by high-pressure milling of a preliminary dispersion comprising a) 10% to 50% by weight of surface-modified silicon dioxide particles, b) at least one glycol monoether of the general formula (A): H3C(CH2)m—O—(CH2)n—[O—(CH2)o]p—OH, c) at least one carboxylic ester of the general formula (B): H2x+1Cx—O—CH2—(CHR)—[O—CHR]y—O—C(═O)—CzH2z+1, d) the molar ratio A/B being 10:90 to 40:60 and m, n, o, p, x, y and z being independent of one another. Dispersion obtainable by this process. Process for producing granules of surface-modified silicon dioxide particles by separating off the liquid phase of the dispersion. Granules obtainable by this process. Use of dispersion and granules in coating materials.

    摘要翻译： 通过高压研磨预备分散体制备平均粒径不大于100nm的表面改性二氧化硅颗粒的分散体的方法，该预分散体包括a）10重量％至50重量％的表面改性二氧化硅颗粒， b）至少一种通式（A）的二醇单醚：H3C（CH2）m-O-（CH2）n- [O-（CH2）o] p-OH，c）至少一种一般的羧酸酯 式（B）：H2x + 1Cx-O-CH2-（CHR） - [O-CHR] y-O-C（= O）-CzH2z + 1，d）摩尔比A / B为10:90〜 ：60和m，n，o，p，x，y和z彼此独立。 通过该方法可获得的分散体。 通过分离分散体的液相来生产表面改性的二氧化硅颗粒的颗粒的方法。 颗粒可以通过这个过程获得。 在涂料中使用分散体和颗粒。

    PROCESS FOR PREPARING REDISPERSIBLE SURFACE-MODIFIED SILICON DIOXIDE PARTICLES
    2.
    发明申请
    PROCESS FOR PREPARING REDISPERSIBLE SURFACE-MODIFIED SILICON DIOXIDE PARTICLES 有权
    制备可重复表面修饰的二氧化硅颗粒的方法

    公开(公告)号：US20110086958A1

    公开(公告)日：2011-04-14

    申请号：US12996936

    申请日：2009-06-02

    申请人： Wolfgang Lortz ,  Gabriele Perlet ,  Uwe Diener ,  Sascha Reitz

    发明人： Wolfgang Lortz ,  Gabriele Perlet ,  Uwe Diener ,  Sascha Reitz

    IPC分类号： C08K5/5419 ,  C07F7/08 ,  C09J11/06 ,  B24B1/00 ,  B82Y30/00

    CPC分类号： C09C1/3018 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/22 ,  C08K3/36 ,  C08K9/06 ,  C09C1/3081 ,  C09C1/309 ,  C09D7/62 ,  C09D7/67 ,  G03G9/09716 ,  G03G9/09725 ,  Y10T428/2995

    摘要： Process for preparing surface-modified silicon dioxide particles with a mean particle diameter of at most 100 nm, comprising the steps of: a) providing a predispersion b) high-pressure grinding of the predispersion to form a dispersion c) removing the liquid phase of the dispersion, the predispersion comprising a1) surface-modified silicon dioxide particles which are at least partly aggregated, are bonded to the surface-modifying component via Si—O—Si bonds and still have reactive groups on their surface, a2) one or more organosilicon compounds which have at least one silicon-carbon bond and at least one functional group which can react with the reactive groups to form a covalent Si—O—Si bond, and a3) one or more solvents. Redispersible, surface-modified silicon dioxide particles obtainable by this process. Use of these in toner powders, silicone rubber, adhesives and scratch-resistance surface coatings.

    摘要翻译： 制备平均粒径为至多100nm的表面改性二氧化硅颗粒的方法，包括以下步骤：a）提供预分散体b）预分散体的高压研磨以形成分散体c）除去 分散体，包含a1）至少部分聚集的表面改性二氧化硅颗粒的预分散体通过Si-O-Si键与表面改性组分键合，并且在其表面上仍具有反应性基团，a2）一个或多个 具有至少一个硅 - 碳键的有机硅化合物和至少一个可与反应性基团反应形成共价Si-O-Si键的官能团，和a）一种或多种溶剂。 可通过该方法获得的可再分散的表面改性二氧化硅颗粒。 在调色剂粉末，硅橡胶，粘合剂和耐刮擦表面涂层中使用这些。

    Dispersion comprising hydrophobized silicon dioxide particles
    3.
    发明授权
    Dispersion comprising hydrophobized silicon dioxide particles 有权
    分散体包含疏水化二氧化硅颗粒

    公开(公告)号：US08377193B2

    公开(公告)日：2013-02-19

    申请号：US12920216

    申请日：2009-03-05

    申请人： Wolfgang Lortz ,  Gabriele Perlet ,  Uwe Diener ,  Sascha Reitz

    发明人： Wolfgang Lortz ,  Gabriele Perlet ,  Uwe Diener ,  Sascha Reitz

    IPC分类号： C04B14/04 ,  C09K17/02 ,  B01F3/12

    CPC分类号： B01F17/0064 ,  B01F17/0007 ,  B82Y30/00 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/22 ,  C01P2006/90 ,  C08K3/36 ,  C09C1/3063 ,  C09C1/3072 ,  C09D5/027 ,  C09D7/43 ,  C09D7/62

    摘要： Aqueous dispersion which comprises hydrophobized silicon dioxide particles and in each case one or more dispersing additives, a basic composition, and which is free of color pigments, inactive fillers and binders, in which the hydrophobized silicon dioxide particles have a methanol wettability of 30 to 60 and are present in the dispersion with a proportion of 0.1 to 50% by weight,—the proportion of water is 30 to 90% by weight based on the dispersion,—the dispersing additive is at least one phosphate ester of an ethoxylated alcohol having 8 to 18 carbon atoms, the proportion of which is 3 to 25% by weight based on the proportion of the hydrophobized silicon dioxide particles,—the basic composition comprises or consists of one or more amines of the general formula RNH2, R2NH and R3N, where R is an alkyl group or a hydroxyl-substituted alkyl group having in each case 2 to 10 carbon atoms, and is present with a proportion of 5 to 30% by weight based on the proportion of hydrophobized silicon dioxide particles,—the dispersion further comprises one or more polyols having 2 to 15 carbon atoms, the proportion of which is 1 to 10% by weight based on the proportion of hydrophobized silicon dioxide particles,—the pH of the dispersion being 9 to 11.

    摘要翻译： 水分散体，其包含疏水化二氧化硅颗粒，并且在每种情况下为一种或多种分散添加剂，碱性组合物，并且不含有颜色的颜料，无活性填料和粘合剂，其中疏水化二氧化硅颗粒的甲醇润湿性为30至60 并且以分散体的比例为0.1〜50重量％存在于分散体中， - 基于分散体的水的比例为30〜90重量％，分散添加剂为至少1种具有8个乙氧基化物的乙氧基化醇的磷酸酯 至18个碳原子，其比例为3-25重量％，基于疏水化二氧化硅颗粒的比例，碱性组成包含一种或多种通式为RNH 2，R 2 NH和R 3 N的胺，其中 R是烷基或羟基取代的烷基，每个碳原子数为2至10个，并且以疏水化比例为基准存在5至30重量％的比例 d二氧化硅颗粒， - 分散体还包含一种或多种具有2至15个碳原子的多元醇，其比例为疏水化二氧化硅颗粒的比例为1至10重量％， - 分散体的pH为9 到11岁

    DISPERSION COMPRISING HYDROPHOBIZED SILICON DIOXIDE PARTICLES
    4.
    发明申请
    DISPERSION COMPRISING HYDROPHOBIZED SILICON DIOXIDE PARTICLES 有权
    分散含有二氧化硅的二氧化硅颗粒

    公开(公告)号：US20110000397A1

    公开(公告)日：2011-01-06

    申请号：US12920216

    申请日：2009-03-05

    申请人： Wolfgang Lortz ,  Gabriele Perlet ,  Uwe Diener ,  Sascha Reitz

    发明人： Wolfgang Lortz ,  Gabriele Perlet ,  Uwe Diener ,  Sascha Reitz

    IPC分类号： C09D7/00

    CPC分类号： B01F17/0064 ,  B01F17/0007 ,  B82Y30/00 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/22 ,  C01P2006/90 ,  C08K3/36 ,  C09C1/3063 ,  C09C1/3072 ,  C09D5/027 ,  C09D7/43 ,  C09D7/62

    摘要： Aqueous dispersion which comprises hydrophobized silicon dioxide particles and in each case one or more dispersing additives, a basic composition, and which is free of colour pigments, inactive fillers and binders, in which the hydrophobized silicon dioxide particles have a methanol wettability of 30 to 60 and are present in the dispersion with a proportion of 0.1 to 50% by weight,—the proportion of water is 30 to 90% by weight based on the dispersion,—the dispersing additive is at least one phosphate ester of an ethoxylated alcohol having 8 to 18 carbon atoms, the proportion of which is 3 to 25% by weight based on the proportion of the hydrophobized silicon dioxide particles,—the basic composition comprises or consists of one or more amines of the general formula RNH2, R2NH and R3N, where R is an alkyl group or a hydroxyl-substituted alkyl group having in each case 2 to 10 carbon atoms, and is present with a proportion of 5 to 30% by weight based on the proportion of hydrophobized silicon dioxide particles,—the dispersion further comprises one or more polyols having 2 to 15 carbon atoms, the proportion of which is 1 to 10% by weight based on the proportion of hydrophobized silicon dioxide particles,—the pH of the dispersion being 9 to 11.

    摘要翻译： 水分散体，其包含疏水化二氧化硅颗粒，并且在每种情况下为一种或多种分散添加剂，碱性组合物，并且不含颜料，无活性填料和粘合剂，其中疏水化二氧化硅颗粒的甲醇润湿性为30至60 并且以分散体的比例为0.1〜50重量％存在于分散体中， - 基于分散体的水的比例为30〜90重量％，分散添加剂为至少1种具有8个乙氧基化物的乙氧基化醇的磷酸酯 至18个碳原子，其比例为3-25重量％，基于疏水化二氧化硅颗粒的比例，碱性组成包含一种或多种通式为RNH 2，R 2 NH和R 3 N的胺，其中 R为烷基或羟基取代的烷基，每种情况为2至10个碳原子，并且以疏水物比例为基准计，按重量计5至30％ 二氧化硅颗粒， - 分散体还包含一种或多种碳原子数为2〜15的多元醇，其比例为疏水化二氧化硅颗粒的比例为1〜10重量％，分散体的pH为9 到11岁

    Process for preparing redispersible surface-modified silicon dioxide particles
    5.
    发明授权
    Process for preparing redispersible surface-modified silicon dioxide particles 有权
    制备可再分散表面改性二氧化硅颗粒的方法

    公开(公告)号：US08399093B2

    公开(公告)日：2013-03-19

    申请号：US12996936

    申请日：2009-06-02

    申请人： Wolfgang Lortz ,  Gabriele Perlet ,  Uwe Diener ,  Sascha Reitz

    发明人： Wolfgang Lortz ,  Gabriele Perlet ,  Uwe Diener ,  Sascha Reitz

    IPC分类号： B32B18/00 ,  B02C19/06

    CPC分类号： C09C1/3018 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/22 ,  C08K3/36 ,  C08K9/06 ,  C09C1/3081 ,  C09C1/309 ,  C09D7/62 ,  C09D7/67 ,  G03G9/09716 ,  G03G9/09725 ,  Y10T428/2995

    摘要： Provided is a process for preparing surface-modified silicon dioxide particles with a mean particle diameter of at most 100 nm, involving (A) high-pressure grinding of a predispersion having (i) surface-modified silicon dioxide particles which are at least partly aggregated, are bonded to the surface-modifying component via Si—O—Si bonds, and still have reactive groups on their surface; (ii) an organosilicon compound which has a silicon-carbon bond and a functional group which can react with the reactive groups to form a covalent Si—O—Si bond; and (iii) a solvent, to form a dispersion; and (B) removing the liquid phase of the dispersion. Also provided are redispersible, surface-modified silicon dioxide particles obtained by this process, and their use in toner powders, silicone rubber, adhesives, and scratch-resistance surface coatings.

    摘要翻译： 提供了一种制备平均粒径为至多100nm的表面改性二氧化硅颗粒的方法，包括（A）高压研磨预分散体，其具有（i）至少部分聚集的表面改性的二氧化硅颗粒 通过Si-O-Si键与表面改性组分键合，并在其表面上仍具有反应性基团; （ii）具有硅 - 碳键和可与反应性基团反应形成共价Si-O-Si键的官能团的有机硅化合物; 和（iii）溶剂，形成分散体; 和（B）除去分散体的液相。 还提供了通过该方法获得的可再分散的表面改性的二氧化硅颗粒，以及它们在调色剂粉末，硅橡胶，粘合剂和耐刮擦表面涂层中的用途。

    DISPERSION CONTAINING TITANIUM DIOXIDE
    6.
    发明申请
    DISPERSION CONTAINING TITANIUM DIOXIDE 有权
    含二氧化钛的分散体

    公开(公告)号：US20080098932A1

    公开(公告)日：2008-05-01

    申请号：US11572018

    申请日：2005-07-05

    申请人： Gabriele Perlet ,  Wolfgang Lortz ,  Christoph Batz-Sohn ,  Werner Will ,  Sascha Reitz

    发明人： Gabriele Perlet ,  Wolfgang Lortz ,  Christoph Batz-Sohn ,  Werner Will ,  Sascha Reitz

    IPC分类号： B05D1/00

    CPC分类号： C03C17/256 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2006/12 ,  C03C2217/212 ,  C03C2218/113 ,  C04B41/009 ,  C04B41/5041 ,  C04B41/87 ,  C04B2111/00586 ,  C04B2111/2061 ,  C04B2111/60 ,  C09C1/3669 ,  C09D17/008 ,  C04B41/4539 ,  C04B33/00

    摘要： Aqueous dispersion obtainable by placing in water an aggregated titanium dioxide powder having a specific surface area of from 20 to 150 m2/g in such an amount that the desired dispersion comprises at least 20 wt. % titanium dioxide, and at least onc amino alcohol having from 1 to 6 carbon atoms, and at least one carboxylic acid from the group comprising dibasic carboxylic acids and/or hydroxycarboxylic acids having from 2 to 6 carbon atoms,—the amino alcohol being present in the dispersion in an amount of from 2.5 to 7.0 μmol./m2 specific surface area TiO2 and the carboxylic acid being present in an amount of from 1.0 to 3.5 μmol./m specific surface area TiO2,—producing a pre-dispersion by introducing energy in an amount of less than 200 kJ/m3 and then producing a dispersion in which the aggregated titanium dioxide powder has a mean, volume-related aggregate diameter of less than 150 nm by grinding the pre-dispersion by means of a high-energy mill at a pressure of at least 500 bar. The dispersion can be used in the coating of glass, ceramics and metal surfaces.

    摘要翻译： 通过将具有20至150m 2 / g比表面积的聚集二氧化钛粉末放入水中而得到的水分散体，其量使得所需分散体包含至少20wt。 ％二氧化钛和至少具有1至6个碳原子的氨基醇，以及至少一种含有2至6个碳原子的二元羧酸和/或羟基羧酸的羧酸， - 存在的氨基醇 在分散体中的量为2.5-7.0μmol/ m 2 SO 3比表面积TiO 2和羧酸的存在量为1.0-3.5μmolol ./m比表面积TiO 2， - 通过引入少于200kJ / m 3的量的能量产生预分散，然后产生分散体，其中 通过在至少500巴的压力下通过高能研磨机研磨预分散体，聚集的二氧化钛粉末具有小于150nm的平均体积相关聚集体直径。 分散体可用于玻璃，陶瓷和金属表面的涂层。

    Dispersion containing titanium dioxide
    9.
    发明授权
    Dispersion containing titanium dioxide 有权
    含二氧化钛的分散体

    公开(公告)号：US07780777B2

    公开(公告)日：2010-08-24

    申请号：US11572018

    申请日：2005-07-05

    申请人： Gabriele Perlet ,  Wolfgang Lortz ,  Christoph Batz-Sohn ,  Werner Will ,  Sascha Reitz

    发明人： Gabriele Perlet ,  Wolfgang Lortz ,  Christoph Batz-Sohn ,  Werner Will ,  Sascha Reitz

    IPC分类号： C23C16/40 ,  C09C1/36 ,  C01G23/047

    CPC分类号： C03C17/256 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2006/12 ,  C03C2217/212 ,  C03C2218/113 ,  C04B41/009 ,  C04B41/5041 ,  C04B41/87 ,  C04B2111/00586 ,  C04B2111/2061 ,  C04B2111/60 ,  C09C1/3669 ,  C09D17/008 ,  C04B41/4539 ,  C04B33/00

    摘要： An aqueous dispersion that can be used in the coating of glass, ceramics and metal surfaces is prepared by placing, in water, an aggregated titanium dioxide powder having a specific surface area of from 20 to 150 m2/g in such an amount that the desired dispersion contains at least 20 wt. % titanium dioxide, and at least one amino alcohol having from 1 to 6 carbon atoms, and at least one carboxylic acid selected from dibasic carboxylic acids and/or hydroxycarboxylic acids having from 2 to 6 carbon atoms. A pre-dispersion is produced by introducing energy in an amount of less than 200 kJ/m3. Then a dispersion is produced in which the aggregated titanium dioxide powder has a mean, volume-related aggregate diameter of less than 150 nm by grinding the pre-dispersion with a high-energy mill at a pressure of at least 500 bar.

    摘要翻译： 可用于玻璃，陶瓷和金属表面涂层的水分散体通过将具有20至150m 2 / g比表面积的聚集二氧化钛粉末放置在水中制备，其量为所需的量 分散体含有至少20wt。 ％二氧化钛和至少一种具有1至6个碳原子的氨基醇，以及至少一种选自具有2至6个碳原子的二元羧酸和/或羟基羧酸的羧酸。 通过引入少于200kJ / m 3的量的能量来产生预分散体。 然后产生分散体，其中通过在至少500巴的压力下用高能磨机研磨预分散体，其中聚集的二氧化钛粉末具有小于150nm的平均体积相关聚集体直径。