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公开(公告)号：US5234715A
公开(公告)日：1993-08-10
申请号：US742640
申请日：1991-08-07
CPC分类号： H01Q15/145 , F41J2/00
摘要： An article comprising a non-conductive substrate having a sub-micron thickness of an oxidizable conductive first metal coating thereon, and a second (promoter) metal which is galvanically effective to promote the corrosion of the first metal, discontinuously coated on the first metal coating. Optionally, the second metal-doped, first metal-coated substrate may be further coated with a salt, to accelerate the galvanic corrosion reaction by which the conductive first metal coating is oxidized. Also disclosed is a related method of forming such articles, comprising chemical vapor depositing the first metal on the substrate and chemical vapor depositing the second metal on the applied first metal coating, and of optionally applying a salt by salt solution contacting of the second metal-doped, first metal-coated substrate. When utilized in a form comprising fine-diameter substrate elements such as glass or ceramic filaments, the resulting product may be usefully employed as an evanescent chaff. In the presence of atmospheric moisture, such evanescent chaff undergoes oxidation of the first metal coating so that the radar signature of the chaff transiently decays.
摘要翻译： 一种制品，其包括其上具有亚微米厚度的可氧化导电第一金属涂层的非导电基底和第二（促进剂）金属，其具有电流有效以促进第一金属的腐蚀，不连续地涂覆在第一金属涂层上 。 任选地，第二金属掺杂的第一金属涂覆的基底可以进一步涂覆盐，以加速导电的第一金属涂层被氧化的电偶腐蚀反应。 还公开了形成这种制品的相关方法，包括在基底上化学气相沉积第一金属和化学气相沉积所施加的第一金属涂层上的第二金属，以及任选地通过与第二金属 - 掺杂的第一金属涂覆的基底。 当以包括诸如玻璃或陶瓷细丝的细直径基底元件的形式使用时，所得产物可有效地用作ev逝的谷壳。 在存在大气水分的情况下，这种消逝的小麦经历第一金属涂层的氧化，使得谷壳的雷达标记瞬时衰变。
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公开(公告)号：US5039990A
公开(公告)日：1991-08-13
申请号：US449708
申请日：1989-12-11
CPC分类号： F41J2/00 , H01Q15/145 , Y10S204/06 , Y10T428/12396 , Y10T428/12535 , Y10T428/12882 , Y10T428/12917
摘要： An article comprising a non-conductive substrate having a sub-micron thickness of an oxidizable conductive first metal coating thereon, and a second (promoter) metal which is galvanically effective to promote the corrosion of the first metal, discontinuously coated on the first metal coating. Optionally, the second metal-doped, first metal-coated substrate may be further coated with a salt, to accelerate the galvanic corrosion reaction by which the conductive first metal coating is oxidized. Also disclosed is a related method of forming such articles, comprising chemical vapor depositing the first metal on the substrate and chemical vapor depositing the second metal on the applied first metal coating, and of optionally applying a salt by salt solution contacting of the second metal-doped, first metal-coated substrate. When utilized in a form comprising fine-diameter substrate elements such as glass or ceramic filaments, the resulting product may be usefully employed as an evanescent chaff. In the presence of atmosphere moisture, such evanescent chaff undergoes oxidation of the first metal coating so that the radar signature of the chaff transiently decays.
摘要翻译： 一种制品，其包括其上具有亚微米厚度的可氧化导电第一金属涂层的非导电基底和第二（促进剂）金属，其具有电流有效以促进第一金属的腐蚀，不连续地涂覆在第一金属涂层上 。 任选地，第二金属掺杂的第一金属涂覆的基底可以进一步涂覆盐，以加速导电的第一金属涂层被氧化的电偶腐蚀反应。 还公开了形成这种制品的相关方法，包括在基底上化学气相沉积第一金属和化学气相沉积所施加的第一金属涂层上的第二金属，以及任选地通过与第二金属 - 掺杂的第一金属涂覆的基底。 当以包括诸如玻璃或陶瓷细丝的细直径基底元件的形式使用时，所得产物可有效地用作ev逝的谷壳。 在气氛水分存在的情况下，这种消逝的壳体经历第一金属涂层的氧化，使得谷壳的雷达标记瞬时衰减。
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3.发明授权Sulfurized chaff fiber having an evanescent radar reflectance characteristic, and method of making the same 失效具有ev逝雷达反射特性的硫化谷壳纤维及其制造方法
公开(公告)号：US5352519A
公开(公告)日：1994-10-04
申请号：US982393
申请日：1992-11-27
申请人： Ward C. Stevens , Edward A. Sturm , Bruce C. Roman
发明人： Ward C. Stevens , Edward A. Sturm , Bruce C. Roman
CPC分类号： H01Q15/145 , F41J2/00 , Y10T428/2904 , Y10T428/2913 , Y10T428/2918 , Y10T428/2933 , Y10T428/294 , Y10T428/2944 , Y10T428/2949 , Y10T428/2956 , Y10T428/2958 , Y10T428/2964
摘要： An article comprising a non-conductive substrate having a sub-micron thickness of a sulfur-doped oxidizable metal coating thereon. Optionally, the sulfur-doped oxidizable metal-coated substrate may be further coated with (i) a promoter metal which is galvanically effective to promote the corrosion of the oxidizable metal, discontinuously coated on the oxidizable metal coating, and/or (ii) a salt, to accelerate the galvanic corrosion reaction by which the oxidizable metal coating is oxidized. When utilized in a form comprising fine diameter substrate elements such as glass or ceramic filaments, the resulting product may usefully be employed as an evanescent chaff. In the presence of atmospheric moisture, such evanescent chaff undergoes oxidation of the oxidizable metal coating so that the radar signature of the chaff transiently decays.
摘要翻译： 一种制品，其包含其上具有亚硫酸盐可氧化金属涂层的亚微米厚度的非导电基底。 任选地，可掺入可掺硫的可氧化金属的基底可以进一步涂覆（i）助催化剂金属，其是电流有效的，以促进不可分散涂覆在可氧化金属涂层上的可氧化金属的腐蚀，和/或（ii） 盐，以加速可氧化金属涂层氧化的电偶腐蚀反应。 当以包括诸如玻璃或陶瓷细丝的细直径基底元件的形式使用时，所得到的产品可有效地用作渐逝的谷壳。 在大气水分存在的情况下，这种消逝的小麦经历可氧化金属涂层的氧化，使得谷壳的雷达信号瞬时衰减。
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4.发明授权Method of making a salt-doped metal-coated article having an evanescent electromagnetic detection signature 失效制备具有ev逝电磁检测标记的盐掺杂金属涂覆制品的方法
公开(公告)号：US5328717A
公开(公告)日：1994-07-12
申请号：US734199
申请日：1991-07-22
申请人： Ward C. Stevens , Edward A. Sturm , Bruce C. Roman
发明人： Ward C. Stevens , Edward A. Sturm , Bruce C. Roman
CPC分类号： F41J2/00 , H01Q15/145 , Y10T428/265 , Y10T428/2944
摘要： An article comprising a non-conductive substrate having a sub-micron thickness of an oxidizable metal coating thereon, and an oxidation enhancingly effective amount of a salt, e.g., from about 0.005 to about 25% by weight of salt, based on the weight of oxidizable metal, present on the oxidizable metal coating. Also disclosed is a related method of forming such article, comprising chemical vapor depositing the oxidizable metal coating on the substrate, applying the salt by contacting of the oxidizable metal-coated substrate with a salt solution, and drying of the salt solution on the oxidizable metal film to yield the product salt-doped, oxidizable metal-coated substrate article. When utilized in a form comprising fine-diameter substrate elements such as glass or ceramic filaments, the resulting product may be usefully employed as an "evanescent" chaff. In the presence of atmospheric moisture, such evanescent chaff undergoes oxidization of the oxidizable metal coating so that the radar signature of the chaff transiently decays, with the level of salt doping of the oxidizable metal film being variable to achieve a desired functional life and decay rate of the chaff radar signature.
摘要翻译： 一种制品，其包含其上具有亚微米厚度的可氧化金属涂层的非导电基材，以及氧化增强有效量的盐，例如约0.005至约25重量％的盐，基于 存在于可氧化金属涂层上的可氧化金属。 还公开了形成这种制品的相关方法，包括在基底上化学气相沉积可氧化金属涂层，通过使可氧化金属涂覆的基底与盐溶液接触来施加盐，并将盐溶液干燥在可氧化金属上 产生盐掺杂的，可氧化的金属涂覆的基材制品。 当以包括诸如玻璃或陶瓷细丝的细直径基底元件的形式使用时，所得产物可有效地用作“ev逝”谷物。 在大气湿度的存在下，这种消逝的小麦经历可氧化金属涂层的氧化，使得谷壳的雷达标记瞬时衰减，可氧化金属膜的盐掺杂水平是可变的，以达到所需的功能寿命和衰变速率 的屁股雷达签名。
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5.发明授权Salt-doped chaff fiber having an evanescent electromagnetic detection signature, and method of making the same 失效具有ev逝电磁检测标记的盐掺杂谷壳纤维及其制造方法
公开(公告)号：US5034274A
公开(公告)日：1991-07-23
申请号：US448252
申请日：1989-12-11
申请人： Ward C. Stevens , Edward A. Sturm , Bruce C. Roman
发明人： Ward C. Stevens , Edward A. Sturm , Bruce C. Roman
CPC分类号： F41J2/00 , H01Q15/145 , Y10T428/265 , Y10T428/2944
摘要： An article comprising a non-conductive substrate having a sub-micron thickness of an oxidizable metal coating thereon, and an oxidation enhancingly effective amount of a salt, e.g., from about 0.005 to about 25% by weight of salt, based on the weight of oxidizable metal, present on the oxidizable metal coating. Also disclosed is a related method of forming such article, comprising chemical vapor depositing the oxidizable metal coating on the substrate, applying the salt by contacting of the oxidizable metal-coated substrate with a salt solution, and drying of the salt solution on the oxidizable metal film to yield the product salt-doped, oxidizable metal-coated substrate article. When utilized in a form comprising fine-diameter substrate elements such as glass or ceramic filaments, the resulting product may be usefully employed as an "evanescent" chaff. In the presence of atmospheric moisture, such evanescent chaff undergoes oxidization of the oxidizable metal coating so that the radar signature of the chaff transiently decays, with the level of salt doping of the oxidizabale metal film being variable to achieve a desired functional life and decay rate of the chaff radar signature.
摘要翻译： 一种制品，其包含其上具有亚微米厚度的可氧化金属涂层的非导电基材，以及氧化增强有效量的盐，例如约0.005至约25重量％的盐，基于 存在于可氧化金属涂层上的可氧化金属。 还公开了形成这种制品的相关方法，包括在基底上化学气相沉积可氧化金属涂层，通过使可氧化金属涂覆的基底与盐溶液接触来施加盐，并将盐溶液干燥在可氧化金属上 产生盐掺杂的，可氧化的金属涂覆的基材制品。 当以包括诸如玻璃或陶瓷细丝的细直径基底元件的形式使用时，所得产物可有效地用作“ev逝”谷物。 在存在大气湿度的情况下，这种消逝的小麦经历可氧化金属涂层的氧化，使得谷壳的雷达标记瞬时衰变，氧化物金属膜的盐掺杂水平可变，以达到所需的功能寿命和衰变速率 的屁股雷达签名。
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6.发明授权
公开(公告)号：US5880692A
公开(公告)日：1999-03-09
申请号：US475744
申请日：1995-06-07
申请人： Ward C. Stevens , Edward A. Sturm
发明人： Ward C. Stevens , Edward A. Sturm
CPC分类号： G01S7/495 , F41J2/00 , H01Q15/145 , H01Q17/00 , Y10T428/265 , Y10T428/2944
摘要： An article comprising a non-conductive substrate, preferably of an environmentally degradeable character, having a thickness of an oxidizable metal coating thereon, and optionally an oxidation enhancingly effective amount of a salt, e.g., from about 0.005 to about 25% by weight of salt, based on the weight of oxidizable metal, present on the oxidizable metal coating. Also disclosed is a related method of forming such article, comprising chemical vapor depositing the oxidizable metal coating on the substrate. When utilized in a form comprising fine-diameter substrate elements such as filaments, the resulting product may be usefully employed as an "evanescent" chaff. In the presence of atmospheric moisture, such evanescent chaff undergoes oxidization of the oxidizable metal coating so that the conductivity and radar absorbance/reflectance characteristics of the chaff transiently decays.
摘要翻译： 一种包含其上具有可氧化金属涂层厚度的非导电性底物，优选具有环境可降解特性的制品，以及任选的氧化增强有效量的盐，例如约0.005至约25重量％的盐 ，基于可氧化金属的重量，存在于可氧化金属涂层上。 还公开了形成这种制品的相关方法，包括在基底上化学气相沉积可氧化金属涂层。 当以包括诸如细丝的细直径基底元件的形式使用时，所得到的产品可以有用地用作“ev逝”谷物。 在大气湿度的存在下，这种消逝的小麦经历可氧化金属涂层的氧化，使得谷壳的电导率和雷达吸收/反射特性瞬间衰减。
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7.发明授权Metal-coated substrate articles responsive to electromagnetic radiation, and method of making the same 失效金属涂覆的基片制品对电磁辐射的响应及其制备方法
公开(公告)号：US5686178A
公开(公告)日：1997-11-11
申请号：US273356
申请日：1994-07-11
申请人： Ward C. Stevens , Edward A. Sturm
发明人： Ward C. Stevens , Edward A. Sturm
CPC分类号： G01S7/495 , F41J2/00 , H01Q15/145 , H01Q17/00 , Y10T428/265 , Y10T428/2944
摘要： An article comprising a non-conductive substrate, preferably of an environmentally degradeable character, having a thickness of an oxidizable metal coating thereon, and optionally an oxidation enhancingly effective amount of a salt, e.g., from about 0.005 to about 25% by weight of salt, based on the weight of oxidizable metal, present on the oxidizable metal coating. Also disclosed is a related method of forming such article, comprising chemical vapor depositing the oxidizable metal coating on the substrate. When utilized in a form comprising fine-diameter substrate elements such as filaments, the resulting product may be usefully employed as an "evanescent" chaff. In the presence of atmospheric moisture, such evanescent chaff undergoes oxidization of the oxidizable metal coating so that the conductivity and radar absorbance/reflectance characteristics of the chaff transiently decays.
摘要翻译： 一种包含其上具有可氧化金属涂层厚度的非导电性底物，优选具有环境可降解特性的制品，以及任选的氧化增强有效量的盐，例如约0.005至约25重量％的盐 ，基于可氧化金属的重量，存在于可氧化金属涂层上。 还公开了形成这种制品的相关方法，包括在基底上化学气相沉积可氧化金属涂层。 当以包括诸如细丝的细直径基底元件的形式使用时，所得到的产品可以有用地用作“ev逝”谷物。 在大气湿度的存在下，这种消逝的小麦经历可氧化金属涂层的氧化，使得谷壳的电导率和雷达吸收/反射特性瞬间衰减。
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8.发明授权Infrared radiation-interactive article, and method of generating a transient infrared radiation response 失效红外辐射交互制品，以及产生瞬态红外辐射响应的方法
公开(公告)号：US5571621A
公开(公告)日：1996-11-05
申请号：US487836
申请日：1995-06-07
申请人： Ward C. Stevens , Edward A. Sturm
发明人： Ward C. Stevens , Edward A. Sturm
CPC分类号： F41J2/00 , F41H3/00 , G01S7/495 , H01Q15/145 , H01Q17/00 , Y10T428/265 , Y10T428/2904 , Y10T428/2913 , Y10T428/2918 , Y10T428/2933 , Y10T428/294 , Y10T428/2944 , Y10T428/2949 , Y10T428/2958 , Y10T428/2964
摘要： An infrared radiation-interactive article comprising a supported or unsupported oxidizable metal film of an infrared radiation-interactive size and shape, with an oxidation-promoting salt in contact with the metal film, arranged so that in exposure to ambient moisture, the metal film is oxidizable to an infrared radiation non-interactive form. The article of the invention may be employed to carry out a method of generating a transient infrared radiation response, e.g., an infrared radiation reflectance signature, or infrared radiation absorption, at a selected locus receiving infrared radiation incident thereon, by disposing at the locus an infrared radiation interactively-effective amount of such infrared radiation-interactive article.
摘要翻译： 一种红外线辐射交互制品，其包括红外辐射交互尺寸和形状的被负载或未负载的可氧化金属膜，其具有与金属膜接触的氧化促进盐，其被布置成使得在暴露于环境湿度下，金属膜为 可氧化成红外辐射非交互形式。 可以采用本发明的物品来实现一种在所选择的接收入射到其上的红外辐射的轨迹上产生瞬态红外辐射响应的方法，例如红外辐射反射特征或红外辐射吸收， 红外辐射交互式有效量的这种红外辐射互动文章。
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9.发明授权
公开(公告)号：US5087515A
公开(公告)日：1992-02-11
申请号：US449695
申请日：1989-12-11
申请人： Ward C. Stevens , Edward A. Sturm , Bruce C. Roman
发明人： Ward C. Stevens , Edward A. Sturm , Bruce C. Roman
CPC分类号： H01Q15/145 , F41J2/00 , Y10T428/24997 , Y10T428/249978 , Y10T428/249979 , Y10T428/24998 , Y10T428/2918 , Y10T428/294 , Y10T428/2942 , Y10T428/2944 , Y10T428/2949 , Y10T428/2956 , Y10T428/2958 , Y10T428/296 , Y10T428/2964
摘要： An article comprising a non-conductive substrate which is coated with a sub-micron thickness of an oxidizable metal and overcoated with a microporous layer of an inorganic electrically insulative material. Optionally, the oxidizable metal-coated substrate may be sulfurized and/or further coated with (i) a promoter metal which is galvanically effective to promote the corrosion of the oxidizable metal, discontinuously coated on the oxidizable metal coating, and/or (ii) a salt, to accelerate the galvanic corrosion reaction by which the oxidizable metal coating is oxidized, prior to overcoating with the microporous insulative layer. Also disclosed is a related method of forming such articles, comprising chemical vapor depositing the oxidizable metal coating on the substrate and contacting the metallized substrate with a sol gel dispersion of the inorganic electrically insulative material which then is dried under suitable conditions to form the microporous layer on the substrate. When utilized in a form comprising fine diameter substrate elements such as glass or ceramic filaments, the resulting product may usefully be employed as an evanescent chaff. In the presence of atmospheric moisture, such evanescent chaff undergoes oxidation of the oxidizable metal coating so that the radar signature of the chaff transiently decays.
摘要翻译： 一种制品，其包括涂覆有亚微米厚度的可氧化金属并用无机电绝缘材料的微孔层涂覆的非导电基底。 任选地，可氧化金属涂覆的基底可以被硫化和/或进一步涂覆（i）催化有效的助催化剂金属，以促进可分解涂覆在可氧化金属涂层上的可氧化金属的腐蚀，和/或（ii） 在用微孔绝缘层覆盖之前加速可氧化金属涂层被氧化的电偶腐蚀反应。 还公开了形成这种制品的相关方法，包括在基底上化学气相沉积可氧化金属涂层并使金属化基底与无机电绝缘材料的溶胶凝胶分散体接触，然后在合适的条件下干燥以形成微孔层 在基板上。 当以包括诸如玻璃或陶瓷细丝的细直径基底元件的形式使用时，所得到的产品可有效地用作渐逝的谷壳。 在大气水分存在的情况下，这种消逝的小麦经历可氧化金属涂层的氧化，使得谷壳的雷达信号瞬时衰减。
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公开(公告)号：US4759950A
公开(公告)日：1988-07-26
申请号：US913000
申请日：1986-09-26
申请人： Ward C. Stevens
发明人： Ward C. Stevens
CPC分类号： C23C16/16 , C23C16/545
摘要： A method for metallizing a filament, wherein the filament is initially coated with a sol gel dispersion of polysilicate, titania, or alumina, and after drying at elevated temperature to form a porous interlayer coating on the filament, a nickel coating is deposited thereon from gaseous nickel carbonyl in a metallizing zone. The gaseous nickel carbonyl is produced in a fluidized bed of particulate nickel through which carbon monoxide make-up and at least a portion of the effluent gases discharged from the metallizing zone are flowed. The resulting nickel coated filament may be cut into fibers for use as a reinforcement in composite materials such as those utilized in electromagnetic inteference (EMI) shielding applications.
摘要翻译： 一种用于金属化长丝的方法，其中丝线首先用聚硅酸盐，二氧化钛或氧化铝的溶胶凝胶分散体包衣，并且在升高的温度下干燥以在长丝上形成多孔中间层涂层，从其上沉积镍涂层 金属化区域中的羰基镍。 气态镍羰基在颗粒状镍的流化床中产生，一氧化碳组成的流化床中，并且从金属化区域排出的至少一部分流出气体流动。 所得的镍涂层长丝可以被切割成纤维，用作复合材料中的增强材料，例如在电磁干扰（EMI）屏蔽应用中使用的那些。
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