Method of preparing a catalyst
    3.
    发明授权

    公开(公告)号:US3751380A

    公开(公告)日:1973-08-07

    申请号:US3751380D

    申请日:1971-12-06

    发明人: O HARA M

    CPC分类号: B01J37/20 C10G45/08

    摘要: A METHOD OF PREPARING A HYDROREFINING CATALYST FOR THE CONVERSION OF C7-INSOLUBLE ASPHALTENES AND SULFUROUS COMPONENTS IN A RESIDUAL OIL. THE CATALYST COMPRISES A REFRACTORY INORGANIC OXIDE CARRIER MATERIAL IMPREGNATED WITH A METAL OR GROUPS VI-B AND VIII. IMPROVED ACTIVITY AND STABILITY RESULTS FROM NOVEL OXIDIZING AND REDUCING PROCEDURES PRIOR TO SULFIDING OF THE CATALYST.

    Method of preparing a catalyst for the hydrorefining of residual oils

    公开(公告)号:US3746660A

    公开(公告)日:1973-07-17

    申请号:US3746660D

    申请日:1971-12-06

    发明人: O HARA M

    摘要: AN IMPROVED METHOD OF PREPARING A CATALYST COMPRISING A GROUP VI-B AND GROUP VIII METAL IMPREGNATED ON A REFRACTORY INORGANIC OXIDE CARRIER MATERIAL, SAID CATALYST BEING PARTICULARLY USEFUL IN THE HYDROREFINING OF RESIDUAL OILS OF HIGH ASPHALTENE CONTENT. THE CARRIER MATERIAL, PRIOR TO IMPREGNATION WITH THE GROUP VI-B AND GROUP VIII METAL COMPONENTS, IS DRIED TO REDUCE THE VOLATILE CONTENT THEREOF TO NOT LESS THAN ABOUT 30 WT. PERCENT, AND CALCINED IN AN OXIDIZING ATMOSPHERE AT A TEMPERATURE INCREASING FROM ABOUT 200* TO ABOUT 600*C. IN A PERIOD FROM ABOUT 30 TO ABOUT 90 MINUTES, AND THEREAFTER AT A TEMPERATURE OF FROM ABOUT 600* TO ABOUT 800*C. THE CATALYST SO PREPARED IS DESIGNED PRIMARILY FOR THE CONVERSION OF C7ISOLUBLE ASPHALTENES.